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White Phosphorus
just for curiosity - why do you need dry wp in ether? |
14-9-2021 at 08:09
by: B.D.E |
White Phosphorus
I think it's better to just transfer it into a beaker with dry inert solvent, then to another one an ... |
14-9-2021 at 08:07
by: B.D.E |
preparation of barbituric acid (question about the mechanism)
Hey there, so here's the preparation:
[file]90100[/file]
I don't understand the purpose of the N ... |
31-8-2021 at 15:56
by: B.D.E |
Preparation of n-butylamine(consult)
So after about 40 hours at ~60-65C(with s.stirring) - almost none of my n-chlorobutane converted to ... |
7-10-2020 at 04:41
by: B.D.E |
Preparation of n-butylamine(consult)
Thanks for all the ideas and information! It really expanded my mind and knowledge on the matter, wh ... |
26-9-2020 at 02:48
by: B.D.E |
Preparation of n-butylamine(consult)
[rquote=645044&tid=156202&author=stoichiometric_steve][rquote=645041&tid=156202&auth ... |
23-9-2020 at 04:08
by: B.D.E |
Preparation of n-butylamine(consult)
Hey there, I'm in need for some n-butylamine and I would highly appreciate your consult and advice r ... |
23-9-2020 at 00:33
by: B.D.E |
Lead 2 acetate basic
[rquote=644626&tid=156161&author=dextro88]
and find out the tryhidrate is just with 3 OH ca ... |
16-9-2020 at 05:23
by: B.D.E |
Lead 2 acetate basic
[rquote=644626&tid=156161&author=dextro88]
but that mean i will need atlest some water in t ... |
16-9-2020 at 05:17
by: B.D.E |
Steven's Rearrangement - Alternative strong bases to NaNH2
First let me just say that Thomas Thompson is a [b][i]bitching name[/i][/b].
Second, although I w ... |
27-8-2020 at 00:58
by: B.D.E |
Synthesis, storage of sodium ethoxide
[rquote=643507&tid=156007&author=unionised][rquote=643501&tid=156007&author=S.C. Wac ... |
25-8-2020 at 21:30
by: B.D.E |
Synthesis, storage of sodium ethoxide
Just saying that producing sodium is quite fun as well.
Also, lithium is quite cheap(per mole) on e ... |
21-8-2020 at 06:35
by: B.D.E |
Synthesis, storage of sodium ethoxide
Never tried the method you've decscribed, but I have made some sodium alkoxides in the past by addin ... |
12-8-2020 at 08:36
by: B.D.E |
HotPlate Branding
[rquote=640599&tid=155794&author=Deathunter88][rquote=640598&tid=155794&author=Brigh ... |
19-7-2020 at 21:53
by: B.D.E |
KCN synthesis. Care to share your thoughts?
[rquote=640571&tid=155774&author=SWIM]
@B.D.E. I just realized that your post was the first ... |
14-7-2020 at 12:35
by: B.D.E |
KCN synthesis. Care to share your thoughts?
Using a cold diluted NaOCl+NaOH solution for the bubbler is probably good enough choice. Keep in min ... |
12-7-2020 at 01:15
by: B.D.E |
successful method for purifying anthranilic acid(quick report)
[rquote=640141&tid=155744&author=mackolol]In case of anthranillic acid, I don't see any othe ... |
8-7-2020 at 12:54
by: B.D.E |
successful method for purifying anthranilic acid(quick report)
[rquote=640138&tid=155744&author=mackolol]...[/rquote]
Glad to hear you find it useful 
... |
8-7-2020 at 08:06
by: B.D.E |
successful method for purifying anthranilic acid(quick report)
[rquote=640125&tid=155744&author=Tsjerk]Why would higher boiling alkanes work faster? The ac ... |
8-7-2020 at 05:36
by: B.D.E |
does autoignition temperature even matter when refluxing a liquid?,
Ace 
Thanks for the useful answers! |
7-7-2020 at 11:47
by: B.D.E |
successful method for purifying anthranilic acid(quick report)
Hey, this is a quick report on a successful attempt of mine to purify anthranilic acid made from pht ... |
7-7-2020 at 10:49
by: B.D.E |
does autoignition temperature even matter when refluxing a liquid?,
I mean, the max temprature probably going to be very close to the b.p, isn't it?
I'm asking becau ... |
6-7-2020 at 03:36
by: B.D.E |
ortho nitration of p-toluenesulfonic acid(QUESTIONS)
[rquote=639152&tid=155581&author=Boffis]OK here's a translation of the most useful paper fro ... |
30-6-2020 at 01:03
by: B.D.E |
Forbidden Knowledge!
[rquote=639083&tid=155647&author=Refinery]...[/rquote]
True. Although most of the times' th ... |
24-6-2020 at 11:19
by: B.D.E |
Forbidden Knowledge!
[rquote=639034&tid=155647&author=dawt]...[/rquote]
+They always use those impractical 0.1mm ... |
23-6-2020 at 23:49
by: B.D.E |
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