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Problem: RDX synthesis created nonflammable white powder
So I performed the synthesis of RDX via the hexamine dinitrate in WFNA method, and in addition to a ... |
4-6-2017 at 11:21
by: Chisholm |
Salts of methazonic acid
[rquote=484565&tid=74449&author=PHILOU Zrealone]I'm not sure the operator did the all Anders ... |
2-6-2017 at 07:23
by: Chisholm |
How much have you spent on your lab?
[rquote=483836&tid=74199&author=j_sum1]Oh, come on. Who spent over a million?
If that was ... |
23-5-2017 at 05:42
by: Chisholm |
How much have you spent on your lab?
[quote]
[b]Poll Guidelines[/b]
For the purposes of this poll, "spent on your lab" refers specifica ... |
21-5-2017 at 08:48
by: Chisholm |
amateurs chemists and energetic material enthusiats are significantly reducing in asia
I find it weird that the birthplace of the firework has tried making individual possession of nitrat ... |
19-5-2017 at 15:05
by: Chisholm |
NPED detonator
What about a method to generate the primary explosive in-situ? Nichrome or other hot-wire resistor c ... |
19-5-2017 at 07:55
by: Chisholm |
My failure in making petn
We need much more information about what you did. An estimate of how much of each reactant, the addi ... |
19-5-2017 at 06:26
by: Chisholm |
Chloropicrin + Cu powder
Picryl chloride in ethanol, treated with a suspension of fine copper, reacts to form hexanitrobiphen ... |
17-5-2017 at 07:20
by: Chisholm |
recrystallization PETN
It's best to keep the temperature below 60ºC for any nitric ester (PETN, MHN, NC, NG, EGDN, ETN, et ... |
9-5-2017 at 14:18
by: Chisholm |
recrystallization PETN
What equipment do you have, and how much are you aiming to make? |
9-5-2017 at 10:01
by: Chisholm |
DBX-1
[rquote=482430&tid=73864&author=energeticone]...maybe I'm not digging enough, I have yet to ... |
6-5-2017 at 05:47
by: Chisholm |
Anhydrous HNO3 from DCM and dry ice
[rquote=482248&tid=73623&author=Dr.Bob]This just sounds like a dangerous prep that requires ... |
3-5-2017 at 18:37
by: Chisholm |
Anhydrous HNO3 from DCM and dry ice
Nobody?
[Edited on 5-3-2017 by Chisholm] |
3-5-2017 at 09:52
by: Chisholm |
TNT without SO3 or N2O5
I have an idea.
Acetone in concentrated sulfuric acid is dehydrated and polymerized into mesityle ... |
26-4-2017 at 05:49
by: Chisholm |
Anhydrous HNO3 from DCM and dry ice
I'm trying to generate about 40mL of anhydrous nitric acid.
Mixing 53 mL azeotropic HNO3 and 48 mL ... |
23-4-2017 at 04:15
by: Chisholm |
I have no idea what I just made
So my TNT odyssey continues. This time, though, I'm not quite sure what my product even is, though I ... |
19-4-2017 at 08:52
by: Chisholm |
Urea nitrate issues
Thank you for the information, but it wasn't what I was asking about. |
19-4-2017 at 03:25
by: Chisholm |
Urea nitrate issues
Urea nitrate is an attractive explosive from an economic perspective: urea is readily available, and ... |
18-4-2017 at 10:11
by: Chisholm |
NQ to diazoaminotetrazole in one pot?
I have a substantial quantity of nitroguanidine (~300g), as well as sodium nitrite, zinc dust, and g ... |
14-4-2017 at 08:10
by: Chisholm |
TNT without SO3 or N2O5
[rquote=480500&tid=73412&author=Praxichys]Why TNT, if not for curiosity?
I think the reas ... |
12-4-2017 at 07:42
by: Chisholm |
TNT without SO3 or N2O5
Every process I've seen for the synthesis of TNT requires fuming sulfuric acid and absolute nitric a ... |
11-4-2017 at 10:10
by: Chisholm |
Alternatives to dichromate for oxidation of TNT to TNB
I'm pretty sure that bleach oxidizes TNT to hexanitrostilbene. |
8-4-2017 at 11:59
by: Chisholm |
Alternatives to dichromate for oxidation of TNT to TNB
The procedure in CoPaE for oxidation of TNT to TNBzOOH with dichromate, followed by decarboxylation ... |
7-4-2017 at 08:01
by: Chisholm |
Trinitrobenzene without nitric acid or benzene
[rquote=480131&tid=73311&author=Boffis]@ Chrisholm, do you have a reference for the dehydrat ... |
7-4-2017 at 07:17
by: Chisholm |
Trinitrobenzene without nitric acid or benzene
The sugar-substitute inositol (cyclohexanehexol) can be dehydrated via concentrated sulfuric acid in ... |
5-4-2017 at 09:10
by: Chisholm |
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