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New Energetic Materials - Current Research
Ammonium carbonate is probably the most likely. It is a very substantial amount and may provide insi ... |
21-11-2025 at 03:14
by: Microtek |
Trinitrotoluene preparation
I have tried this a couple of times using detergent gasoline (mix of saturated aliphatic and cyclic ... |
14-11-2025 at 14:53
by: Microtek |
New Energetic Materials - Current Research
Recently I have been looking at furazan derivatives again. There are a number of procedures for diam ... |
13-11-2025 at 00:03
by: Microtek |
Easy SMX
It's not so much the decomposition temperature that is the problem but rather that in 18 days at 20 ... |
7-11-2025 at 11:39
by: Microtek |
Easy SMX
Yes, I used dimethoxypropane for the protection step. Very clean and easy reaction. I used way too m ... |
7-11-2025 at 00:54
by: Microtek |
Easy SMX
I did some work on SMX in my final thesis at the university (though I called it NDBD at the time). I ... |
6-11-2025 at 10:08
by: Microtek |
DIY BAM Friction test
These kinds of difficulties were some of the reasons that I decided to use a hybrid approach for my ... |
1-11-2025 at 00:45
by: Microtek |
3,3’-Diamino-5,5’-bis(1H-1,2,4-triazole) and Derivatives
I have prepared what I believe to be Bis(3-(nitroimino)-1H-1,2,4-triazol-5-yl)ethane. I didn't have ... |
2-10-2025 at 09:17
by: Microtek |
Exotic Primaries - Complex Salts
I tried the chlorate. I prepared it from copper acetate without any issues. It is fairly soluble in ... |
2-10-2025 at 09:00
by: Microtek |
Exotic Primaries - Complex Salts
Hmm. I will double check that I haven't confused the bromate with the nitrate by doing another prepa ... |
28-9-2025 at 01:18
by: Microtek |
Exotic Primaries - Complex Salts
I tested the initiating ability of both the bromate and nitrate with respect to RDX. Both substances ... |
27-9-2025 at 07:41
by: Microtek |
Exotic Primaries - Complex Salts
I wanted to try out the copper 4-amino-1,2-4-triazole bromate complex, so I added 4-ATRI to a soluti ... |
24-9-2025 at 22:36
by: Microtek |
Trinitrotoluene preparation
[quote]
I recomend you to follow 3 step process rather than 1 or 2 step for better and pure yeild ... |
21-7-2025 at 00:24
by: Microtek |
Exotic Primaries - Complex Salts
I see you use a large excess of bromate. Did that improve yields relative to what I got? I used the ... |
7-7-2025 at 23:29
by: Microtek |
Exotic Primaries - Complex Salts
I used the inadverdent NaOCl product. It gave quite a large amount of amorphous powder that seemed q ... |
7-7-2025 at 03:00
by: Microtek |
Exotic Primaries - Complex Salts
How did you ignite it? When flame ignited from above on a piece of Al-foil it pops, but does not pen ... |
6-7-2025 at 23:25
by: Microtek |
Shit RDX yields without acetic anhydride
Magnesium nitrate works a lot like sulfuric acid, and is indeed reuseable (as is sulfuric acid). You ... |
4-7-2025 at 00:18
by: Microtek |
Hexanitrogen
Well, unlike the highly nitrated cubanes, this doesn't seem too difficult to make (though I don't th ... |
3-7-2025 at 14:06
by: Microtek |
Shit RDX yields without acetic anhydride
When drying AN, you wan't to avoid making it liquify. The water has a much harder time escaping from ... |
2-7-2025 at 23:30
by: Microtek |
Exotic Primaries - Complex Salts
Yes, my crude does look something like that. I recommend a recrystallization from water. It makes be ... |
2-7-2025 at 12:09
by: Microtek |
Shit RDX yields without acetic anhydride
In my experience, water content in the AN can dramatically lower your yield, and will practically gu ... |
1-7-2025 at 00:51
by: Microtek |
Exotic Primaries - Complex Salts
Hmm, I don't cool it much before filtering, just to about room temp. I do cool the hydroxide soln si ... |
1-7-2025 at 00:42
by: Microtek |
Exotic Primaries - Complex Salts
Interesting. I might try that at some point, though I will be away from the lab for some time.
Ab ... |
30-6-2025 at 08:41
by: Microtek |
Exotic Primaries - Complex Salts
Well, I have tried a number of the methods.
I adapted the method in this open source paper: https: ... |
30-6-2025 at 00:11
by: Microtek |
Exotic Primaries - Complex Salts
I have done some sensitivity tests on BLG-1, and unfortunately it seems a lot more sensitive than NA ... |
28-6-2025 at 13:54
by: Microtek |
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