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Preparation of Methylammonium nitrate
Trimethylamine perchlorate is a material of interest because of its sensitivity at a drop test of 25 cm ...
3-11-2012 at 09:15
by: Rosco Bodine
Preparation of Methylammonium nitrate
... search hits would be interesting
http://www.sciencemadness.org/talk/search.php?token=&srchtxt=methylamine&srchfield=body&srchuname=Rosco+Bodine&f%5B%5D=a ll&srchfrom=0&searchs ...
27-9-2012 at 22:13
by: Rosco Bodine
HMTD Decomposition Rate and Recrystallization
Trimethylamine is a principal decomposition product of HMTD and it is basic, corrosive, hygroscopic and ...
28-2-2012 at 02:40
by: Rosco Bodine
Ethyl Perchlorate
... ave low melting points. Some candidate materials for such mixtures would be guanidine perchlorate, methylamine perchlorate, trimethylamine perchlorate, tetramethylammonium perchlorate, betaine perchl ...
29-11-2011 at 14:32
by: Rosco Bodine
Some tips about 5-ATZ nitrate
... and guanidine perchlorate is not correct. The perchlorates are more
powerful for guanidine and for methylamine and for other amines.
The only real concern there is unknown sensitivity to moisture.
...
28-6-2011 at 20:01
by: Rosco Bodine
Some tips about 5-ATZ nitrate
... which would have perfect chemical compatibility.

Of course more mundane guanidine perchlorate or methylamine perchlorate, would be better economy for use as a secondary explosive or base charge whi ...
28-6-2011 at 17:00
by: Rosco Bodine
Ethylene diamine perchlorate
... g that comes to mind as a possible candidate mixture. Betaine Perchlorate, Choline Perchlorate, Trimethylamine Perchlorate, and Tetramethylammonium Perchlorate
in OB mix with DAHTP or some complex m ...
10-2-2011 at 03:07
by: Rosco Bodine
Diammonium Hydrazinium Tetraperchlorate
... lving substituted ammonias and/or substituted hydrazines are also possible. For example perhaps a methylamine perchlorate with semicarbazide perchlorate would form an analogous double salt.

Good ...
8-2-2011 at 09:31
by: Rosco Bodine
Ethylene diamine perchlorate
... ael reaction. Paraformaldehyde is what I have on hand and
will doubtlessly convert some of it to methylamine perchlorate as I have no doubt that simpler well known reaction will work. I was simpl ...
18-10-2010 at 15:51
by: Rosco Bodine
Ethylene diamine perchlorate
... thod for "red goo".

My idea was that the proposed compound is possibly a variant "derivative" of methylamine perchlorate via an
intermediate methyleneimine derived from the initial reaction of the ...
18-10-2010 at 09:33
by: Rosco Bodine
5-ATZ(5-Aminotetrazole), the nitrotetrazolate ion and friends
... e, Biguanide Diperchlorate, as well as many other perchlorates of a non-guanidine relation, such as methylamine Perchlorate, Betaine Perchlorate, Nitrocholine Perchlorate, and possibly others. By vir ...
7-10-2010 at 13:32
by: Rosco Bodine
Synthetic route to tetrazoles from urea & ammonium nitrate
... n as well as by the readily forming aluminum isopropoxide. This reagent will reduce nitromethane to methylamine and
it would be expected to similarly reduce the nitro group of nitroguanidine.
20-10-2009 at 07:42
by: Rosco Bodine
The short questions thread (1)
... e amine. This is not something I have ever seen described
but there is an analogous reaction for methylamine.

These reactions could be hazardous, but manageable.

You would have to distill o ...
17-12-2008 at 01:05
by: Rosco Bodine
Perchlorate compositions
... One scheme which should be considered is the "formite"
aqueous reaction mixture which produces the methylamine nitrates from reaction of formaldehyde or paraformaldehyde with ammonium nitrate in the ...
20-1-2007 at 11:11
by: Rosco Bodine
Can anyone figure out what this may be??
... of 7 : 3 =
2.33 : 1

Anyway it is possible that you have a mixture of the
adduct along with the methylamine perchlorate and
the di and trimethylamine perchlorates and formic acid ,
ammonium form ...
4-10-2006 at 00:04
by: Rosco Bodine
Can anyone figure out what this may be??
The methylamine perchlorates are white in color so
whatever are the darker products are probably decrea ...
3-10-2006 at 22:08
by: Rosco Bodine
Can anyone figure out what this may be??
The reaction can probably be done in aqueous solution
as a parallel to the patented method for methylamine nitrate , and then the product secured by evaporating the water away .

I think usin ...
3-10-2006 at 20:44
by: Rosco Bodine
Can anyone figure out what this may be??
... e possible reaction of trioxane with ammonium perchlorate and the possibility of detonation of the
methylamine perchlorate and dimethylamine and trimethylamine perchlorates which could also form , if ...
3-10-2006 at 19:47
by: Rosco Bodine
Perchlorate compositions
...
IIRC , one of the schemes utilized addition of lime and sulfur to the melt , and other things like methylamine nitrates from the " formit " reaction of formaldehyde and ammonium nitrate . Other possi ...
31-8-2006 at 08:05
by: Rosco Bodine
Perchlorate compositions
... seems like the HDN should decompose in that mix
when melted , but could additionally form a bit of methylamine nitrate in the melt .
There is also potential for a urea-formaldehyde
polymer / sens ...
16-8-2006 at 00:23
by: Rosco Bodine
Perchlorate compositions
...

It would be my guess that trioxane would possibly work even better than formalin or para in the methylamine salt formation reaction with ammonium salts , but I think some water will be required an ...
29-7-2006 at 10:33
by: Rosco Bodine
Perchlorate compositions
... r similarly as the
reaction of ammonium nitrate in this regard , the product being principally the methylamine salt , along with lesser amounts of the di and tri methylamine salts as minor further re ...
28-7-2006 at 20:14
by: Rosco Bodine
C.T.M.T.N.A (R-salt)
A simultaneous reaction is not practical because the
methylamine formation is favored by high temperatures ,
while the TMTN formation requires low tempe ...
10-7-2006 at 21:32
by: Rosco Bodine
C.T.M.T.N.A (R-salt)
... he formaldehyde is also reactive .
In acidic systems there is a different reaction which
leads to methylamine derivatives and di and tri-methylamine derivatives instead of the hexamethylene
cyclisa ...
9-7-2006 at 15:01
by: Rosco Bodine
Sodium Metasilicate
... he page

Curiously , whenever using the tire cleaner , I have often
noticed a distinct smell of methylamine emanating from the
surface of the tire being contacted by the cleaner .
So it would se ...
19-6-2006 at 23:11
by: Rosco Bodine
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