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2023 Science Madness Secret Santa – The fun begins!
[rquote=690093&tid=159902&author=B(a)P]I have recently returned from a trip away to find tha ...
14-1-2024 at 03:34
by: Bedlasky
Simple guide for analytical chemistry
I haven't experiment with much of these rarer elements. I have done quite extensive research on moly ...
13-1-2024 at 21:54
by: Bedlasky
Simple guide for analytical chemistry
I've decided to make this guide for those of you who are new in analytical chemistry to make your be ...
13-1-2024 at 20:09
by: Bedlasky
Easy way to make phosphorus pentachloride with easy to get reagents
[rquote=690002&tid=160088&author=Texium]Zinc is a transition metal in name only, though. Che ...
8-1-2024 at 14:11
by: Bedlasky
Direct bromatometric titrations
Bromatometry can be very useful for quick determination of certain reducing compounds. Direct titrat ...
7-1-2024 at 19:06
by: Bedlasky
Easy way to make phosphorus pentachloride with easy to get reagents
[rquote=689975&tid=160088&author=leucine75]Almost all metal phosphides hydrolysis to phosph ...
7-1-2024 at 17:41
by: Bedlasky
Titanium dioxide
TiO2 should dissolve in molten NaHSO4. At least according to literature.
6-1-2024 at 10:59
by: Bedlasky
Recrystallisation question - help me design an experiment for junior students
Mn2+, Fe2+ and Cu2+ have similar ionic radii, so they can replace each other in a crystalline struct ...
6-1-2024 at 10:57
by: Bedlasky
Recrystallisation question - help me design an experiment for junior students
I am little bit worried about double dissplacement with NaNO3/KNO3/CuSO4 mix.

Solubility of CuSO4 ...
5-1-2024 at 00:55
by: Bedlasky
Recrystallisation question - help me design an experiment for junior students
What about chrome alum and potassium nitrate? There isn't any dissplacement reaction, potassium nitr ...
4-1-2024 at 06:28
by: Bedlasky
pseudoisomethylionone by Aldol condensation of citral with methylethylketone
[rquote=689039&tid=160010&author=Fery]No way how to assess the purity.
[/rquote]

If you ...
2-1-2024 at 07:45
by: Bedlasky
pseudoionone by Aldol condensation of citral with acetone
Again, nice work Fery!
2-1-2024 at 07:30
by: Bedlasky
alpha and beta ionone by cyclization of pseudoionone
Great work Fery, as always! It's always pleasure to read your detailed procedures.
2-1-2024 at 07:29
by: Bedlasky
Fake Terbium?
You can try dissolve Tb(OH)3 in sulfuric acid and make some terbium sulfate. Lanthanide sulfates hav ...
13-12-2023 at 17:22
by: Bedlasky
Fake Terbium?
[rquote=689336&tid=160034&author=ItalianChemist]
With NaOH only the hydrated hydroxide seem ...
11-12-2023 at 05:27
by: Bedlasky
Fake Terbium?
Iron contamination is usually big problem in fluorescent materials. Tb(III) is very slightly pink, s ...
11-12-2023 at 04:11
by: Bedlasky
New Europium complex?
I don't think that this complex is boring. I find it very interesting. Good work ItalianChemist!
26-11-2023 at 07:48
by: Bedlasky
Reaction of Persulfates with Magnesium and other metals
If you want some interesting experiments with persulfate, I recommend oxidation of Mn2+/Cr3+ in to M ...
22-11-2023 at 03:34
by: Bedlasky
Notice: Subforum reorganization
I am glad for making analytic chemistry subforum. I've been thinking about making some posts about t ...
19-11-2023 at 20:39
by: Bedlasky
Understanding (1+1) Reagent
[rquote=688579&tid=159965&author=woelen]This "(a+b)" convention indeed is horrible.
What do ...
18-11-2023 at 14:43
by: Bedlasky
Devardas alloy making.
Mix everything together and heat it. Melting point of Devarda's alloy is 490-560 °C, so your mix wi ...
15-11-2023 at 08:01
by: Bedlasky
Understanding (1+1) Reagent
Concentration of acid is usually most commonly available. So 36% HCl, 65% HNO3, 96% H2SO4 etc.
14-11-2023 at 12:31
by: Bedlasky
Recovery of silver, mercury and chromium from acid mixture
[rquote=688539&tid=159961&author=Eithern]Hi guys, thanks for your replies!

[rquote=688493 ...
13-11-2023 at 13:59
by: Bedlasky
The Short Questions Thread (4)
I don't think that this will work. Hydroxylamine is strong reducing agent and refluxing it with HNO3 ...
12-11-2023 at 09:46
by: Bedlasky
Dissolution of d-block metals in HCl vs HF
[rquote=688520&tid=159575&author=bolbol]Worth noting that the V pellets I used had a very th ...
11-11-2023 at 23:01
by: Bedlasky
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