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Does anyone have experience using TBAB as a PTC? Does it cause emulsions?
I was planning to run the reaction from the start with only separable solvents, such as Xylene/Water ... |
28-12-2016 at 08:21
by: FireLion3 |
Does anyone have experience using TBAB as a PTC? Does it cause emulsions?
I've been thinking of playing around with some phase transfer catalyst reactions and got my hands on ... |
27-12-2016 at 22:18
by: FireLion3 |
Can I separate amines of different polarity/bulkiness via partial A/B extraction?
I'm not talking about separating them based on differences in acidity, but rather sterics or hydroph ... |
6-9-2016 at 08:59
by: FireLion3 |
Can I separate amines of different polarity/bulkiness via partial A/B extraction?
Couldn't find any information on this but it seems like it would work in theory.
If there is a 5 ... |
6-9-2016 at 07:49
by: FireLion3 |
Caustic Vapor from adding Sodium Hydroxide to water?
But this all still begs the question, how is an aerosol getting created? I've had these caustic vapo ... |
13-4-2016 at 21:57
by: FireLion3 |
Caustic Vapor from adding Sodium Hydroxide to water?
I didn't realize something such as Sodium Hydroxide could be so easily volatile into the air, especi ... |
11-4-2016 at 12:05
by: FireLion3 |
Caustic Vapor from adding Sodium Hydroxide to water?
This has stumped me for years now and I've never really been bothered enough to look into it until n ... |
11-4-2016 at 11:39
by: FireLion3 |
What's the best way to recover Pd from Pd-Organic complexes?
I'll try heating it, though I don't think I have an inert atmosphere at my disposal, but metal salts ... |
1-3-2016 at 18:04
by: FireLion3 |
What's the best way to recover Pd from Pd-Organic complexes?
I have a bunch of Pd that is bound to some organic (phosphine) complexes (in the form of PdCl2), and ... |
1-3-2016 at 17:36
by: FireLion3 |
Does DMSO dissolve..... glass, to any extent?
Hm. I did remove one of the stoppers briefly and it still appears to be unfrosted, but then again I ... |
4-2-2016 at 20:23
by: FireLion3 |
Does DMSO dissolve..... glass, to any extent?
I feel like this is a dumb question but I have to ask.
For the first time ever I was using DMSO ... |
4-2-2016 at 20:08
by: FireLion3 |
Boiling to dryness - risk of explosion?
I should be okay then. There are no organics in the mixture, and yes the metal is Pd (as indicated b ... |
14-12-2015 at 20:35
by: FireLion3 |
Boiling to dryness - risk of explosion?
Boiling some leftover aqua regia + water mixture off to recover a metal salt, and I need to boil it ... |
14-12-2015 at 19:27
by: FireLion3 |
Need some advice/help on recovering Palladium from Aqua Regia...
@gdflp
Back suction of the neutralizing solution would introduce the carbonate resulting in sodi ... |
22-10-2015 at 16:14
by: FireLion3 |
Need some advice/help on recovering Palladium from Aqua Regia...
I did some googling and found one source say that it's not exclusive HCl that will cause palladium t ... |
21-10-2015 at 19:25
by: FireLion3 |
Need some advice/help on recovering Palladium from Aqua Regia...
I wasn't sure how to interpret the soluble in trace amounts note. So you think if I neutralize all t ... |
21-10-2015 at 16:06
by: FireLion3 |
Need some advice/help on recovering Palladium from Aqua Regia...
What I thought would be a two day process of dissolving the Pd and boiling excess off, has become a ... |
21-10-2015 at 15:31
by: FireLion3 |
What kind of non-acidic solvent can I use for PdCl2?
Does chloroform dissolve Palladium Chloride? I actually have some on hand. I googled that and couldn ... |
8-10-2015 at 16:31
by: FireLion3 |
What kind of non-acidic solvent can I use for PdCl2?
I'm trying to form a PdCl2 complex and need to avoid the use of acidic solvents. I've read PdCl2 is ... |
8-10-2015 at 15:43
by: FireLion3 |
Do aryl amines react with alkyl halides?
Aryl Amines have never been much interest to me, and I wasn't able to find information about this on ... |
7-9-2015 at 01:37
by: FireLion3 |
Handling Benzoyl Chloride?
That's good. I have a pretty good filter system. My experience with Benzyl Chloride also had it heat ... |
13-8-2015 at 00:15
by: FireLion3 |
Handling Benzoyl Chloride?
I was planning to get some of this for a Benzoylation reaction, since the Anhydride seems to be supe ... |
11-8-2015 at 22:13
by: FireLion3 |
Is Raney Nickel inherently flamable, or only after pressure reactions?
[rquote=376562&tid=35812&author=CuReUS][rquote=376307&tid=35812&author=FireLion3]Guy ... |
10-12-2014 at 09:08
by: FireLion3 |
Is Raney Nickel inherently flamable, or only after pressure reactions?
I'm not worried about storing it post reaction. I am more concerned with storing the unused Raney Ni ... |
9-12-2014 at 14:10
by: FireLion3 |
What is the mechanism for catalytic cleavage of ethers by Lewis Acid's?
[b]forgottenpassword[/b],
If you had been paying attention to the thread you would see that such ... |
9-12-2014 at 10:53
by: FireLion3 |
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