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anyone have a hotplate/stirrer for sale?
Looking for a hotplate/stirrer. Been working with a kitchen hot plate and a magnetic stirrer I made ...
4-5-2013 at 20:35
by: Furboffle
possible to perform Grignard with no solvent?
I've performed plenty of grignard reactions at the university under supervision in the past, I can s ...
2-5-2013 at 18:29
by: Furboffle
possible to perform Grignard with no solvent?
sorry if the thread didn't have a very clear cut purpose. is it reasonable to perform grignard witho ...
27-4-2013 at 12:09
by: Furboffle
possible to perform Grignard with no solvent?
I'll be synthesizing some bromo-ethane as soon as my order of sodium bromide arrives in a couple day ...
26-4-2013 at 21:49
by: Furboffle
problem with inorganic IR spec
In intermediate inorganic lab class we did an experiment where we dissolved triphenylphosphine in ac ...
3-4-2013 at 17:48
by: Furboffle
Glassware - whats this again?
organikum - first one appears to be a percolator. one thing I haven't used in a lab to know its purp ...
16-3-2013 at 11:49
by: Furboffle
What chemicals do you need?
I'm in need of lithium aluminum hydride and tetrahydrofuran. The chemical supplier I use for LiAlH[s ...
12-3-2013 at 14:40
by: Furboffle
waterbath vs. steambath
awesome this cleared up some uncertainty. Once my reagents arrive Tuesday I can get this underway. I ...
20-1-2013 at 12:50
by: Furboffle
waterbath vs. steambath
I'm performing an experiment soon that requests a steam bath. I don't have a proper steam bath appar ...
20-1-2013 at 12:02
by: Furboffle
is lah soluble in dcm?
I'm reducing an amide. I have no intention of using DCM as I have THF readily available. This is mor ...
10-11-2012 at 15:04
by: Furboffle
is lah soluble in dcm?
Can lah reduction be carried out in DCM?
I've seen one vague comment on another forum saying its p ...
9-11-2012 at 10:51
by: Furboffle
Primary amine oxidation
I'm trying to figure a good way to get from a primary amine to a carboxylic acid.
I used the search ...
1-11-2012 at 19:40
by: Furboffle
problem with vacuum distillation set up
[rquote=264083&tid=22038&author=Magpie][rquote=264074&tid=22038&author=Furboffle]
a ...
31-10-2012 at 14:11
by: Furboffle
problem with vacuum distillation set up
[rquote=264062&tid=22038&author=watson.fawkes]So you answered the second question but not th ...
31-10-2012 at 06:43
by: Furboffle
problem with vacuum distillation set up
[rquote=264042&tid=22038&author=watson.fawkes]How did you prepare the pump for operation? By ...
30-10-2012 at 22:01
by: Furboffle
problem with vacuum distillation set up
I just bought this vacuum pump at harbor freight today:

http://www.harborfreight.com/25-cfm-vacuu ...
30-10-2012 at 19:14
by: Furboffle
Fischer speier esterification
[rquote=262767&tid=21844&author=kristofvagyok]P.S.: I know that the IAA esters are really ni ...
19-10-2012 at 10:46
by: Furboffle
Fischer speier esterification
I've attempted the Fischer-speier reaction involving indole-acetic acid and methanole to convert IAA ...
18-10-2012 at 19:36
by: Furboffle
Indole 3 acetic acid -> methyl indole acetate
I'm trying to convert indole acetic acid to its methyl ester, I tried the fischer-speier esterificat ...
15-10-2012 at 16:51
by: Furboffle
Vacuum aspirator
I recently purchased a vacuum aspirator on amazon. Not the most professional device, but I'm looking ...
15-10-2012 at 15:21
by: Furboffle

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