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New tramadol to M1 ref discovered, EASY
[rquote=213024&tid=14655&author=Globey]Well if this were so easy, by extension, couldn't you ...
16-6-2011 at 14:11
by: Picric-A
Moisture and oxygen sensitive compounds.
Preperation of Chromium (II) acetate would be a good start. Your product should be a bright red. If ...
13-6-2011 at 08:32
by: Picric-A
The short questions thread (3)
After atempting to reduce 1,3-dinitrobenzene with NaBH4 in methanoic solution I instantly obtained ...
30-5-2011 at 07:57
by: Picric-A
Phenylthiocarbamide
Thanks for all the great replys guys, it has been realy helpful. Im going to see if we have any ammo ...
17-5-2011 at 14:36
by: Picric-A
Phenylthiocarbamide
[rquote=210022&tid=16334&author=ScienceSquirrel]Have a look at this paper, if you can get yo ...
17-5-2011 at 10:38
by: Picric-A
Phenylthiocarbamide
Thanks for the reply. That makes sense. I will probably order the Phenyl Isothiocyanate in because i ...
17-5-2011 at 05:15
by: Picric-A
Phenylthiocarbamide
'70% of humans can taste this non-toxic compound and it tastes incredible bitter, 30% can not taste ...
17-5-2011 at 04:11
by: Picric-A
it differences between diglyme and THF in LAH reaction
Diglyme is sometimes more favorable if a higher boiling point is required in reactions requiring mor ...
26-4-2011 at 02:40
by: Picric-A
Drying out aqueous ammonium nitrate
Unfortunatly its an un-branded/loca shop here so there wont be another one like it but my point was ...
23-4-2011 at 11:14
by: Picric-A
Drying out aqueous ammonium nitrate
Just for your personal reference, i completly disagree that NH4NO3 is hard to get in the UK!!

I b ...
23-4-2011 at 10:03
by: Picric-A
Rare chemicals
[rquote=206171&tid=15968&author=phlogiston]This is exactly why you needed to elaborate on wh ...
7-4-2011 at 11:35
by: Picric-A
5-Ethoxyvanillin via Ullmann - Failure...
What would the yields be like if i did the following;

-Dissolve 5 moles of NaOH in excess methano ...
2-4-2011 at 13:29
by: Picric-A
N2O synthesis
Hi Jor, what is the reference for that reaction? Looks very intersting, definitly something i should ...
30-3-2011 at 09:45
by: Picric-A
N2O synthesis
I have done this reaction several tims to generate chemically pure N2O for the barking dog rxn.

T ...
29-3-2011 at 10:23
by: Picric-A
"Pellets" in NM
Most certainly from your description they are molecular sieves, used to keep the NM dry.
26-3-2011 at 12:47
by: Picric-A
looking for a route to aluminium tribromide
[rquote=204795&tid=15829&author=DJF90]If you bothered to read what Woelen wrote you will see ...
21-3-2011 at 09:45
by: Picric-A
looking for a route to aluminium tribromide
[rquote=204784&tid=15829&author=Jor]Woelen, you can use conc. H2SO4 ;). I prepared conc. col ...
21-3-2011 at 05:46
by: Picric-A
Synthesis of Resorcinol
When using Fentons Reagent to oxidise benzene to phenol how does one actually go about this?
Benzen ...
12-3-2011 at 00:10
by: Picric-A
Vacuum
[rquote=203539&tid=15156&author=Lord Emrone]... but I'm not really into chemistry ... [/rquo ...
10-3-2011 at 12:28
by: Picric-A
Make Potassium (from versuchschemie.de)
My reflux system is he same as everyone else is using, a 100ml rbf. with q.fit liebig condenser and ...
22-2-2011 at 10:50
by: Picric-A
Make Potassium (from versuchschemie.de)
Im not sure the t-BuOH is being kept in the system, i will test the decanted paraffin later and see ...
22-2-2011 at 02:55
by: Picric-A
garbage can chloroform
This seems like suicide to me, i can almost guarantee a runaway reaction (notorious with haloform re ...
21-2-2011 at 14:12
by: Picric-A
Make Potassium (from versuchschemie.de)
One thing i forgot to mention- before use i dryed the paraffin overnight with sodium metal.

My ma ...
21-2-2011 at 14:07
by: Picric-A
Make Potassium (from versuchschemie.de)
Ok, I tryed this reaction using 2-methylpropan-2-ol and paraffin as the solvent. The only form of ma ...
21-2-2011 at 02:58
by: Picric-A
Make Potassium (from versuchschemie.de)
[rquote=202079&tid=14970&author=DJF90]I've seen it sold for 15£/500ml commercially, and £1 ...
19-2-2011 at 06:46
by: Picric-A
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