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Preparation of elemental phosphorus @Magpie-- Nice work as usual! Was your ceramic retort made of alumina? You may have success trying t ...	6-3-2010 at 09:15 by: Strepta
Preparation of elemental phosphorus @blogfast: I've used the CO2 before even with elemental Al in the tube. While some may have been ...	5-3-2010 at 10:51 by: Strepta
Preparation of elemental phosphorus I took some photos of the quartz tube from my AlPO4 experiment near the point where the tube broke. ...	4-3-2010 at 17:22 by: Strepta
Preparation of elemental phosphorus Sorry about that last post (removed). I'll edit the photos down in size and re-post later.	3-3-2010 at 17:31 by: Strepta
Preparation of elemental phosphorus I should clarify my objectives a bit. In the above experiment with AlPO4 I wanted to verify that P w ...	1-3-2010 at 17:57 by: Strepta
Attempted Reduction of AlPO4 with Carbon [b]Introduction[/b] Intrigued by an article posted by SC Wack (Preparation of Elemental Phosphoru ...	28-2-2010 at 13:55 by: Strepta
Preparation of elemental phosphorus pip: Of course it can be scaled up, albeit with somewhat different apparatus. I would suggest procee ...	7-1-2010 at 04:48 by: Strepta
Electrolysis of LiCl in DMSO @ sakshaug007: I was very interested in your results with LiCl in acetone which you mentioned in th ...	11-4-2009 at 04:43 by: Strepta
Preparation of elemental phosphorus Tip of the hat to not_important; I tried boron trioxide (from boric acid by heating) in place of sil ...	2-7-2008 at 11:29 by: Strepta
Preparation of elemental phosphorus [quote][i]Originally posted by len1[/i] Its worse than I thought, Al powder is not just watched its ...	17-6-2008 at 09:17 by: Strepta
Preparation of elemental phosphorus Yes, garage chemist, other aluminums will work at higher onset temperatures. I did a number of exper ...	15-6-2008 at 15:22 by: Strepta
Preparation of elemental phosphorus Method for Preparation of Small Amounts of P4. The attached is a description of a technique I ha ...	15-6-2008 at 11:34 by: Strepta
Preparation of elemental phosphorus What was your expected yield? Do you think too much P went off as PH3? What do you think needs to ...	7-3-2007 at 06:46 by: Strepta
Preparation of elemental phosphorus Note: See attachment for pictures. I attempted the reduction of Pb3(PO4)2 according to the metho ...	3-3-2007 at 17:46 by: Strepta
Lithium from Pyridine [i]posted by BromicAcid[/i] [Lithium cannot be obtained by the electrolysis of aq. soln. of its s ...	15-5-2004 at 17:05 by: Strepta
High boiling organics with densities greater than 1 You need an inert liquid with a density of 1 g/cm3 or above with a boiling point of greater then 100 ...	15-5-2004 at 16:24 by: Strepta
Bromic's technique with patu's wire loop I replaced the nickel sheet metal cathode with a loop of iron wire (.35 cm dia.). This allowed me to ...	9-5-2004 at 04:30 by: Strepta
BromicAcid's use of resistance heating I've been following this topic for awhile and have tried several experiments. Just this evening ...	6-5-2004 at 17:28 by: Strepta
unconventional sodium [quote][i]Originally posted by chemoleo[/i] Bromic, your method doesn't seem all that differen ...	6-5-2004 at 16:59 by: Strepta

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