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DMF substitute in Wacker oxidation?
What kind of wacker are you planning?

using benzoquinone as the O2 source will run fine using met ...
10-3-2011 at 13:59
by: antibody
Eschweiler-Clarke Procedure
et voila!

http://www.erowid.org/archive/rhodium/pdf/eschweiler-clarke.solventfree.pdf
10-3-2011 at 13:53
by: antibody
size of formaldehyde molecule and 3A molecular sieves
Thank you Chordate.

I'll use just enough sieves to absorb the amount of H2O I anticipate being p ...
1-3-2011 at 16:21
by: antibody
size of formaldehyde molecule and 3A molecular sieves
I'm thinking of using 3A molecular sieves to help drive the imine formation using formaldehyde and a ...
1-3-2011 at 11:43
by: antibody
read up on fractional distillation
http://en.wikipedia.org/wiki/Fractional_distillation

or if the BPs of your solvents have more tha ...
26-2-2011 at 10:11
by: antibody
New wisdom on the subject
According to this JOC article Na is actually a poor and obsolete way of drying THF. They have severa ...
22-2-2011 at 14:09
by: antibody
L-tryptophan decarboxylation
Yes, Thanks for that Turd. I downloaded it earlier today but haven't had the time yet to delve into ...
8-2-2011 at 14:02
by: antibody
L-tryptophan decarboxylation
[rquote=201090&tid=8574&author=madscientist]The use of a ketone catalyst will result in the ...
8-2-2011 at 13:05
by: antibody
L-tryptophan decarboxylation
You are right 2-Cyclohexen-1-one is a challenge to source. It isn't available locally and shipping i ...
8-2-2011 at 09:34
by: antibody

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