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1-(3-bromo,4-methoxyphenyl)-2-nitroethene reduction
Thanks samsung, I think I will try the CTH reduction. |
28-7-2005 at 21:16
by: enima |
1-(3-bromo,4-methoxyphenyl)-2-nitroethene reduction
Nicoderm, I have reduced 4-methoxyphenylnitroethene using NaBH4 and CTH, the reduction works well. T ... |
27-7-2005 at 13:04
by: enima |
1-(3-bromo,4-methoxyphenyl)-2-nitroethene reduction
I'm trying to reduce
1-(3-bromo,4-methoxypheny)-2-nitroethene to the appropriate phenethylami ... |
27-7-2005 at 00:39
by: enima |
New chemistry forum for Hive Bees
teenagers?
On the topic of the 'hives return' the dns server does have the a name chan ... |
27-7-2005 at 00:13
by: enima |
New chemistry forum for Hive Bees
Tor network?
Not sure if anyone has used or heard of the tor network of the EFF. It provides for ... |
26-7-2005 at 12:08
by: enima |
3,4,5-trimethoxy-beta-nitrostyrene synthesis
Quick question: @ what temp does the aldehyde, either 3,4,5-trimethoxybenzaldehyde or the 5-hydroxyv ... |
24-7-2005 at 22:41
by: enima |
toluene --> benzaldehyde
well the much _easier_ route would be an elb oxidation of toluene using a persulfate salt and a meta ... |
24-7-2005 at 18:20
by: enima |
3,4,5-trimethoxy-beta-nitrostyrene synthesis
joe, the ethylenediamine can be found at photo suppliers. It is pretty cheap. The freebase is in liq ... |
20-7-2005 at 09:11
by: enima |
OTC diethylamine, the easy way
DMT synthesis? maybe? not sure exactly. You can also make it by reacting ammonium chloride and paraf ... |
12-4-2005 at 08:09
by: enima |
Oxidation method
NaBH4 works really well at reducing the imine to the amine, I can post the proceedure for that as we ... |
9-4-2005 at 18:09
by: enima |
alternative method maybe?
How about oxidizing the secondary halide to the ketone via V2O5/H2O2. Reaction of the ketone with hy ... |
9-4-2005 at 10:20
by: enima |
Vapor phase oxidation of toluene...
Vanadium pentoxide is a great oxidation catalyst, you can oxidize alcohols to aldehydes or ketones u ... |
8-4-2005 at 13:10
by: enima |
Chemical 'hacking' of self-destructing DVDs
[quote][i]Originally posted by I am a fish[/i]
[quote][i]Originally posted by Organikum[/i]
Wouldn ... |
28-3-2005 at 10:44
by: enima |
Ozonolysis
yes, I would greatly appreciate it, I'm curious whether the chloroform could be substituted wit ... |
22-3-2005 at 23:23
by: enima |
Ozonolysis
Hi I'm looking for a proceedure, or references for a proceedure to an ozonolysis reaction, main ... |
22-3-2005 at 06:29
by: enima |
Rhodiums loss of GABA to GHB
The method works as advertised. The product is effectively formed. Usage of the Sodium Nitrite gave ... |
17-3-2005 at 03:09
by: enima |
N-bromo Succinimide
Nice find Mephiso. I wonder how well the DBDHM would work on activated aldehyde groups. Those are ve ... |
15-3-2005 at 00:11
by: enima |
Phenyl-2-nitropropene reduction
The zinc ic activated in the hcl solution, which is then filitered and washed with water to remove t ... |
13-3-2005 at 11:39
by: enima |
Phenyl-2-nitropropene reduction
I'm not sure exactly, hehe but methylamine is a foul smelling chemical.
You could use ammoni ... |
12-3-2005 at 19:00
by: enima |
Phenyl-2-nitropropene reduction
Synthetic Communications 34(4), 599-605(2004)
for the magnesium catalyzed reduction. I believe its ... |
12-3-2005 at 15:32
by: enima |
Phenyl-2-nitropropene reduction
Al/Hg is good for reducing oximes. 
Also Ammonium Formate and Zinc work ok.
I think you may ge ... |
12-3-2005 at 03:21
by: enima |
Oxydation of Ethylamine into Nitroethane?
Guess the water to nitroethane azeotrope isn't too bad. I wonder if youd be able to seperate i ... |
10-3-2005 at 19:10
by: enima |
Phenyl-2-nitropropene reduction
yea, I understand why you'd want to avoid mercury salts. I'm so paranoid that I go through ... |
10-3-2005 at 19:08
by: enima |
Chem price from Québec
[quote][i]Originally posted by rift valley[/i]
1 liter of bromine, how cool would it be to have tha ... |
10-3-2005 at 15:37
by: enima |
Phenyl-2-nitropropene reduction
Take a look at the Al/Hg reduction of nitrostyrenes on rhodiums website, p2np is reduced to amphetam ... |
10-3-2005 at 15:34
by: enima |
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