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Proposed novel 6-step syntheis of 5-MeO-4-AcO-DMT Oh I have that thread bookmarked, still have to try that synthesis out. I didn't read through the wh ... |
11-6-2021 at 21:28 by: mr_bovinejony |
Proposed novel 6-step syntheis of 5-MeO-4-AcO-DMT Do you have the link for that thread? |
11-6-2021 at 09:41 by: mr_bovinejony |
16 oz of nitroethane. Buy or nah? Ohh I recognize that brand. I'm curious to know how much of a yield you get if you distill it |
7-6-2021 at 09:05 by: mr_bovinejony |
Indole-3-Carbinol Oxidation Sure haven't! I'm going to run a tlc on these indoles I have now for practice |
5-6-2021 at 07:47 by: mr_bovinejony |
Indole-3-Carbinol Oxidation I had some succes recrystallizing indole 3 aldehyde with dmf and water, maybe it'll work for indole ... |
5-6-2021 at 06:43 by: mr_bovinejony |
Indole-3-Carbinol Oxidation Yeah I still have them, but the color is stupid and two recrystalizations later helped none. It's a ... |
5-6-2021 at 06:23 by: mr_bovinejony |
Indole-3-Carbinol Oxidation I have already tried this with PCC twice with no success, but I haven't seen any other trials so don ... |
5-6-2021 at 03:58 by: mr_bovinejony |
Vilsmeier reagent/POCl3 formation Not sure why I can't edit the posts, but I have the images saved for if they do disappear. I don't t ... |
28-5-2021 at 17:41 by: mr_bovinejony |
LabDIRECT is now an Official US TCI Distributer! Is there any kind of markup for these products? I imagine a very good percentage of my chemicals wil ... |
27-5-2021 at 14:56 by: mr_bovinejony |
Vilsmeier reagent/POCl3 formation The end of the vilsmeier saga: part one
5 grams of pcl5 is added to 5 ml of dmf. This heats up a ... |
26-5-2021 at 16:12 by: mr_bovinejony |
Elemental Scientific Liquidating Chemicals, glassware, and used equipment Is this something you have to pick up in person? Or can they be shipped? |
25-5-2021 at 19:28 by: mr_bovinejony |
A foray into phenethylamines of the Shulgin kind Very!! Bromo saccharin is incredibly easy to make. And it's much less irritating than nbs, although ... |
24-5-2021 at 20:23 by: mr_bovinejony |
A foray into phenethylamines of the Shulgin kind Yes it did work, in fact it was as easy as replacing nbs with it in this bromination of 2ch. But fo ... |
24-5-2021 at 17:28 by: mr_bovinejony |
A foray into phenethylamines of the Shulgin kind Dissolve 2ch in a minimum amount of gaa and add an equal weight of nbs! The product will precipitate ... |
24-5-2021 at 15:11 by: mr_bovinejony |
Vilsmeier reagent/POCl3 formation Of course not, I'm looking for some indole identification right now
The stuff decomposed once it ... |
24-5-2021 at 08:38 by: mr_bovinejony |
Vilsmeier reagent/POCl3 formation One last update until I get some real results, this first picture here is what I'm thinking is the f ... |
24-5-2021 at 07:52 by: mr_bovinejony |
Vilsmeier reagent/POCl3 formation Some interesting thing happens now, 5 grams of pcl5 are added to 5 ml of ice cold dmf. After this is ... |
24-5-2021 at 00:22 by: mr_bovinejony |
A foray into phenethylamines of the Shulgin kind You added all the nabh4 at once to a solution of the nitrostyrene and refluxed? Or they were partial ... |
21-5-2021 at 17:27 by: mr_bovinejony |
Vilsmeier reagent/POCl3 formation All experiments with the formation of the vh reagent in dmf and pcl5 have failed, I guess there is s ... |
21-5-2021 at 10:20 by: mr_bovinejony |
Vilsmeier reagent/POCl3 formation I'm not sure where you buy your reagents but the place I get mine from pocl3 is readily available, a ... |
19-5-2021 at 03:10 by: mr_bovinejony |
Vilsmeier reagent/POCl3 formation I have the opposite problem, I have pcl5 easily but not p2o5. I have seen that procedure though, and ... |
17-5-2021 at 10:44 by: mr_bovinejony |
Vilsmeier reagent/POCl3 formation I have plans to try out the Vilsmeier Haack reaction, but only have PCl5 for it. I found a paper her ... |
15-5-2021 at 21:31 by: mr_bovinejony |
Thermometers,Clamps and stuff Is this real life? It's nice to see this account posting again |
13-5-2021 at 21:15 by: mr_bovinejony |
Dichromate overoxidation Oooo don't give me any more ideas! There's already too much on the list |
24-4-2021 at 16:10 by: mr_bovinejony |
Dichromate overoxidation @carl I do have that paper downloaded like 3 times on my phone, ill have to dig for it. The only rea ... |
24-4-2021 at 10:58 by: mr_bovinejony |
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