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Experimental: Alternative to Al/Hg - the Al/Cu
The reaction definitely does work, with beta nitrostyrene at least but I can't get consistent result ... |
17-8-2014 at 22:43
by: pepsimax |
Sand Blast Cabinet -> Glove Box Conversion
Great idea!
Yes I think the light is definitely something to worry about, I'm sure ether would h ... |
8-8-2014 at 22:04
by: pepsimax |
Sand Blast Cabinet -> Glove Box Conversion
Great idea!
Yes I think the light is definitely something to worry about, I'm sure ether would h ... |
8-8-2014 at 22:00
by: pepsimax |
Containing Cl gas for long term storage
Hi, basic question here but I've never really worked much with gasses.
I'm wanting to trap a sma ... |
30-7-2014 at 01:56
by: pepsimax |
25g 4-Fluorobenzoyl chloride
Does anyone have any use for this reagent? I bought it for a project but found an alternative so nev ... |
26-7-2014 at 04:25
by: pepsimax |
Experimental: Alternative to Al/Hg - the Al/Cu
Been thinking, would this system run much smoother on nitrostyrene if the carbon carbon double bond ... |
25-7-2014 at 23:33
by: pepsimax |
Experimental: Alternative to Al/Hg - the Al/Ga
Wanting to try a different substrate, bit bored of phenethylamine after 20 odd experiments with your ... |
22-7-2014 at 11:43
by: pepsimax |
Some questions about the Al/Hg reduction system.
You need around the same quantity of Al as substrate, ie 10g foil per 10g nitrostyrene. Maybe a slig ... |
21-7-2014 at 21:21
by: pepsimax |
Experimental: Alternative to Al/Hg - the Al/Ga
Ah interesting, thanks! The Ga was sold as 99.999% though I usually take that with a pinch of salt. ... |
21-7-2014 at 17:28
by: pepsimax |
Experimental: Alternative to Al/Hg - the Al/Ga
I can't seem to get the gallium to react properly. An alloy made with a few bits of aluminum and gal ... |
20-7-2014 at 01:36
by: pepsimax |
Experimental: Alternative to Al/Hg - the Al/Ga
Damn you copper man, I've only just got my shed clean from the copper experimentation.
I'd rec ... |
29-6-2014 at 15:43
by: pepsimax |
Experimental: Alternative to Al/Hg - the Al/Cu
Another run....
5g substrate, 75ml reagent EtOH, 4.5g Al (half strips like first post, half of th ... |
29-6-2014 at 11:11
by: pepsimax |
Experimental: Alternative to Al/Hg - the Al/Cu
[rquote=336300&tid=30297&author=ChemicalCowboy84]Also which CuCl2 should be used the anhydro ... |
29-6-2014 at 09:42
by: pepsimax |
Experimental: Alternative to Al/Hg - the Al/Cu
[rquote=336294&tid=30297&author=Burner]If you use the gallium you do not need the CuCl2.
[/ ... |
29-6-2014 at 09:41
by: pepsimax |
Experimental: Alternative to Al/Hg - the Al/Cu
I didn't check the pH, too late now though as it has all been binned. I"ve found some aluminum swarf ... |
29-6-2014 at 00:39
by: pepsimax |
Experimental: Alternative to Al/Hg - the Al/Cu
This was the gloopy stuff separated from the water distillate then put in fresh water to see if it s ... |
23-6-2014 at 08:25
by: pepsimax |
Experimental: Alternative to Al/Hg - the Al/Cu
Is benzyl chloride soluble in xylene? According to wiki it shouldn't be, where as this stuff is. I p ... |
23-6-2014 at 05:11
by: pepsimax |
Experimental: Alternative to Al/Hg - the Al/Cu
Hey that makes absolute perfect sense, I think you're dead on there. The nitrostyrene was recrystali ... |
22-6-2014 at 13:36
by: pepsimax |
Experimental: Alternative to Al/Hg - the Al/Cu
Ah, no salt. Thanks, perhaps that contributed to my 'chloroform'. I was looking at a prep for chloro ... |
21-6-2014 at 08:20
by: pepsimax |
Experimental: Alternative to Al/Hg - the Al/Cu
Do you recommend still using the same amount of nacl with the copper? Ie 1g cu 20g na, or adjust acc ... |
21-6-2014 at 05:16
by: pepsimax |
Experimental: Alternative to Al/Hg - the Al/Cu
beta nitrostyrene to PEA. Here's the ingredient lest on the alcohol.
3. COMPOSITION/INFORMATIO ... |
21-6-2014 at 03:13
by: pepsimax |
Experimental: Alternative to Al/Hg - the Al/Cu
Ah my mistake, should have read that better. Finished the steam distil. I took the first 70mls off, ... |
21-6-2014 at 01:35
by: pepsimax |
Experimental: Alternative to Al/Hg - the Al/Cu
Well, first things first I am an amateur. I'm posting excatly what I did in the hope others will not ... |
20-6-2014 at 11:36
by: pepsimax |
Experimental: Alternative to Al/Hg - the Al/Cu
All the Al has gone. It should be noted this particularly violent reaction could have been because o ... |
20-6-2014 at 07:02
by: pepsimax |
Experimental: Alternative to Al/Hg - the Al/Cu
Yeah, not in a hurry to try IPA again so waiting on more EtOH, reagent grade. Should be here soon, m ... |
19-6-2014 at 11:06
by: pepsimax |
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