| Search |
| [Next Page] |
A foray into phenethylamines of the Shulgin kind
You added all the nabh4 at once to a solution of the nitrostyrene and refluxed? Or they were partial ... |
21-5-2021 at 17:27
by: mr_bovinejony |
Vilsmeier reagent/POCl3 formation
All experiments with the formation of the vh reagent in dmf and pcl5 have failed, I guess there is s ... |
21-5-2021 at 10:20
by: mr_bovinejony |
Vilsmeier reagent/POCl3 formation
I'm not sure where you buy your reagents but the place I get mine from pocl3 is readily available, a ... |
19-5-2021 at 03:10
by: mr_bovinejony |
Vilsmeier reagent/POCl3 formation
I have the opposite problem, I have pcl5 easily but not p2o5. I have seen that procedure though, and ... |
17-5-2021 at 10:44
by: mr_bovinejony |
Vilsmeier reagent/POCl3 formation
I have plans to try out the Vilsmeier Haack reaction, but only have PCl5 for it. I found a paper her ... |
15-5-2021 at 21:31
by: mr_bovinejony |
Thermometers,Clamps and stuff
Is this real life? It's nice to see this account posting again |
13-5-2021 at 21:15
by: mr_bovinejony |
Dichromate overoxidation
Oooo don't give me any more ideas! There's already too much on the list  |
24-4-2021 at 16:10
by: mr_bovinejony |
Dichromate overoxidation
@carl I do have that paper downloaded like 3 times on my phone, ill have to dig for it. The only rea ... |
24-4-2021 at 10:58
by: mr_bovinejony |
Dichromate overoxidation
Are there any more mild oxidizing agents other than IBX/DMP/TEMPO that might work for it then? Maybe ... |
24-4-2021 at 07:23
by: mr_bovinejony |
Dichromate overoxidation
I was thinking of using IBX but I have very little and it took a while to make. Might not have a cho ... |
23-4-2021 at 08:34
by: mr_bovinejony |
Dichromate overoxidation
Nile red has a video on making propionaldehyde but uses some heated condenser water which adds more ... |
23-4-2021 at 08:17
by: mr_bovinejony |
Improved Purification Procedure Decarboxylation of L-tryptophan to Tryptamine with Benzoate salt
Did some more testing, It looks like anhydrous ipa can be used as an alternative to acetone. But due ... |
20-4-2021 at 18:45
by: mr_bovinejony |
Large scale anthranilic acid prep
My inability to do reactions under a 3 gram scale has been my downfall. But when it works its the gr ... |
19-4-2021 at 15:32
by: mr_bovinejony |
Improved Purification Procedure Decarboxylation of L-tryptophan to Tryptamine with Benzoate salt
I am very happy to report a kind of pure tryptamine product from the benzoate salt. My thiele tube t ... |
19-4-2021 at 10:54
by: mr_bovinejony |
Large scale anthranilic acid prep
@oxide I just don't like the reaction, titration of store bought bleach is a pain and temperature co ... |
18-4-2021 at 17:45
by: mr_bovinejony |
Improved Purification Procedure Decarboxylation of L-tryptophan to Tryptamine with Benzoate salt
Here is the post washed and filtered paste
https://imgur.com/iP4piBT
And here is some of the p ... |
18-4-2021 at 09:50
by: mr_bovinejony |
Large scale anthranilic acid prep
The hoffman reaction is bullshit for any chemical lol. I weighed all this yesterday and it was 210 g ... |
18-4-2021 at 08:31
by: mr_bovinejony |
Large scale anthranilic acid prep
I definitely think so, even with the brown discoloration it had a very sharp melting point. |
18-4-2021 at 07:23
by: mr_bovinejony |
Large scale anthranilic acid prep
From what I've seen, the hoffman route usually gives a brown product. When I was filtering this prod ... |
18-4-2021 at 04:35
by: mr_bovinejony |
Improved Purification Procedure Decarboxylation of L-tryptophan to Tryptamine with Benzoate salt
I did this procedure. Heres how it went
20 grams of tryptophan mixed with 150 mls of turpentine a ... |
17-4-2021 at 18:40
by: mr_bovinejony |
Large scale anthranilic acid prep
Eh that's what happens when its left out in the open for 3 weeks! |
17-4-2021 at 14:44
by: mr_bovinejony |
Large scale anthranilic acid prep
https://imgur.com/ujQ4mhy
https://imgur.com/tnqXB1u
https://imgur.com/p92ZDLC
Here are some ... |
17-4-2021 at 10:58
by: mr_bovinejony |
Activating metals post-addition
Hcl won't do anything to the reaction. I reduced benzlin with tin and hcl and it worked just fine |
16-4-2021 at 17:15
by: mr_bovinejony |
Vanillin chemistry: 3,4,5-trimethoxyphenethylamine
I tried starting from vanillin as well, I gave up after the 3rd attempt. Syringaldehyde is cheap and ... |
12-4-2021 at 22:27
by: mr_bovinejony |
Improved Purification Procedure Decarboxylation of L-tryptophan to Tryptamine with Benzoate salt
I'm curious if you plan on using this benzoate salt in some other reactions with tryptamine, or if y ... |
8-4-2021 at 02:50
by: mr_bovinejony |
| [Next Page] |
