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Sodium Thiosulfate Synthesis and Purification
My overall interest in this method began from watching a YouTube video on synthesizing STS from boil ...
17-8-2018 at 08:42
by: Doped-Al2O3-fusion
Sodium Thiosulfate Synthesis and Purification
To be honest, I've not had a chance to proofread anything I've written tonight. My family has been ...
15-8-2018 at 19:29
by: Doped-Al2O3-fusion
Hydrothermal Synthesis of Sulfides
The lighter brown colored stuff in the black product is mainly iron (III) oxide. I used a nail insi ...
15-8-2018 at 19:18
by: Doped-Al2O3-fusion
Hydrothermal Synthesis of Sulfides
It has a metallic luster under the microscope, but that's just the visual appearance most likely due ...
15-8-2018 at 19:11
by: Doped-Al2O3-fusion
Sodium Thiosulfate Synthesis and Purification
The slower the crystals are grown, the larger and more pure they'll be. They are easily washed off ...
15-8-2018 at 18:44
by: Doped-Al2O3-fusion
Sodium Thiosulfate Synthesis and Purification
I plan on replying to this thread with much greater detail in the future. I'll leave the humor out ...
15-8-2018 at 18:37
by: Doped-Al2O3-fusion
Sodium Thiosulfate Synthesis and Purification
I have been searching the forum for this topic specifically and I came across some threads discussin ...
15-8-2018 at 18:30
by: Doped-Al2O3-fusion
Laws regulating chemicals for a tiny home lab
I'm in the same situation. I live in a rented town home/apartment and my lab is in my home office. ...
31-7-2018 at 08:04
by: Doped-Al2O3-fusion
Hydrothermal Synthesis of Sulfides
[rquote=526529&tid=85360&author=Ubya]waiting for results:cool:[/rquote]

Leak test was suc ...
30-7-2018 at 17:37
by: Doped-Al2O3-fusion
Hydrothermal Synthesis of Sulfides
I performed the first test on the autoclave today. I added 20mL of distilled water into the 50mL ve ...
28-7-2018 at 23:03
by: Doped-Al2O3-fusion
Good source of arsenic?
I recently boiled down a quart of waste HCl containing god knows what from dissolving local rocks/mi ...
26-7-2018 at 06:51
by: Doped-Al2O3-fusion
Hydrothermal Synthesis of Sulfides
I'll most likely be using FeSO4 (heptahydrate) & Na2S2O3 (pentahydrate) in my reaction vessel. ...
24-7-2018 at 16:18
by: Doped-Al2O3-fusion
Hydrothermal Synthesis of Sulfides
[rquote=525585&tid=85360&author=MJ101]@Doped-Al2O3-fusion: I've just read about the Verneuil ...
24-7-2018 at 11:33
by: Doped-Al2O3-fusion
Hydrothermal Synthesis of Sulfides
I used 3.5g of iron powder and 2g of sulfur to make this batch of iron sulfide. Product yield was 5 ...
24-7-2018 at 11:25
by: Doped-Al2O3-fusion
Hydrothermal Synthesis of Sulfides
Here is the actual vessel I purchased:

https://www.ebay.com/itm/50ml-PPL-lined-Hydrothermal-synth ...
24-7-2018 at 11:05
by: Doped-Al2O3-fusion
Hydrothermal Synthesis of Sulfides
Here is a paper I found on the hydrothermal synthesis of transition metal sulfides. I thought up the ...
24-7-2018 at 10:59
by: Doped-Al2O3-fusion
Hydrothermal Synthesis of Sulfides
[rquote=525206&tid=85360&author=elementcollector1]What's the max pressure for your hydrother ...
24-7-2018 at 10:51
by: Doped-Al2O3-fusion
Hydrothermal Synthesis of Sulfides
[rquote=525091&tid=85360&author=Ubya]nice project, i'm also intrested in hydrothermal crysta ...
22-7-2018 at 10:17
by: Doped-Al2O3-fusion
Hydrothermal Synthesis of Sulfides
I'm in a side quest to create synthetic pyrite because I want to. Practicality is of no concern as ...
21-7-2018 at 17:40
by: Doped-Al2O3-fusion
Whats the most dangerous chemical you've ever synthesized?
TATP (Acetone Peroxide)

I accidentally created this compound recently while attempting to further ...
21-7-2018 at 16:21
by: Doped-Al2O3-fusion
Ag & Cu crystals
I've got some copper sulfide I recently created. There are some microscopic faceted crystals of eit ...
21-7-2018 at 16:08
by: Doped-Al2O3-fusion
Isolating cobalt, copper and lithium from an old LiPo RC Helicopter battery.
Here are some pictures of what I've got so far.

There is a shot of the last bit of cobalt sludge ...
21-7-2018 at 15:33
by: Doped-Al2O3-fusion
Isolating cobalt, copper and lithium from an old LiPo RC Helicopter battery.
I realized I never posted photos of the initial solution. Here are a couple with one showing the fi ...
19-7-2018 at 21:29
by: Doped-Al2O3-fusion
Isolating cobalt, copper and lithium from an old LiPo RC Helicopter battery.
I'm thinking about trying selective precipitation by adjusting the pH of the solution. It's pretty ...
19-7-2018 at 21:09
by: Doped-Al2O3-fusion
Isolating cobalt, copper and lithium from an old LiPo RC Helicopter battery.
[rquote=524621&tid=85051&author=MrHomeScientist]I don't really have any comments, but just w ...
19-7-2018 at 15:13
by: Doped-Al2O3-fusion
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