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Ephedrine from Propiophenone...
It's not even from a patent, it was a literature entry.
[quote][i]Originally posted by stoichiome ... |
5-2-2008 at 06:30
by: Drunkguy |
Hydride question
How strong of a reducer is NaH?
For example, NaH is used in the Dieckman cyclization.
^Clearly ... |
3-2-2008 at 05:23
by: Drunkguy |
Ephedrine from Propiophenone...
I have the Henry reaction here. Under vigorous conditions the nitrostyrene is formed because of a de ... |
2-2-2008 at 13:07
by: Drunkguy |
Ephedrine from Propiophenone...
Norpseudoephedrine = Phenylpropanolamine
Phenylpropanolamine is more conveniently prepared by Hen ... |
24-1-2008 at 06:40
by: Drunkguy |
One last one. May be hopeless, though...
^I thought the vial is brown glass accounting for the color.
Bromine would not need to be stored ... |
21-1-2008 at 03:36
by: Drunkguy |
One last one. May be hopeless, though...
Anything extremely moisture or air sensitive may be stored in vials especially done so for: (a) smal ... |
21-1-2008 at 03:13
by: Drunkguy |
Reduction of Nitro Toluene
My experience has been that the reduction of NO2 with Sn/HCl and also of "Schiff bases" with Zn/HOAc ... |
17-1-2008 at 11:22
by: Drunkguy |
H2 adsorption ability of Ru, Pt, Ni metal powder
The thing about heating it in the furnace is prior to purchasing the "alloy" to make the active form ... |
14-1-2008 at 21:07
by: Drunkguy |
H2 adsorption ability of Ru, Pt, Ni metal powder
[color=Purple]The introduction by Raney (1927) of a new form of catalyst (the Raney nickel catalyst) ... |
11-1-2008 at 04:36
by: Drunkguy |
H2 adsorption ability of Ru, Pt, Ni metal powder
[color=Purple]Im not at all familiar with this reaction. They say those Parr Hydrogenators are avail ... |
10-1-2008 at 17:34
by: Drunkguy |
Possible synthesis to 1,5,7-trihydroxydecahydronaphthalene-2-carboxylic acid?
3,5-dimethoxybromobenzene as base chemical to make the corresponding alpha-tetralone.
Then, to get ... |
31-12-2007 at 06:47
by: Drunkguy |
NEED SOME IODINE?
Yeah, I find it interesting that Science Lab (previously Science Alliance) has managed to survive af ... |
30-12-2007 at 10:54
by: Drunkguy |
Reduction of Aromatic Nitro compounds with Zn / HCl A write up
Zinc is a more mild reducing agent than iron, which in turn is milder than tin.
If you had used t ... |
28-12-2007 at 06:21
by: Drunkguy |
Catalytic Hydrogenation ......comments
Keep up the good work guys 
At least with balloon hydrogenations a T-bore adapter is used. The ... |
27-12-2007 at 20:46
by: Drunkguy |
Homebuilt 1300°C tube furnace
Ich habe jetzt deine furnace gesehen.
Jawohl! Bravo! Prima!
Now I know who i'll will be employ ... |
25-12-2007 at 18:07
by: Drunkguy |
"Sealed Tube"
I'm not that experienced with chemistry that I would be able to follow the discussion in the above l ... |
23-12-2007 at 00:43
by: Drunkguy |
Catalytic Hydrogenation ......comments
That looks like a really sweet set-up. I would be ill able to afford something as neat as that in th ... |
22-12-2007 at 12:15
by: Drunkguy |
Catalytic Hydrogenation ......comments
This was during the preparation of 7-azabicyclo[2.2.1]heptanes related to epibatidine total synthesi ... |
22-12-2007 at 09:18
by: Drunkguy |
Catalytic Hydrogenation ......comments
I also want to envelope hydrogenation into the synthetic repertoire of my organic chemistry. I've do ... |
22-12-2007 at 01:07
by: Drunkguy |
*&$#ing hazmat fees.. a rant.
Everyone knows hazmat fees are far in excess of what is reasonable. |
21-12-2007 at 03:46
by: Drunkguy |
"Sealed Tube"
Thanks guys. This chemical is commerically available at not particularly inflated cost but the synth ... |
20-12-2007 at 11:21
by: Drunkguy |
bromination of phenyl group
Assuming one actually wanted 1,4-dibromobenzene though.
Does anybody have a procedure for this? |
20-12-2007 at 09:46
by: Drunkguy |
"Sealed Tube"
On some reactions I have been reading it claims the reactants are mixed in a "sealed tube" and then ... |
20-12-2007 at 08:52
by: Drunkguy |
Reduction of nitrostyrene using Vitride (Red-Al)
I saw the Lemmigner reduction in the production of a compound called "AL." At first I was very optim ... |
19-12-2007 at 13:34
by: Drunkguy |
bromination of phenyl group
The bromination of benzene is typically done with Br2 and pyridine ala Vogel textbook of organic che ... |
19-12-2007 at 09:36
by: Drunkguy |
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