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butanoic acid from sandmeyer rxn
Try to remove all the GHB/GBL with more water and distillation. Distilling seems the easiest.

Wh ...
21-8-2013 at 11:48
by: I Like Dots
Connecting distillation apparatus to tap faucet?
Ok, This is what i do.
Now in most sinks, on the head of the faucet there is a thing that scews int ...
20-8-2013 at 18:01
by: I Like Dots
Liquid Nitrogen Dioxide
ME TOO BromicAcid. It was before I had a proper hotplate. It was not hot enough to boil the acid, on ...
20-8-2013 at 17:50
by: I Like Dots
Experimental Preparation of Chlorobutanol
Now im thinking about other this reaction with other halogens.. I saw bromic acid possibly produced ...
20-8-2013 at 13:45
by: I Like Dots
Experimental Preparation of Chlorobutanol
Hey guys,

I had a go at this synthesis, and like most was left with slightly yellow, watery crys ...
5-7-2013 at 17:25
by: I Like Dots
Copper acetate and residue
You don't need to be exact with this.
Just make a solution of copper sulfate, and add sodium bicar ...
17-6-2013 at 16:42
by: I Like Dots
3D print lab supplies?
I have access to a nice 3D printer, Im wondering if anyone has 3D models of keck clips.

I checke ...
11-6-2013 at 19:49
by: I Like Dots
Please Assist the Noob... Attempting to extract compounds from Plants.
I have always struggled with plant extractions. They require patience, good technique, and above all ...
11-6-2013 at 13:20
by: I Like Dots
synthetic liquor, no hangover
If you were hardcore you could drink ethyl ether. I have heard it described as "400 proof".
8-6-2013 at 16:45
by: I Like Dots
Trying to find a home for a glass jar of ~13 kg of mercury
acetone
>ace-tone
>ass-tone
>tone-ass
7-6-2013 at 09:47
by: I Like Dots
Stories of extremely chemophobic parents and yours :p
Don't lose interest cou. Im in college right now, and in a club that has access to a well stocked l ...
7-6-2013 at 09:38
by: I Like Dots
Homemade stands
Did someone say 'Custom' stand?? Got impatient and McGyvered myself a stand.
Its... uhh... whats t ...
23-5-2013 at 11:30
by: I Like Dots
Thinking about buying some glassware.. advice for a beginner?
Funkerman I have to say I like the first kit you posted. I can see how the glass petcock could be a ...
7-5-2013 at 14:01
by: I Like Dots
Thinking about buying some glassware.. advice for a beginner?
I was looking for some glassware, I feel like I am limiting myself without proper equipment. You kno ...
7-5-2013 at 11:16
by: I Like Dots
Weird things happening to H2O2 catalysts
While I was making copper acetate, I saw the same thing.
I used regular vinegar with 30% H2O2.
...
29-4-2013 at 14:30
by: I Like Dots
nitroglycerin
Thank you for your thoughtful reply!

It was kept between 6-10 C in a ice/salt/water bath chilled ...
12-4-2013 at 08:50
by: I Like Dots
nitroglycerin
Hey guys, first post. Yesterday I tried my hand at this.
6ml Sulfuric Acid
4gm ammonium nitrate
...
10-4-2013 at 16:40
by: I Like Dots

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