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First attempt at the rearrangement of 2-phenylpropanal
"Maybe I am missing something here but isn't it at least kind of cool that the rearrangement seemed ...
31-3-2012 at 13:42
by: jon
Forest of amines! (saccharin to cyclic and asymmetric amines)
have you thought of throwing a base in the mix to deprotonate that nitrogen? maybe kalium carbonate ...
31-3-2012 at 10:47
by: jon
First attempt at the rearrangement of 2-phenylpropanal
cause for celebration

[file]18213[/file]
31-3-2012 at 09:29
by: jon
Reddit AMA with a former Hive member
for real he was (self) nominated for a nobel prize wow! the chutzpah!

[Edited on 5-3-2012 by jon]
5-3-2012 at 13:39
by: jon
Education on Illicit substances
none of these arguements really matter when you consider the real motivations behind drug prohibitio ...
27-2-2012 at 19:53
by: jon
Preparation of Palladium Acetate from Palladium Chloride
no i don't think so you would need to make palladium black with formalin and naoh.
then treat it wi ...
18-2-2012 at 21:22
by: jon
3,4-MD-Phenmetrazine
in the aminorex class methoxylation only led to dampened stimulant (more like antidepressant propert ...
12-1-2012 at 23:57
by: jon
Opioid Aminobenzycyclanols derived from Menthone
oh i'm sure there are plenty of ways to do that.
you know it occured to me you could forego the oxi ...
8-1-2012 at 22:32
by: jon
Opioid Aminobenzycyclanols derived from Menthone
next time try MnO2.
or you could make the ethylene ketal of piperidone and n-alkylate that.

yeah ...
8-1-2012 at 20:44
by: jon
Opioid Aminobenzycyclanols derived from Menthone
i wonder if that aldol condensation could be acid catalyzed it seems like that would also work.
7-1-2012 at 14:54
by: jon
Old man driven out of business by the DEA
why buy the iodine if he was smart he would have employed subterfuge and made his own iodine.
14-12-2011 at 23:09
by: jon
how does the ring form??
i think the carbonate pulls protons off the tetrahedral intermediate.
at least that's my theory bec ...
9-12-2011 at 20:38
by: jon
dechlorinating 1,4-Dichlorobenzene
ammonium formate/palladium on carbon, and methanol is a good way to dechlorinate aryl chlorides.
ye ...
22-11-2011 at 11:55
by: jon
3,4-dimethylaminorex
yeah i can say you don't want to mess with these class of drugs i did and the end result was violent ...
19-11-2011 at 19:23
by: jon
NMR - Restricted Rotation
looks like resonance to me
31-10-2011 at 17:18
by: jon
1-methyl-lysergic acid preparation
1 in the numbering system of ergolines implies the carbon adjacent to the indole ring for example
3-9-2011 at 12:05
by: jon
1-methyl-lysergic acid preparation
you should have transesterified the amide with methanolic hydrogen chloride
3-9-2011 at 12:03
by: jon
Potassium Cyanate - Purification
all i did was filter and crash with ethanol there is nothing to this.
25-8-2011 at 17:55
by: jon
how difficult would it be to get a reagent for gold production
i think it's the stigma it carries you know sort of like how strychnine sounds bad.
5-8-2011 at 17:36
by: jon
how difficult would it be to get a reagent for gold production
looks like they handing out 2 years in the federal pound me in the ass penitentiary for declaring it ...
4-8-2011 at 21:48
by: jon
Australian man charged for posessing "Explosive Materials"
they would'nt buy the lunatic defence, they rarely do.
god may forgive, the man won't.
it does'nt ...
4-8-2011 at 06:47
by: jon
how difficult would it be to get a reagent for gold production
yeah i was looking at a much larger scale and i thought it might raise some eyebrows.
i'm sure with ...
4-8-2011 at 06:32
by: jon
Oslo and the amateur experimenter
i get the impression too, that the manifesto may have been altered.
you can't believe everything th ...
4-8-2011 at 04:35
by: jon
Oslo and the amateur experimenter
boomerang or no the laws are still in force
4-8-2011 at 02:30
by: jon
Oslo and the amateur experimenter
well as the ruling elite would say "never let a crisis go to waste"
and he played right into thier ...
4-8-2011 at 02:11
by: jon
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