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Vanillin to Piperonal
I always thought the Mannich was a little dodgy with primary amines and ammonia, since the resulting ...
3-5-2017 at 14:02
by: Cryolite.
The Problem with SynthSource
It's a shame that these resins aren't Li-6 enriched... owning a solid sample of Li-6 carbonate would ...
3-5-2017 at 13:11
by: Cryolite.
preparation of maleic anhydride
Nicely done! Although, the use of acetyl chloride seems a bit excessive. Have you tried direct heati ...
29-4-2017 at 09:32
by: Cryolite.
The Problem with SynthSource
FLiBe?
27-4-2017 at 11:35
by: Cryolite.
ninhydrin synthesis
@atara: What about using nitrosophenol instead of NDMA? Its synthesis is similarly straightforward, ...
24-4-2017 at 18:34
by: Cryolite.
Ruthenium dust (and more!) for sale from US. International shipping is possible.
Well, the amount of ferrocyanide in salt is approximately 50ppm. The amount of HCN producde from usi ...
23-4-2017 at 19:09
by: Cryolite.
Packet Desicants
Regardless of the nice idea of using silica to keep reagents dry, I don't think it will work with pT ...
18-4-2017 at 18:14
by: Cryolite.
Getting rid of forum spam
I'm still not sure why we don't have a better registration process though. The email confirmation th ...
17-4-2017 at 18:53
by: Cryolite.
Ruthenium dust (and more!) for sale from US. International shipping is possible.
I would like to raise my contribution to 15 dollars (+5 shipping).
13-4-2017 at 15:46
by: Cryolite.
Ruthenium dust (and more!) for sale from US. International shipping is possible.
Honestly, I feel that just selling it off at a fixed price might be more convenient for all involved ...
12-4-2017 at 14:05
by: Cryolite.
Ruthenium dust (and more!) for sale from US. International shipping is possible.
Any update on this?
12-4-2017 at 05:18
by: Cryolite.
Chemicals that are expensive to buy but easy to make
[rquote=480466&tid=73192&author=JJay]
Dioxane actually looks tremendously useful... I'm not ...
11-4-2017 at 17:19
by: Cryolite.
hypophosphoric convertion
And it's extremely good at reducing benzylic alcohols to alkanes... (no, not that substrate) It woul ...
10-4-2017 at 22:23
by: Cryolite.
Ethyl acetoacetate with Mg(OEt)2 catalyst
Jeez, where the hell do you live and how can i move there? :o
9-4-2017 at 15:46
by: Cryolite.
Ethyl acetoacetate with Mg(OEt)2 catalyst
I never said that it would be cheap, but for a small scale experiment like this I don't see why lith ...
9-4-2017 at 12:53
by: Cryolite.
Ethyl acetoacetate with Mg(OEt)2 catalyst
An interesting OTC extraction you could try would be extracting lithium metal from lithium AA batter ...
8-4-2017 at 20:20
by: Cryolite.
Ethyl acetoacetate with Mg(OEt)2 catalyst
Maybe lithium would be worth a try if you have it?
8-4-2017 at 18:47
by: Cryolite.
Chemicals that are expensive to buy but easy to make
How about benzene? Nigh impossible to get outside of chemical suppliers, but easy enough to make fro ...
8-4-2017 at 11:52
by: Cryolite.
Ethyl acetoacetate with Mg(OEt)2 catalyst
An issue with magnesium alkoxides is low solubility. I worry that even with good mechanical agitatio ...
7-4-2017 at 21:21
by: Cryolite.
What states still sell Toluene?
Sadly, over here in California I have not been so fortunate :( I can't find toluene on the shelves h ...
5-4-2017 at 21:57
by: Cryolite.
Modafinil: its preparation via Bunte salt
If you read the paper, it clearly states that the concentration of benzyhydryl cations in solution w ...
5-4-2017 at 18:31
by: Cryolite.
Nitroethane via NaNO2/DMF
Such a shame that DMSO reacts with ethyl bromide... :(

Why is it that nitrite esters don't form i ...
28-3-2017 at 12:16
by: Cryolite.
Maximizing chloroform from the haloform reaction
Bleaching powder works, but I found that the massive quantities of insoluble calcium hydroxide produ ...
28-3-2017 at 12:11
by: Cryolite.
Nitroethane via NaNO2/DMF
The Victor-Meyer necessitates a tedious recycling of the waste silver halide back to silver nitrate. ...
28-3-2017 at 11:36
by: Cryolite.
Nitroethane via NaNO2/DMF
>works in polyethylene glycol

That's funny, considering the only place I've heard that is from ...
28-3-2017 at 10:34
by: Cryolite.
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