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Fume Cupboard
[rquote=191798&tid=14784&author=Mossydie]
Also could you possible explain what baffles are? ...
3-11-2010 at 10:46
by: Picric-A
Fume Cupboard
It looks like you wont get a lot of airflow through that small hose... certainly not enough that i w ...
2-11-2010 at 11:42
by: Picric-A
oxalic acid synthesis
[rquote=191770&tid=14126&author=Random]Can I use nitrate salt mixed with hcl instead of pure ...
2-11-2010 at 01:42
by: Picric-A
Create crazy Halloween pumpkins
Whats the decomposition product of Mercury thiocyanate?
1-11-2010 at 04:49
by: Picric-A
Soxhlet thimble help
[rquote=191187&tid=14727&author=Ozone]Coffee filters "sealed" with twine or wire.

O3[/rqu ...
26-10-2010 at 14:33
by: Picric-A
Soxhlet thimble help
Yes very fine glass wool works fine aswell! Nice trick of the trade ;)

[Edited on 25-10-2010 by Pic ...
25-10-2010 at 10:39
by: Picric-A
Distinguishing two compounds
[rquote=191127&tid=14724&author=psychokinetic][rquote=191123&tid=14724&author=anothe ...
25-10-2010 at 09:02
by: Picric-A
Distinguishing two compounds
Thanks for all the replies so far.

Results from the lab show this;
With sodium the dark red liq ...
24-10-2010 at 06:49
by: Picric-A
Distinguishing two compounds
I do not have a thermometer high enough to measure the b.p's of both these compounds so i was ideall ...
24-10-2010 at 05:03
by: Picric-A
Soxhlet thimble help
Simply fill the bottom with cotton wool, followed by your material to be extracted then put another ...
23-10-2010 at 01:53
by: Picric-A
Distinguishing two compounds
[rquote=190932&tid=14724&author=Nicodem]bp[/rquote]
I thought of this however it uses relat ...
22-10-2010 at 08:42
by: Picric-A
Distinguishing two compounds
I have just received two bottles of chemicals, both plastic 100ml bottles.

One contains 2-chloroe ...
22-10-2010 at 08:29
by: Picric-A
Benzene from PET
That looks very similar to the product i got form decarboxylation of TPA so yes that seems very prom ...
21-10-2010 at 10:17
by: Picric-A
Benzene from PET
[rquote=190841&tid=14715&author=ScienceSquirrel]I doubt it will work.
Might be worth a try ...
21-10-2010 at 09:39
by: Picric-A
New tramadol to M1 ref discovered, EASY
[rquote=190165&tid=14655&author=madscientist]
In the case of tramadol, this metabolite is m ...
14-10-2010 at 11:24
by: Picric-A
The short questions thread (3)
[rquote=189616&tid=14239&author=dann2]Thanks for reply.
I am dissolving Bismuth to make BiC ...
8-10-2010 at 22:59
by: Picric-A
The short questions thread (3)
[rquote=189524&tid=14239&author=dann2]Hello,

Can anyone tell me how to make Aqua Regia.
...
8-10-2010 at 00:43
by: Picric-A
DIY magic filter papers - a video demonstration
I have used these many time before. They are called Hydrophobic Frits.
Another benefit of them is t ...
8-10-2010 at 00:39
by: Picric-A
Diphenhydramine hydrochloride
I didnt find a patent for this specific reaction however there were many patents with similar reacti ...
25-9-2010 at 04:41
by: Picric-A
Diphenhydramine hydrochloride
Yes, by reacting 2-chloroethanol with dimethylamine under reflux. Yields ok but cost of raw material ...
24-9-2010 at 13:57
by: Picric-A
Diphenhydramine hydrochloride
I would just like to update this thread.
After my LONG efforts at trying to synthesise dimethyletha ...
24-9-2010 at 10:27
by: Picric-A
The short questions thread (3)
Does anybody know of an OTC source of methyl acrylate?

I am attempting to perform a Michael addit ...
2-9-2010 at 09:13
by: Picric-A
Burning sulphur
This red liquid is molten sulphur. Sulphur dioxide is a colourless gas.
21-8-2010 at 11:18
by: Picric-A
The short questions thread (3)
[rquote=184517&tid=14239&author=turd][rquote=184487&tid=14239&author=Picric-A]
Wow ...
6-8-2010 at 04:12
by: Picric-A
The short questions thread (3)
[rquote=184493&tid=14239&author=panziandi]I made methyl formate from formic acid (98%) and m ...
5-8-2010 at 16:11
by: Picric-A
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