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Making sodium tellurite from tellurium dioxide?
I recently prepared selenium dioxide from crude selenium purchased off of Ebay. The selenium dioxide ... |
29-6-2010 at 20:48
by: benzylchloride1 |
A Twofer Prep - Two Acyl Chlorinating Reagents Made at One Step
Something that may be of interest that I found while browsing Weygand and Hilgetag's Preparative Org ... |
3-6-2010 at 12:09
by: benzylchloride1 |
Preparation of solid aluminium isopropoxide
This may be slightly off topic, can titanium tetraisopropoxide be synthesized in a similar manner? T ... |
14-5-2010 at 17:56
by: benzylchloride1 |
Drying Ether for Grignard
When I run syntheses involving Grignard Reagents, I distill my ether from engine starting fluid. Thi ... |
13-5-2010 at 09:45
by: benzylchloride1 |
Column chromatography materials
[rquote=176053&tid=13715&author=Pomzazed]I tend to use the cat-pee sand of the cheapest pric ... |
20-4-2010 at 09:16
by: benzylchloride1 |
Camphor: Any interesting experiment?
Terpene chemistry, one of my favorite fields. Camphorquinone which is really a diketone can be produ ... |
20-4-2010 at 09:11
by: benzylchloride1 |
Hi-Valley Chemicals
I actually would not be worried about buying chemicals from this type of supplier. First thing If yo ... |
15-2-2010 at 20:24
by: benzylchloride1 |
Hi-Valley Chemicals
My university orders solvents and other chemicals from Hi-valley chemicals. They are reputable suppl ... |
12-2-2010 at 07:30
by: benzylchloride1 |
Synthesis of malonic acid
I have a possible solution to the unavailability of diethyl malonate. If sodium metal can be obtaine ... |
26-1-2010 at 22:07
by: benzylchloride1 |
Total Synthesis of Carpanone from Catechol
I have been experimenting with the bromination of 1,2-methylenedioxybenzene in methanol using using ... |
24-1-2010 at 22:30
by: benzylchloride1 |
Preparation of solid aluminium isopropoxide
I recently conducted a large scale synthesis of aluminumn isopropoxide. A bottle of iso heet which i ... |
24-1-2010 at 22:16
by: benzylchloride1 |
Buchi Model Rs, Three Working on Jack Stands For Sale
What is the best way to change a vapor duct in a Buchi rotovap with out breaking it? I have a Buchi ... |
10-1-2010 at 21:52
by: benzylchloride1 |
Benzotrichloride, Benzoyl Chloride, and Phthalyl Chloride - Illustrated Practical Guide
Benzoyl chloride can be produced in high yield using aluminum chloride as a catalyst.
150g of the b ... |
10-1-2010 at 21:46
by: benzylchloride1 |
Preparation of Pyridine
About a month ago, I synthesized some pyridine by the same method after reading the results of Magpi ... |
15-12-2009 at 11:03
by: benzylchloride1 |
Benzotrichloride, Benzoyl Chloride, and Phthalyl Chloride - Illustrated Practical Guide
Len1, your are right about the academics not doing research, once they get tenure, they quit for goo ... |
15-12-2009 at 10:51
by: benzylchloride1 |
Benzotrichloride, Benzoyl Chloride, and Phthalyl Chloride - Illustrated Practical Guide
My research laboratory is located at 8000 feet, so the boiling points are considerably reduced. I li ... |
14-12-2009 at 08:38
by: benzylchloride1 |
Preparation of Malonic Acid
An extremely good method for producing malonic acid, thank you very much for posting this. I have re ... |
13-12-2009 at 21:44
by: benzylchloride1 |
Benzotrichloride, Benzoyl Chloride, and Phthalyl Chloride - Illustrated Practical Guide
I recently finished the synthesis of benzotrichloride from 100 mL of toluene. The chlorination to th ... |
13-12-2009 at 21:38
by: benzylchloride1 |
Total Synthesis of Carpanone from Catechol
Here is the reference for the hydrolysis of aryl diazonium salts to phenols using copper (II) nitrat ... |
13-12-2009 at 21:23
by: benzylchloride1 |
Total Synthesis of Carpanone from Catechol
A synthesis progress report:
The reduction of 4-nitro-1,2-methylenedioxybenzene in 2-propanol with ... |
10-12-2009 at 09:56
by: benzylchloride1 |
Preparation of Bromine
Magpie, I like your method for the production of bromine, I use a similar method all the time for th ... |
10-12-2009 at 09:45
by: benzylchloride1 |
Total Synthesis of Carpanone from Catechol
The nitrated product weighed 20 grams, for a percentage yield of 75%, based on 1,2-methylenedioxyben ... |
17-11-2009 at 07:46
by: benzylchloride1 |
Purple chlorophenol?
The red oil that distilled after the phenol was possibly phenyl salicyclate; the oil dissolved in to ... |
15-11-2009 at 23:12
by: benzylchloride1 |
Total Synthesis of Carpanone from Catechol
Nicodem, thanks for your help on this synthesis. I am considering using a catalyzed hydrazine redu ... |
15-11-2009 at 22:58
by: benzylchloride1 |
Purple chlorophenol?
I have experimented with the pyrolysis of sodium salicyclate about a year ago. The sodium salicyclat ... |
12-11-2009 at 21:53
by: benzylchloride1 |
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