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Heating something under reflux
19903
31-7-2013 at 06:21
by: dangerous amateur
What kind of vacuum pump is suitable for a 24/40 setup?
Uhm, if I may ask, forgive my ignorance:
What is meant by "24/40 setup"?
30-7-2013 at 11:13
by: dangerous amateur
Coffee filter vs. "folded" filter papers from lab supply
Im going to expand my means soon.

I allready have a small buchner + a set op papers, but i was s ...
13-7-2013 at 02:30
by: dangerous amateur
erythritol tetranitrate recrystallization

[quote]
Wait, there's difference in tap water and drinking water?[/quote]
Where I live there is ...
12-7-2013 at 13:38
by: dangerous amateur
erythritol tetranitrate recrystallization
Hi

considering the neutralisation issue, is it necessary to use NaHCO3 ect. ?

Ethanol is not ...
12-7-2013 at 11:38
by: dangerous amateur
Coffee filter vs. "folded" filter papers from lab supply
Hi guys,

how much better are in your opinion/experience the special lab filters?

Coffee filter ...
11-7-2013 at 12:22
by: dangerous amateur
Test reaction for hydrazine
Thank you for your answers.

Yes I know toxicity, i only mess around with very small amounts and o ...
8-7-2013 at 02:16
by: dangerous amateur
Test reaction for hydrazine
Unfortunately I don't have both TCCA and iodine here.

I was told the material [i]might [/i] also ...
7-7-2013 at 12:15
by: dangerous amateur
Test reaction for hydrazine
Hi,

do you guys know a simple test reaction for hydrazine solutions?

I've got a batch of hydra ...
6-7-2013 at 13:31
by: dangerous amateur
Lead styphnate vs AP, TATP, HMTD

[quote]
@ Dangerous Amature "-it's extremely sensitive to static, and static is something that is ...
6-7-2013 at 12:26
by: dangerous amateur
Lead styphnate vs AP, TATP, HMTD
Because

-its most likely mixed into some pyrotechnical composition and not pure. Also the amount ...
5-7-2013 at 10:10
by: dangerous amateur
NHN Synthesis, what procedure do you prefer, EtOH or not?
Hi,

what procedure do you prefer for NHN?
What gives the best crystals, heat it or not?
Use Eth ...
4-7-2013 at 03:12
by: dangerous amateur
ETN synthesis issue

[quote]
boiled close to azeotrope[/quote]

How do you know?
My guess would be your acid is not ...
4-7-2013 at 02:09
by: dangerous amateur
Please do not "play" with Organic Peroxides.

[quote]
What is the best primary explosive for kitchen pyros :D ? Sodium azide is very expensive ...
4-7-2013 at 01:55
by: dangerous amateur
Detonation properties of moist AN
@Hennig Brand:
A very interesting point. Thank you for your answer.


[quote]
and i don't get w ...
27-3-2013 at 11:36
by: dangerous amateur
Detonation properties of moist AN
I hoped to get some serious answers and no kewl AP shit.

I know about those water gels, but they ...
25-3-2013 at 14:11
by: dangerous amateur
Detonation of erythritol tetranitrate (ETN) with heated aluminum
If someone likes to develop such things for fun, why not?

I think it is doable, my caps, or rathe ...
21-3-2013 at 01:22
by: dangerous amateur
Detonation properties of moist AN

[quote]
You put it in 10 liters plastic water bottles with duct tape on the screw. It keeps dry f ...
19-3-2013 at 08:49
by: dangerous amateur
Detonation of erythritol tetranitrate (ETN) with heated aluminum
This is NOT an EBW.

[quote]
I set 6 of them off and all but one worked[/quote]

Yeah, they ma ...
19-3-2013 at 08:38
by: dangerous amateur
Detonation properties of moist AN
Hi,

when I do experiments with AN I allways make sure my AN is absolutely dry.

However, how do ...
19-3-2013 at 04:36
by: dangerous amateur
Detonation of erythritol tetranitrate (ETN) with heated aluminum
If it works like an EBW, whats the flash for?

I do not think this design will be reliable. I play ...
19-3-2013 at 04:20
by: dangerous amateur
Double salts storage stability
Underwater storage is out of question with finished caps, but thanks.

Any more suggestions on th ...
7-3-2013 at 01:32
by: dangerous amateur
Double salts storage stability
Hi,

is there any experience or database out there concerning silver acetylide/nitrate salts stora ...
6-3-2013 at 04:53
by: dangerous amateur
ETN recrystallization for max density
I did that before, but never bothered obout crystal shape and density.

My ETN is usually extremel ...
26-2-2013 at 02:43
by: dangerous amateur
MnO2 as a catalyst in Miedziankit and AN-mixtures
Hi there,

What do you know about the use of MnO2 as a catalyst for compositions with KClO3 and al ...
30-1-2013 at 08:06
by: dangerous amateur
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