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Why is methyl benzoate more reactive to EAS bromination than m-xylene?
Conditions: 0.5 mL of 0.05 M Br[sub]2[/sub] in 90% AcOH, added to 0.5 mL of 0.25 M solution of aryl ... |
19-3-2013 at 10:05
by: killswitch |
Proper Neutralization of Nitroglycerine
Mixing granular solid material into an acidic nitric ester is a very bad idea. |
4-3-2013 at 07:33
by: killswitch |
Transesterification
The blob behaved just like nitroglycerin, only a lot less viscous. |
4-3-2013 at 07:31
by: killswitch |
Best method for cleaning esters?
[rquote=276113&tid=23502&author=Motherload]Why sodium methoxide ?
A strong base like that m ... |
26-2-2013 at 10:10
by: killswitch |
Transesterification
I encountered this phenomenon firsthand when trying to purify picric acid via recrystallization from ... |
26-2-2013 at 06:43
by: killswitch |
Best method for cleaning esters?
I use the standard bicarb+brine method for deacidification and dessication, but was wondering if the ... |
26-2-2013 at 06:34
by: killswitch |
Peroxides and HBr
This line of thinking came up when I was introduced to anti-Markovnikov bromination via the HBr + H2 ... |
21-2-2013 at 09:38
by: killswitch |
Peroxides and HBr
The standard synthesis for TATP and HMTD call for HCl and H2O2. It occurs to me that using HBr with ... |
20-2-2013 at 08:05
by: killswitch |
Goddamned NMR
I know this sounds juvenile, but when deprived of computerized tools that do the work for me, interp ... |
11-12-2012 at 12:08
by: killswitch |
1,1’-azobis-1,2,3-triazole
So, any ideas on the bis(tetrazinedioxide) compound?
There would probably be an easier synthesis ... |
10-12-2012 at 12:55
by: killswitch |
Preparation of trinitromethane
[rquote=268001&tid=3061&author=starman]The admin gifted this member with the epithet " Do No ... |
10-12-2012 at 11:44
by: killswitch |
1,1’-azobis-1,2,3-triazole
[rquote=267863&tid=22584&author=AndersHoveland][rquote=267564&tid=22584&author=kills ... |
8-12-2012 at 01:06
by: killswitch |
1,1’-azobis-1,2,3-triazole
I'm working on an over-the-counter prep for the bistriazole.
Ethanol from everclear+drierite
Sod ... |
5-12-2012 at 16:04
by: killswitch |
1,1’-azobis-1,2,3-triazole
-------------------------------------
Glyoxal to triazole
REFERENCE EXAMPLE 1
preparation of Gl ... |
5-12-2012 at 15:01
by: killswitch |
1,1’-azobis-1,2,3-triazole
Sodium dichloroisocyanurate, per Klapotke's work. I've only done the 1,2,3 compound, though.
And ... |
5-12-2012 at 12:38
by: killswitch |
1,1’-azobis-1,2,3-triazole
Preparation of 1,1’-azobis-1,2,3-triazole
[img]http://upload.wikimedia.org/wikipedia/commons/th ... |
3-12-2012 at 07:49
by: killswitch |
dicyanoacetylene
What about tetrakis(cyanoethynyl)methane?
And I know this last one is pie-in-the-sky, but what ab ... |
11-11-2012 at 10:14
by: killswitch |
methyl nitrate
[rquote=262793&tid=744&author=PHILOU Zrealone][rquote=262572&tid=744&author=Kalium][ ... |
27-10-2012 at 15:56
by: killswitch |
Selling it all!
[rquote=261980&tid=21764&author=Ephesian]Reagents
Tons of Sigma Aldrich chemicals i'm not n ... |
16-10-2012 at 10:57
by: killswitch |
N,N-diethylaniline
I've been searching for ways to produce N,N-diethylaniline using over-the-counter reagents for quite ... |
16-10-2012 at 10:52
by: killswitch |
methyl nitrate
[rquote=260434&tid=744&author=Ral123]I just found my old 2.5cc model aircraft engine. First ... |
12-10-2012 at 11:35
by: killswitch |
dicyanoacetylene
Unbelievable! [url=http://www.tandfonline.com/doi/abs/10.1080/10601326708053999#preview]These guys[/ ... |
12-10-2012 at 10:52
by: killswitch |
dicyanoacetylene
I've been interested in this compound for some time now but have no clue how to synthesize it with a ... |
10-10-2012 at 09:37
by: killswitch |
Functionalization and polymerization of cubane
I've heard that functional groups can be added to cubane, but I haven't been able to find any public ... |
27-9-2012 at 16:38
by: killswitch |
PROBLEM DETONATING PICRIC ACID
Someone mentioned color. My picric acid is a bit yellowish, but I don't know if it's too yellow or i ... |
15-9-2012 at 17:17
by: killswitch |
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