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New Energetic Materials - Current Research
I diluted the solution with water to make it easy to crystallize, but this can make unprotonated ANQ ... |
24-5-2016 at 14:04
by: kratomiter |
New Energetic Materials - Current Research
After more than 12 hours in the freezer a little amount crystallized. It was my fault: large excess ... |
24-5-2016 at 13:32
by: kratomiter |
New Energetic Materials - Current Research
Need some help with ANQ nitrate. ANQ disolved instantly in large excess 67% HNO3 at 70ºC. Then I le ... |
23-5-2016 at 03:50
by: kratomiter |
Short question / quick answer - Thread
Thank you for your warning ecos. It will be a little batch, just to see if it's useful as a cheap pr ... |
22-5-2016 at 07:44
by: kratomiter |
New Energetic Materials - Current Research
It was a mistake, I mean ANQ nitrate. I'll post results tomorrow if I get something interesting. |
21-5-2016 at 13:14
by: kratomiter |
New Energetic Materials - Current Research
Wow, synthesis of DNQ seem pretty easy and straightforward for an amateur. I have some nitroguanidin ... |
20-5-2016 at 08:48
by: kratomiter |
New Energetic Materials - Current Research
I'm also interested in the synthesis of aminonitroguanidine. I'm gonna try the synthesis of guanidin ... |
19-5-2016 at 08:55
by: kratomiter |
Short question / quick answer - Thread
Thanks PHILOU for your answer, I'll try it soon.
[Edited on 19-5-2016 by kratomiter] |
19-5-2016 at 08:49
by: kratomiter |
Short question / quick answer - Thread
One quick question: I want to try the synthesis of guanidine perchlorate using ammonium perchlorate ... |
17-5-2016 at 12:35
by: kratomiter |
Exotic Primaries - Complex Salts
Recently I made two batches of NHN. The first was blue and very impure, I think EtOH made Calcium Hy ... |
13-5-2016 at 08:48
by: kratomiter |
Guanazoguanazole derivatives
I think I found the key: the sulfuric acid. I use drain cleaner which have lots of impurities. It do ... |
3-5-2016 at 12:11
by: kratomiter |
Guanazoguanazole derivatives
I did more test. I guess the yellow precipitated is HDNT with some impurities that give it its colou ... |
29-4-2016 at 13:33
by: kratomiter |
Guanazoguanazole derivatives
Of course, I'll send the paper to your mail.
I guess the presence of the azidotriazoles will be ... |
29-4-2016 at 09:16
by: kratomiter |
Guanazoguanazole derivatives
Great job PHILOU!
I've tried the diazotation with of the guanazole solution with the same conditi ... |
28-4-2016 at 12:59
by: kratomiter |
Guanazoguanazole derivatives
Thank you for both answers. I don't know what compound it is, maybe a nitrosamine, or maybe the cycl ... |
28-4-2016 at 02:59
by: kratomiter |
Guanazoguanazole derivatives
@Boffis This is the structure of guanazoguanazole (3,5,7-triamino-1,2,4-triazolo [4,3-A]-1,3,5-triaz ... |
27-4-2016 at 01:02
by: kratomiter |
Guanazoguanazole derivatives
I've tried the synthesis of guanazoguanazole from 2-cyanoguanidine and hydrazine sulphate just mixin ... |
26-4-2016 at 10:32
by: kratomiter |
Short question / quick answer - Thread
Hi! I'm trying to perform the synthesis of guanazoguanazole (and guanazole as byproduct) from 2-cyan ... |
24-4-2016 at 03:44
by: kratomiter |
Sodium methylenenitronate isolation
Thank you for your answer PHILOU! I'll give it another try when I get NaOMe. |
27-2-2016 at 12:59
by: kratomiter |
Sodium methylenenitronate isolation
Hi, I'm wondering if there's any way to dry and store sodium methylenenitronate.
It's easy to obta ... |
23-2-2016 at 09:59
by: kratomiter |
1,3,5-trichlorohexahydrotriazine
Recently I try to synthesize 1,3,5-trichlorohexahydrotriazine without success, using NaDCC instead o ... |
16-8-2015 at 02:58
by: kratomiter |
Designing a protocol to isolate alkaloids using SCX resin
BTW, a glass microfiber filter would be better for isolating alkaloids than standard lab paper filte ... |
6-10-2013 at 14:39
by: kratomiter |
Designing a protocol to isolate alkaloids using SCX resin
Thank you phlogiston. I don't use MeOH + glacial acetic acid, but I'll try next time (in step 1).
I ... |
1-10-2013 at 10:36
by: kratomiter |
Designing a protocol to isolate alkaloids using SCX resin
Hi!
I am conducting the first attempts to isolate Mitragyna Speciosa (Kratom) alkaloids using a s ... |
1-10-2013 at 05:47
by: kratomiter |
What is the actual mechanism for HMTD?
[rquote=282499&tid=24077&author=chemcam][rquote=282497&tid=24077&author=kratomiter]T ... |
30-4-2013 at 13:31
by: kratomiter |
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