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Drying alcohols with Sodium Glycoxide
The idea was that if one dissolved the glycoxide in ethanol, then the ethoxide would be generated wi ...
4-1-2010 at 18:48
by: unome
Drying alcohols with Sodium Glycoxide
Attached please find a paper on the drying of alcohols using sodium glycoxide (the sodium alkoxide o ...
3-1-2010 at 17:24
by: unome
Phosphoryl Halides - From P4O10 & Halide Salts
Told them I was cooking chips, cooking oil burns from that are a significant portion of all burns ca ...
25-12-2009 at 15:01
by: unome
What sort of shock/entropic change would set of Acetone peroxide?
Just wondering, 'if' the researcher's who studied the topic (from Israel, they have vast experience ...
24-12-2009 at 22:37
by: unome
Indole Synthesis
Attached find a review of the Fischer Indole synthesis.

24-12-2009 at 13:45
by: unome
Good (Legal-type) Journal Article on the Analogue Act
Here is a really interesting read for all who wish to understand the US Federal Analogue Act 1986 (i ...
24-12-2009 at 05:43
by: unome
Ephedrine from Propiophenone...
I've been thinking about something, we've all seen the papers where students are shown how to make [ ...
24-12-2009 at 05:08
by: unome
Phosphoryl Halides - From P4O10 & Halide Salts
Normal procedurally, seems the oil (cheap oil, used MANY, MANY times before at the same temp.) had a ...
20-12-2009 at 03:44
by: unome
Phosphoryl Halides - From P4O10 & Halide Salts
No, I have been searching for any and all references to this reaction specifically, and also similar ...
18-12-2009 at 21:32
by: unome
Phosphoryl Halides - From P4O10 & Halide Salts
Ok

I assume most people here have encountered the paper from Tarbutton, et al, which detailed a c ...
16-12-2009 at 01:16
by: unome
Conversion of Ecgonidine methyl ester to Ecgonine methyl ester
[rquote=166937&tid=13099&author=solo][b]Reference Information[/b]


[b]Enantioselective S ...
11-12-2009 at 17:36
by: unome
Preparation of elemental phosphorus
[rquote=166749&tid=65&author=watson.fawkes][rquote=166739&tid=65&author=unome]isn't ...
3-12-2009 at 22:03
by: unome
Preparation of elemental phosphorus
Often wondered.... As [url=http://en.wikipedia.org/wiki/Silicon]silicon[/url] is fairly easily arriv ...
3-12-2009 at 00:20
by: unome
Products from Ca benzoate and Ca propionate
UTFSE - hang on, just back up a little and have a look at the other threads on this first page of th ...
2-12-2009 at 23:09
by: unome
Acetic anhydride preparation
For the other devotees of Tarbutton, et al's work, here is one of the papers they actually disproved ...
2-12-2009 at 15:55
by: unome
Catechol preparation
Have to double-post (must have missed the deadline) but for anyone here who (1) speaks German; and ( ...
24-11-2009 at 00:57
by: unome
Catechol preparation
Why would diazotization be necessary? There are several papers where p/m/o-amino groups have been re ...
22-11-2009 at 20:49
by: unome
Yes You Can Make Your Own TCT - If You Dare!
Thought these might be interesting... On reacting glycine with 3 equivalents of hypochlorite, resear ...
4-11-2009 at 23:59
by: unome
Nitroethane - Does the ntirite have to dissolve?
Here is two on the use of a column to form the nitroalkane(s) from sodium/silver nitrite in a column ...
4-11-2009 at 20:37
by: unome
Ephedrine from Propiophenone...
Here is a procedure in which the authors (Patrick, McBee & Hass) prepare the relevant benzedrine ...
4-11-2009 at 16:30
by: unome
Preparation of ionic nitrites
Will sodium sulfate displace calcium nitrite? Calcium nitrite is widely available and cheap as chips ...
2-11-2009 at 06:34
by: unome
Amine electrophiles
There is also the reportedly facile decarboxylation of [url=http://orgsynth.org/orgsyn/pdfs/CV5P0567 ...
29-10-2009 at 22:36
by: unome
Ephedrine from Propiophenone...
Propiophenone can be got to via known routes (from benzoic acid and propionic acid by the procedure ...
29-10-2009 at 20:15
by: unome
Nitroethane - Does the ntirite have to dissolve?
What would be interesting is whether or not another metallic salt could be swapped for silver nitrit ...
28-10-2009 at 12:40
by: unome
Nitroethane - Does the ntirite have to dissolve?
I'm waiting on two papers from Kornblum, the one where he uses Sodium Nitrite with [url=http://pubs. ...
26-10-2009 at 17:23
by: unome
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