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Decent cell build.... Jeez....the simple K perchlorate+reducer mixtures seem so feeble and anemic because of the high deco ... |
17-6-2019 at 04:49 by: markx |
First yield of KClO3 from my cell [rquote=614867&tid=148990&author=yobbo II]Methylene blue is very sensitive towards perchlora ... |
10-6-2019 at 22:54 by: markx |
Decent cell build.... [rquote=614866&tid=144788&author=yobbo II]Perchlorate is much more stable than chlorate[/rqu ... |
10-6-2019 at 07:22 by: markx |
Decent cell build.... I also tried 87/13 and 65/35 ratios KClO[sub]4[/sub]/C respectively. These do not burn at all or do ... |
10-6-2019 at 01:20 by: markx |
Decent cell build.... I did spin some visco based on the KClO[sub]4[/sub]:
[file]75858[/file] [file]75860[/file] [ ... |
6-6-2019 at 12:27 by: markx |
Decent cell build.... The yield from the 205g (135ml) stock solution when converted into KClO[sub]4[/sub]:
[file]7 ... |
5-6-2019 at 08:30 by: markx |
Decent cell build.... The second conversion is done.....so is the anode. I let it cook until it passivated completely at t ... |
3-6-2019 at 00:13 by: markx |
Chemistry behind RDX "Chemistry and Technology of Explosives", By T. Urbański has rather comprehensive information about ... |
29-5-2019 at 02:50 by: markx |
Decent cell build.... She's clearly cooked and done (08.05.19-24.05.19):
[file]75644[/file] [file]75646[/file] [fi ... |
25-5-2019 at 01:25 by: markx |
PETN imposter? Can you conjure up a way to measure the melting point? It should be close to 140C for the desired e ... |
16-5-2019 at 23:27 by: markx |
Decent cell build.... I did measure the KClO[sub]4[/sub] yield in the collected liqour from the small 150ml cell conversio ... |
16-5-2019 at 04:18 by: markx |
Gas pressure/flow regulator There is no technical or chemical incompatibility between CO2 and N2 pressure regulators, but the th ... |
16-5-2019 at 03:12 by: markx |
Decent cell build.... It is coming along very nicely. ClO[sub]4[/sub]- content is growing steadily as recognized from prec ... |
15-5-2019 at 15:15 by: markx |
PETN imposter? Electrical coffee grinder works wonders on pulverizing raw materials. Beats a mortar and pestle by l ... |
15-5-2019 at 15:00 by: markx |
Gas pressure/flow regulator A decent rotameter with an adjustable needle valve after the pressure reducer be perhaps the simples ... |
15-5-2019 at 10:30 by: markx |
Decent cell build.... Zooo....the contrapulation has been fizzing away on my tabletop for about 5 days now. The anode stem ... |
13-5-2019 at 09:53 by: markx |
Cell design [rquote=611955&tid=148145&author=underground]Mark thanks a lot for your reply. So the 3"x10" ... |
9-5-2019 at 03:12 by: markx |
Cautionary tale I've had a very similar event happening under my watch. Fortunately the cell was outside and posed t ... |
8-5-2019 at 23:04 by: markx |
Ethanol Purification for Synthesis [rquote=611762&tid=148767&author=nimgoldman]Thanks for reassuring about the sufficiency of g ... |
8-5-2019 at 06:29 by: markx |
Do not buy this type of digital scales Everything comes from China nowadays....at least partly, so there is no guaranteed way around the is ... |
8-5-2019 at 05:44 by: markx |
Decent cell build.... The Ti rods arrived, so I proceeded to fabricate a new anode stem for the "ubercell":
[file]7528 ... |
8-5-2019 at 03:27 by: markx |
Do not buy this type of digital scales [rquote=611802&tid=149271&author=Keras]I am planning to buy a precision scale. Since I don†... |
7-5-2019 at 03:49 by: markx |
Centrifuge for pressing primary [rquote=611693&tid=149681&author=XeonTheMGPony] I do not think you guys have don any serious ... |
6-5-2019 at 08:21 by: markx |
Decent cell build.... The 600C 4 coat anode died at last......after accomplishing three full conversions of a total volume ... |
5-5-2019 at 23:22 by: markx |
Centrifuge for pressing primary [rquote=611680&tid=149681&author=twelti]Would it be correct to assume that if using an (ener ... |
5-5-2019 at 22:49 by: markx |
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