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Differentiating between amide and acid -- Case of an unknown material
Crush up some of your sample, seal one end of your capillary with a torch. Then pack in about 3mm of ...
6-2-2013 at 22:23
by: mnick12
Differentiating between amide and acid -- Case of an unknown material
I am not sure about the rate of hydrolysis for the compounds in question, I am assuming you are tal ...
5-2-2013 at 11:48
by: mnick12
N-acylation of L-proline
Thanks for the ref,

I hope I have some time to try this out in the next few weeks.
4-2-2013 at 10:25
by: mnick12
Differentiating between amide and acid -- Case of an unknown material
The hydrolysis of nitriles in acidic or alkaline conditions produces amides before they are further ...
4-2-2013 at 10:22
by: mnick12
Latest chemical order?
phenylhydrazine 500g
4-methoxyphenol 500g
phosphoryl chloride 1Kg
chloroacetamide 1Kg
THF 1L
4- ...
2-2-2013 at 00:10
by: mnick12
N-acylation of L-proline
Are you sure the nitrogen in proline is capable of participating in aminolysis with acceptable yield ...
31-1-2013 at 15:25
by: mnick12
N-acylation of L-proline
Hello everyone,

I am interested in synthesizing the some various N-acyl derivatives of L-proline. ...
30-1-2013 at 15:16
by: mnick12
Issues with reduction of vanillin
I did this reaction a while ago a on a larger scale, but the procedure was pretty similar to what s ...
23-1-2013 at 14:15
by: mnick12
Latest chemical order?
L-proline 250g
glycine 500g
L-alanine 500g

Anyone know where to buy chloroacetamide or ethyl ch ...
23-1-2013 at 13:44
by: mnick12
Acid Etching Metals
I worked in a lab where we did a lot of etching for examination of micro-structures. We were mostly ...
17-1-2013 at 11:48
by: mnick12
More fun with thiourea
Yes, I believe the product you are referring to is called Tarn-X. That surfactant could be a pain to ...
12-1-2013 at 14:24
by: mnick12
Distilling Ethanol
Back in junior high for a science fair I managed to make about 500ml of alcohol (not sure of the con ...
2-1-2013 at 23:40
by: mnick12
Williamson Ether Synthesis of Acetic Anhydride
I don't know why everyone gets the impression AA and acetyl chloride are so difficult to come by. Ma ...
2-1-2013 at 23:28
by: mnick12
The sol-gel process for electrodes; boehmite
edgecase is correct bentonite clays are a variety of ionic aluminosilicate minerals. Whereas Diatoma ...
9-8-2012 at 17:20
by: mnick12
Digoxin Extraction from Digitalis Purpurea.?????
I doubt you have a quantifiable amount of digoxin from two leaves,

The concentration is quite low ...
6-8-2012 at 12:59
by: mnick12
p-hydroxybenzaldehyde?
The p-hydroxybenzaldehyde which I have is a light reddish-pink, and even after recrystallizations fr ...
4-8-2012 at 21:19
by: mnick12
Multilayer Metal Oxide / Titanium Anodes for Chlorate/Perchlorate
Interesting,

Unfortunately I dont have the money for a teflon lined autoclave, and high pressure ...
4-8-2012 at 21:10
by: mnick12
Multilayer Metal Oxide / Titanium Anodes for Chlorate/Perchlorate
Well things arent looking so well,

Today I took the MnO2 and subjected it to 400C on my hotplate ...
3-8-2012 at 20:59
by: mnick12
Multilayer Metal Oxide / Titanium Anodes for Chlorate/Perchlorate
[rquote=256078&tid=9783&author=Xenoid]Your experience with electrodeposition would appear to ...
2-8-2012 at 19:36
by: mnick12
Multilayer Metal Oxide / Titanium Anodes for Chlorate/Perchlorate
Hmm I dont have any tin compounds however I suppose I could make some from some tine wire.

I know ...
1-8-2012 at 10:23
by: mnick12
Multilayer Metal Oxide / Titanium Anodes for Chlorate/Perchlorate
Hi Xenoid,

The MnO2 was deposited by using a modified version of Nurdrages procedure. From his vi ...
31-7-2012 at 10:04
by: mnick12
Multilayer Metal Oxide / Titanium Anodes for Chlorate/Perchlorate
Hate to bump an old thread, but I think this is the most appropriate thread to ask my question.

A ...
30-7-2012 at 16:23
by: mnick12
Sodium Acetate Impurities
IIRC most vinegar is made from the fermentation of grain ethanol, which involves the dilution of con ...
30-7-2012 at 15:38
by: mnick12
The short questions thread (3)
IIRC they quite available, http://www.ebay.com/sch/i.html?_nkw=rubber+septum&_sacat=0&_odkw= ...
28-7-2012 at 21:53
by: mnick12
chloroform is not forming
Did you confirm the presence of hypochlorite? Without doing some sort of conclusive testing it is ha ...
17-7-2012 at 16:09
by: mnick12
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