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Garage Experiments With Trichloromethane.
Do a search for trinitromethane (also called nitroform). And you should get plenty of information. |
27-9-2007 at 15:53
by: stygian |
dumbshit question of the week - reversed ester
I knew MPTP was a possible byproduct of manufacture, but do these esters indeed metabolise to the ne ... |
27-9-2007 at 09:30
by: stygian |
whats the HCOOH/Al reduction called?
The archetypical ammonium formate leuckart amination produces the N-formyl derivative, which is comm ... |
18-9-2007 at 08:14
by: stygian |
whats the HCOOH/Al reduction called?
To reduce an amide to an N-methyl. Not many of your more common agents seem capable of that. I was ... |
17-9-2007 at 19:53
by: stygian |
whats the HCOOH/Al reduction called?
A few years back I remember reading that it was an exceptionally powerful (yet simple) reducing syst ... |
17-9-2007 at 19:43
by: stygian |
aldol question, phenylpropane-1,2-diol?
I'm no chemist but what little I know seems to tell me that one could synthesize this quite easily f ... |
16-9-2007 at 19:35
by: stygian |
3-pyrrolidone?
Isn't the usual NMP the 2-keto form? is there a way to enolize/oxidize it to 3-keto? or is there ano ... |
9-5-2007 at 09:33
by: stygian |
Glyoxal Synthesis
The Org. Syn. Page says it can also be made by hydrolysis of dichlorodioxane. Would this be the sam ... |
11-6-2006 at 13:29
by: stygian |
Formaldehyde
[quote]
Production
Industrially, formaldehyde is produced by the catalytic oxidation of methanol. ... |
9-6-2006 at 18:15
by: stygian |
Guess I should have said phenylacetylcarbinol...
but anyway.. this is what I was trying to ask.
A known phenylacetone synth is BzCN + EtOAc -NaOMe ... |
4-6-2006 at 10:38
by: stygian |
Acetylating mandelonitrile?
Last night in a dream, I overheard an elf and a leprechaun saying something about how mandelonitrile ... |
4-6-2006 at 07:35
by: stygian |
Im confused. PhCHO + RNO2 = ?
I've always thought that benzaldehyde + nitroalkane -base-> nitroalkene, but I just read about ma ... |
13-5-2006 at 18:57
by: stygian |
Nitrile to ketone? with EtMgBr
I was wondering about the intermediate |
13-5-2006 at 18:18
by: stygian |
Nitrile to ketone? with EtMgBr
What is/are the intermediates formed from methadone nitrile and EtMgBr, to eventually yield the keto ... |
12-5-2006 at 15:19
by: stygian |
hydantoin alkylation?
My target was the benzylmethylhydantoin, via strecker or bucherer, hoping to find a way to a-Me-Phen ... |
27-4-2006 at 20:06
by: stygian |
hydantoin alkylation?
Interesting thanks. But Another idea has struck me.
Anybody want to speculate on the reaction of ... |
26-4-2006 at 16:23
by: stygian |
hydantoin alkylation?
Assume one has some 5-methylhydantoin.
Can this be alkylated at the 5 carbon with alkyl chloride ... |
25-4-2006 at 21:20
by: stygian |
keto-enol question
If you have a ketone like MEK, would the enol form be:
CH3C(OH)CHCH3 or CH2C(OH)CH2CH3 ? |
22-4-2006 at 13:37
by: stygian |
methylisopropylamines
Dont know if this should go in here or organic, but..
Assume you react acetone in a leuckart-styl ... |
18-4-2006 at 09:47
by: stygian |
This could be useful... new ketene prep?
Just stumbled across this pdf.
http://www.dupont.com/dms/docs/DMS_PUSH_Bulletin.pdf
Claims that ... |
23-2-2006 at 22:06
by: stygian |
pyrrolidinediethyl diacetate?
Googling "pyrrolidinediethyl diacetate" or any sort of lexical variation gives nothing but a tropino ... |
18-2-2006 at 14:56
by: stygian |
pyrrolidinediethyl diacetate?
I'm sure most here have read this:
[qoute]Tropinone. 10 g of pyrrolidinediethyl diacetate are h ... |
18-2-2006 at 12:55
by: stygian |
Electrochemical ozone generation
http://freepatentsonline.com/4316782.html |
30-1-2006 at 08:49
by: stygian |
Venlafaxine
Norephedrine isn't correct. It's norepinephrine (noradrenaline). It's norephedrine with catechol i ... |
27-12-2005 at 14:10
by: stygian |
Venlafaxine
I have used effexor recreationally before. A single time use dose (high enough, 150mg+) creates a p ... |
25-12-2005 at 19:20
by: stygian |
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