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Experimental Preparation of Chlorobutanol
Yes. So that's what that precipitate was...ahh...Truly a pain in the ass indeed. I will have to ...
27-4-2004 at 18:10
by: thunderfvck
Experimental Preparation of Chlorobutanol
Melting point 76*C. Not very good.

It still numbs my tongue though, so it must be chlorobutanol.
...
27-4-2004 at 15:46
by: thunderfvck
Experimental Preparation of Chlorobutanol
The reaction was kept cold until the boiling of acetone began. Even when I started heating it (at th ...
27-4-2004 at 11:03
by: thunderfvck
Experimental Preparation of Chlorobutanol
Well I'm finished...almost.

750 ml bleach (lemon scented - I had nothing else) with 15 ml ac ...
27-4-2004 at 00:07
by: thunderfvck
Experimental Preparation of Chlorobutanol
Interesting thread. I'm in the process of doing this as we speak! MUAHAHAH.

I found a good l ...
26-4-2004 at 19:53
by: thunderfvck
Trouble with vacuum filtration/better source of filter paper?
I'm using a vacuum pump that works well for every other filtration I try. Flow rate is good, it ...
24-4-2004 at 12:38
by: thunderfvck
Trouble with vacuum filtration/better source of filter paper?
Okay, well it worked fine with another little thing I have going at the moment. So I guess the last ...
22-4-2004 at 22:45
by: thunderfvck
Trouble with vacuum filtration/better source of filter paper?
You see, I could imagine myself using my mouth to suck out the liquid from a coffee filter. I mean, ...
22-4-2004 at 10:20
by: thunderfvck
Trouble with vacuum filtration/better source of filter paper?
Okay, I got a vacuum awhile ago and now I'm really trying to use it.

I have a buchner funnel ...
21-4-2004 at 17:35
by: thunderfvck
Possibility of sulphuric acid?
It's at Pharmaprix. Bottle reads:

Atlas (producer, labratoire Atlas inc., montreal, Quebec, ...
21-4-2004 at 16:16
by: thunderfvck
high-purity Mg needed for Grignards?
Sorry.

Woops! My bad. It'll only work for bromobenzene. Or chlorobenzene, etc. A hydrogen r ...
21-4-2004 at 15:06
by: thunderfvck
high-purity Mg needed for Grignards?
My chemistry book fails to mention iodine being used in Grignards. This is kind of sad. If I were to ...
21-4-2004 at 14:23
by: thunderfvck
Possibility of sulphuric acid?
Not even at the pharmacies? I'm sure you've already looked, but that's where I found ...
20-4-2004 at 08:10
by: thunderfvck
Cheaps scales vs. Pricey scales
haha

Yes, of course! This would seem more obvious to me if only I had my scale. Or maybe if I did ...
19-4-2004 at 15:07
by: thunderfvck
Cheaps scales vs. Pricey scales
Yep! Well I'm actually bidding on another one. I'm using SnipeRight, they have their own s ...
19-4-2004 at 14:39
by: thunderfvck
Containers
WHat about wine jars? Those are nice, amber usually. I have a nice 4 L one that's just asking m ...
19-4-2004 at 13:03
by: thunderfvck
Cheaps scales vs. Pricey scales
Thanks guys, I appreciate your replies.

I do think I will be sticking with the ohaus though. The ...
19-4-2004 at 13:02
by: thunderfvck
Cheaps scales vs. Pricey scales
You actually have to calibrate a mechanical scale? I thought it wasn't necessary...This may see ...
19-4-2004 at 07:19
by: thunderfvck
Cheaps scales vs. Pricey scales
Most excellent reply, Hermes. You have convinced me to go with the balance. I had no idea these digi ...
19-4-2004 at 00:06
by: thunderfvck
Cheaps scales vs. Pricey scales
Yes! So I found this REALLY cheap scale (0.01 g, 50 g max) on ebay...

http://cgi.ebay.com/ws/eBay ...
18-4-2004 at 22:10
by: thunderfvck
Battery acid
Well, I finally did it! My hotplate was out for repairs over the past week or two, and I haven' ...
18-4-2004 at 00:34
by: thunderfvck
Containers
I am trying to figure out what to use to hold my concentrated H2SO4. Will HDPE be alright? I have th ...
18-4-2004 at 00:27
by: thunderfvck
Nitrous oxide(laughing gas) to nitric acid
Ah! The alcohol strikes again! Sorry about that, axehandle. When you mentioned the V2O5, I immediate ...
15-4-2004 at 23:26
by: thunderfvck
Nitrous oxide(laughing gas) to nitric acid
LOL

Not many people are as...gifted...as you, axehandle.

:)
15-4-2004 at 00:01
by: thunderfvck
Nitrous oxide(laughing gas) to nitric acid
Just think about it man, if it was THIS easy, people at the explosives and weapons forum wouldn' ...
10-4-2004 at 11:24
by: thunderfvck
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