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Acetic anhydride, the 2nd.
Another interesting method:

Quite interesting...this is how chemistry attempted to produce sodiu ...
16-9-2003 at 05:50
by: BASF
Oleum prep
What about boiling/heating H2SO4 with a big portion of dissolved + undissolved KHSO4(or NaHSO4).
Su ...
13-9-2003 at 08:09
by: BASF
Distillation equipment
?? How is that meant?

After the distillation is complete, and the mix cools down(or is cooled dow ...
13-9-2003 at 07:50
by: BASF
Impressive cooling mixtures without dry ice
Thanks for the link...it turned out Linde is really selling dry-ice.

Let´s get ready for a trip ...
13-9-2003 at 07:38
by: BASF
Distillation equipment
I can only say i´ve tried both professional glassware and the improvised method using a stainless s ...
10-9-2003 at 02:40
by: BASF
radical-bromination of RDX
I´d like to try this next we, i have an idea on how to do it, but its fairly vague.

These are th ...
26-8-2003 at 05:23
by: BASF
Another one: the formaldehyde-"retro"-synth
Heat calcium formate.
26-8-2003 at 05:10
by: BASF
Acetic anhydride preparation
Anorganisch-chemisches Praktikum II

Darstellung von Schwefeldichlorid SCl2 aus Schwefelmonochlori ...
22-8-2003 at 07:06
by: BASF
Acetic anhydride preparation
BTW, what about zeolithes("molecular sieves";) for dehydrating HAc to Ac2O?

Molecular si ...
22-8-2003 at 07:01
by: BASF
Sodium (or Potassium) Sarcosinate
Wanna get tall and strong? :P:);)
22-8-2003 at 05:30
by: BASF
Impressive cooling mixtures without dry ice
I was hoping this would be the case...so, Haggis, this sounds like being quite uncomplicated and cos ...
22-8-2003 at 05:28
by: BASF
maybe hard, but not that hard
[quote]
Very Hard

Without PCl3 or PCl5, very hard.

http://www.rhodium.ws/chemistry/anhydride ...
20-8-2003 at 08:18
by: BASF
Impressive cooling mixtures without dry ice
https://www1.fishersci.com/education/resources/eqtip06.jsp

http://www.fisher.co.uk/techzone/table ...
20-8-2003 at 07:53
by: BASF
Impressive cooling mixtures without dry ice
After that many useful organic reactions are requiring less than -10....-20°C, and i now have a lit ...
20-8-2003 at 07:32
by: BASF
Acetic anhydride, the 2nd.
Hmm... could you explain your idea with a practical example?

This could be interesting, but aren ...
8-8-2003 at 04:38
by: BASF
Hexamine-Aluminumnitrate-x-hydrate-adduct
A coordination-compound out of hexamine and aluminum-nitrate precipitates out of a solution in ethyl ...
31-7-2003 at 07:42
by: BASF
Another weird idea...
Melt aluminum with an inorganic salt(or a combination of different ones) having the same specific de ...
29-7-2003 at 02:32
by: BASF
High-t (useful) ion exchange
Cool. Maybe you have a link about that?
But what exactly is semi-solid-state reaction? - Does it me ...
29-7-2003 at 02:17
by: BASF
High-t (useful) ion exchange
I recall that Al2O3 has a V E R Y high melting point, and i think adding other chlorides like CaCl2( ...
23-7-2003 at 09:12
by: BASF
Anyone interested in sulfur nitride?
Sounds interesting...

Sulfur nitride has not been discussed yet...not here, not on other forums, ...
23-7-2003 at 09:05
by: BASF
You the User!
Music: stoner metal !:cool::o:P:D

Chemistry: "The preparatory manual of explosives"
18-7-2003 at 09:32
by: BASF
HMX by way of nitration of dpt
Wouldn´t the phosphoric acid also act as a buffer, to certain extent?
If so, then maybe this would ...
17-7-2003 at 05:59
by: BASF
energetic coordination-compounds
Imagine a nitramine like RDX or HMX, or whatever.
The aza-functions of the ring are good lewis-base ...
27-6-2003 at 08:30
by: BASF
Bromination using KBR
Hmm.
Well, let´s explain another problem.
I´d also like to try bromination of RDX, but i only ha ...
26-6-2003 at 09:48
by: BASF
Iodination of organic compounds
Thanks for your thoughts so far!

It seems that the Finkelstein-reaction would be useful...i´ve a ...
26-6-2003 at 09:14
by: BASF
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