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Phenylacetaldehyde from Phenylalanine
I converted the supplementary materials to a PDF. Maybe that will help.
[file]51015[/file ... |
25-5-2016 at 07:19
by: Crowfjord |
Phenylacetaldehyde from Phenylalanine
Here's the paper and supplemental materials.
[b]Facile one-pot synthesis of tetrahydroisoquinolin ... |
24-5-2016 at 22:05
by: Crowfjord |
Phenylacetaldehyde from Phenylalanine
JJay: Did you see my post in that same thread? In order to isolate aldehyde in any decent yield, dil ... |
24-5-2016 at 15:45
by: Crowfjord |
borohydride/alcohol reactions and role in reductions
[quote]
Is the reaction between borohydride and alcohol required to produce the reducing agent re ... |
18-5-2016 at 18:42
by: Crowfjord |
borohydride/alcohol reactions and role in reductions
[quote]
or triacetoxyborohydride if ethanol is used[/quote]
Surely you mean triethoxy. Triaceto ... |
18-5-2016 at 15:22
by: Crowfjord |
help with mechanisms
Little to nothing should have reacted until base was added. Hydroxide deprotonates the nitroalkane t ... |
17-5-2016 at 17:58
by: Crowfjord |
A question
Probably. You will have to have a private chat with a mod. |
14-5-2016 at 09:25
by: Crowfjord |
A question
Ahhh, I see. |
14-5-2016 at 09:07
by: Crowfjord |
A question
Eosin Y, are you sure you have been banned and not temporarily suspended, or something? Usually when ... |
14-5-2016 at 08:46
by: Crowfjord |
dimethylation procedures & reagent choice
Chemrox, the following two articles contain experimental information you may find useful. They both ... |
19-4-2016 at 08:19
by: Crowfjord |
How to get started in sulfur organic chemistry?
How about alkyl thiosulfates (Bunte salts)? They are easily prepared from alkyl halides, preferably ... |
28-3-2016 at 20:10
by: Crowfjord |
electrochem reductionof org halides
TBAP (tetrabutylammonium perchlorate) is trivial to prepare from TBAB (tetrabutylammonium bromide). ... |
13-3-2016 at 10:20
by: Crowfjord |
Copper(I) Iodide Synthesis
Those sound fine for getting the iodide in there, but I don't see a reducer anywhere? How do you pla ... |
18-2-2016 at 14:15
by: Crowfjord |
Isolation of Cholesterol?
I think the ones we had at school were donated from a local hospital. Maybe you can get some if you ... |
14-2-2016 at 16:46
by: Crowfjord |
Isolation of Cholesterol?
I also isolated cholesterol from human gallstones as a college organic chemistry exercise. Pure cry ... |
14-2-2016 at 10:15
by: Crowfjord |
Oxidation of styrene to phenylacetaldehyde
Tetrahedron Letters 55 (2014) 5047–5051 describes the reactions of several amino acids with sodium ... |
1-2-2016 at 12:10
by: Crowfjord |
N,N-diethylamino-ethyl chloride synthesis
Here's one that uses thionyl chloride, from JACS Vol 66 pp 1921-1924 (1944):
[quote]
Preparation ... |
18-1-2016 at 15:23
by: Crowfjord |
N,N-diethylamino-ethyl chloride synthesis
The two are structurally related. It is the chlorinated analog of triethylamine. However, just becau ... |
17-1-2016 at 17:44
by: Crowfjord |
benzyl chloride syn
It does, Blogfast. It has to be concentrated hydrochloric acid, but it works pretty well. I have don ... |
29-12-2015 at 14:45
by: Crowfjord |
Pretty Pictures (2)
[file]46695[/file] [file]46697[/file] [file]46699[/file]
About a year and a half ago I made ... |
26-12-2015 at 10:30
by: Crowfjord |
The Short Questions Thread (4)
[rquote=432033&tid=25055&author=CuReUS]
what if you reacted 3-nitrobenzaldehyde with R-MgX ... |
20-12-2015 at 12:16
by: Crowfjord |
HBr in diazotation
HBr will work in the diazotation. I'm not so sure about the lactic acid version. |
19-12-2015 at 15:01
by: Crowfjord |
Bornyl chloride as alkylating agent?
[rquote=431662&tid=64678&author=blogfast25]
Is that mainly due to higher polarisation of th ... |
17-12-2015 at 16:04
by: Crowfjord |
The Short Questions Thread (4)
Grignards react with aromatic and aliphatic nitro compounds to give the disubstituted hydroxylamines ... |
17-12-2015 at 10:35
by: Crowfjord |
Bornyl chloride as alkylating agent?
The [url=http://pubs.rsc.org/en/Content/ArticleLanding/1931/JR/jr9310003340#!divAbstract]reference[/ ... |
16-12-2015 at 16:45
by: Crowfjord |
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