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Things I Will Never Make
Not really sure what the point of this thread is?
9-3-2017 at 11:26
by: DJF90
How to separate terpenes and sesquiterpenes dissolved in alcohol
Are you sure your compounds form an azeotrope with Ethanol?
19-2-2017 at 08:30
by: DJF90
Preparation of Chrome Yellow and Chrome Orange
Wonderful bright colours Amos, congratulations.
17-2-2017 at 02:37
by: DJF90
Super oxidizer: combination of periodate and peroxodisulfate
Could the dark solid be nickel peroxide, NiO2?
16-2-2017 at 00:35
by: DJF90
Decided on a goal - chloramphenicol.
[rquote=474262&tid=72226&author=PirateDocBrown]Well, I'm going to aim at racemic synthesis a ...
10-2-2017 at 04:44
by: DJF90
Diffusion pump oil
[rquote=473915&tid=72141&author=ElizabethGreene]That same oil was mentioned here (fascinatin ...
7-2-2017 at 05:15
by: DJF90
Lab scale contact process for H2SO4 (report)
@Microtek - Thanks for taking the time to elaborate. I took a few minutes after my last comment to h ...
7-2-2017 at 02:03
by: DJF90
Lab scale contact process for H2SO4 (report)
Nice reduction to practice. I'm sure with further time and resources you can get it to run more effi ...
6-2-2017 at 14:23
by: DJF90
Alternatives to sulphuric acid for make ethyl borate
Start with boric anhydride. It can be made by heating the acid under suitable conditions.
5-2-2017 at 14:00
by: DJF90
Tosylation of ethanolamine (??)
[rquote=473477&tid=71566&author=DrDevice]
I used morpholine rather than pyridine as it is e ...
2-2-2017 at 06:10
by: DJF90
Separating volatile oil in water emulsion to 2 separate layers
NaCl should work fine; 25 %w/w is about saturated at RT, so make sure you're using enough in order t ...
30-1-2017 at 10:15
by: DJF90
Chemie et Industrie
You should be able to get Bull Soc Chim here: http://gallica.bnf.fr
30-1-2017 at 06:33
by: DJF90
Separating volatile oil in water emulsion to 2 separate layers
You could try salting it out by saturating the aqueous phase with NaCl...
30-1-2017 at 04:48
by: DJF90
latest glassware purchase
[rquote=472214&tid=71645&author=Sulaiman]I do not know how you will manage without a fifth n ...
21-1-2017 at 11:06
by: DJF90
Benzoquinone from Paracetamol
You might find that by cooling the distillate in the fridge/ice bath for a few hours might make the ...
16-1-2017 at 08:35
by: DJF90
Benzoquinone from Paracetamol
I don't think it poses that much of an issue, or it wouldn't be recommended.

See http://www.orgs ...
16-1-2017 at 08:09
by: DJF90
Benzoquinone from Paracetamol
Benzoquinone is not particularly soluble in water and so should crystallise out. Just collect the di ...
16-1-2017 at 04:29
by: DJF90
Benzoquinone from Paracetamol
I would set up for steam distillation and use this property of benzoquinone to advantage. Amarego an ...
15-1-2017 at 23:37
by: DJF90
Two spectroscopic questions
i have been using ESI-MS for over two years now on a daily basis and routinely only see the parent i ...
15-1-2017 at 03:54
by: DJF90
Mystery Glassware Identification Thread
It is intended to sit in a bottle of standardised solution ready for whenever the need for titration ...
12-1-2017 at 02:07
by: DJF90
Mystery Glassware Identification Thread
Its an auto-filling burette?
11-1-2017 at 16:05
by: DJF90
When drying salts how do you prevent cake formation sticking to glass?
I don't see what the problem is? Just scrape it with a spatula.
11-1-2017 at 07:24
by: DJF90
My library
Nice books, Veg. Thats quite a collection you've got there!
10-1-2017 at 04:46
by: DJF90
correct size ring stand for 1000ml sep funnel?
@Magpie - Its a PTFE gland from Cowie:
http://www.cowie.com/catalogue/guides.htm
...details on the ...
2-1-2017 at 11:49
by: DJF90
correct size ring stand for 1000ml sep funnel?
Nope. On that scale the sep funnel is stationary; phase mixing is performed in a 20 L flask and then ...
2-1-2017 at 10:12
by: DJF90
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