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Sodium tetrachloroaluminate
Found a paper that suggests that NaAlCl4 can be electrolyzed in Propylene carbonate to form sodium m ...
18-8-2021 at 06:22
by: Triflic Acid
Building a Lab Sink.
No one needs to know:P
17-8-2021 at 20:29
by: Triflic Acid
Building a Lab Sink.
So, I've been thinking of routing the waste into a French drain type thing that already right outsid ...
17-8-2021 at 13:03
by: Triflic Acid
Building a Lab Sink.
I'm pretty good about getting rid of the stuff before dumping, but its a real pain when I'm working ...
15-8-2021 at 20:32
by: Triflic Acid
Building a Lab Sink.
Lacking any source of running water is a challenge for my garage lab. I could always get water from ...
15-8-2021 at 16:53
by: Triflic Acid
Big Glassware Sale!
Might I ask what happened to your lab? You keep selling stuff off. Sorry to be nosy
14-8-2021 at 21:36
by: Triflic Acid
Unsure if Followed Dinitrophenol Synthesis Correctly
That looks like tar, did you keep the temperature under control? Generally phenol nitration is prett ...
14-8-2021 at 06:57
by: Triflic Acid
Too good to be true?
@karlos, I might just commit scientific fraud to watch that :P
12-8-2021 at 19:13
by: Triflic Acid
Too good to be true?
Found this patent a few days ago from china: https://patents.google.com/patent/CN1209290C/en

Clai ...
12-8-2021 at 06:19
by: Triflic Acid
Any uses for lithium metal
Take a large chunk, and cast it down into the shape of L and i. Then encase your new element sample ...
7-8-2021 at 13:14
by: Triflic Acid
Oxalyl Chloride Challenge
So the oxalyl chloride produced reacts with the free amine on the atrazine. Maybe making the dihydro ...
6-8-2021 at 07:07
by: Triflic Acid
Oxalyl Chloride Challenge
cyanuric chloride reacts with oxalyl acid to form oxalyl chloride
5-8-2021 at 15:44
by: Triflic Acid
cleaning up radium containing sample somewhat
Nuetralize, and then just dump it where you found the tailings. The place is radioactive anyways.
4-8-2021 at 09:01
by: Triflic Acid
hydrazobenzene
Have you tried hydrogenating the azobenzene. I would think you have a good amount of it by now. Hydr ...
3-8-2021 at 06:50
by: Triflic Acid
Quenching excess H2 in a reaction.
Tom from tom's lab is still okay after lighting the excess hydrogen: https://www.youtube.com/watch?v ...
1-8-2021 at 09:11
by: Triflic Acid
Help! Finding cheap flow chemistry reactor tube & accessories
Well, what are you making in flow?
1-8-2021 at 07:30
by: Triflic Acid
Quenching excess H2 in a reaction.
Or, just light a match at the end of a long thin glass tube coming from the reaction vessel. Burns o ...
1-8-2021 at 07:28
by: Triflic Acid
Protecting groups for tertiary amines
Ethanol should work as a solvent. If you have more than one go at this, try both ways. The diethyl o ...
31-7-2021 at 07:24
by: Triflic Acid
Heating bath agitation and temp control?
Well, for the first question, I would recommend an aquarium air bubbler at a low flow rate. As long ...
29-7-2021 at 10:10
by: Triflic Acid
Is vulcanizing latex reasonable to DIY? Are there OTC chemicals to do it?
Try sulfur chlorides. There is a prep somewhere here on using for rubber vulcanization.
29-7-2021 at 05:55
by: Triflic Acid
Electrodeposition of alkaline metals from propylene carbonate solutions of salts
Also, for those looking for PC, some types of non-acetone nail polish removers have PC and EtOH mixe ...
28-7-2021 at 05:30
by: Triflic Acid
nitrosobenzene
For the condensation reaction, you seem to be talking about the ehrlich-sachs reaction. I've never d ...
27-7-2021 at 06:15
by: Triflic Acid
Compilation: Synthetic routes to tetrazole compounds based on OTC materials.
If anyone wants to try a better way of getting guanidine nitrate, check nurdrage's video. Just react ...
27-7-2021 at 05:09
by: Triflic Acid
Help with solvent extraction and TLC of 5 hydroxymethyl furfural
The streaking is not actually because of a large spot, the dmso doesn’t evaporate and carries some ...
26-7-2021 at 21:11
by: Triflic Acid
Help with solvent extraction and TLC of 5 hydroxymethyl furfural
Yeah, don’t have any hexane sadly. But, dcm seemed to work well. Tlc attached. The dmso screwed th ...
26-7-2021 at 18:24
by: Triflic Acid
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