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so much Cerium and InCl3 what to do with it?
CeCl3 is quite good at this: http://en.wikipedia.org/wiki/Luche_reduction
EDIT: somewhere on this ... |
20-1-2014 at 22:13
by: UnintentionalChaos |
Reduction of rust to Fe(0)
[rquote=316113&tid=28599&author=elementcollector1]Clearly (and I don't mean to insult here) ... |
20-1-2014 at 16:28
by: UnintentionalChaos |
Synthesis of unsym.-heptachloropropane and hexachloropropene (updated)
It only took me 13 months, but I finally got around to dehydrohalogenating my unsym-heptachloropropa ... |
19-1-2014 at 13:07
by: UnintentionalChaos |
Bad days in the lab or with glassware?
[rquote=267260&tid=24908&author=Eddygp]A hot test tube dropped in a cold water bath... CRACK ... |
17-1-2014 at 23:51
by: UnintentionalChaos |
Molybdenum from molybdic acid - success!
Molybdenum readily forms heteropolyacids with things like silicon oxides, arsenic oxides, phosphates ... |
17-1-2014 at 23:16
by: UnintentionalChaos |
Science equipment looking for a home
[img]http://fanboygaming.com/wp-content/uploads/2013/06/shut-up-and-take-my-money.jpeg[/img]
[b]D ... |
17-1-2014 at 20:40
by: UnintentionalChaos |
Pretty Pictures (2)
Not the best shot ever, but these hydroxylammonium chloride crystals won't cooperate with my camera. ... |
17-1-2014 at 13:10
by: UnintentionalChaos |
Ether drying, amount of Na needed?
[rquote=315683&tid=23247&author=Damitwhy]I've found that when making Diethyl Ether via Sulfu ... |
16-1-2014 at 19:12
by: UnintentionalChaos |
Preparation of Hünig's base (diisopropylethylamine)
Excellent work. DIPEA is probably overkill for most preparations vs TEA but it's inability to form q ... |
13-1-2014 at 17:18
by: UnintentionalChaos |
Drying Sodium Hydroxide
Don't bother, the only good way to dry it is to heat it while molten after which you still have to g ... |
13-1-2014 at 15:43
by: UnintentionalChaos |
Preparation of 2,4-dinitrobromobenzene
[rquote=315262&tid=28480&author=TheChemiKid]Are you uploading this to your youtube channel o ... |
13-1-2014 at 14:06
by: UnintentionalChaos |
Preparation of 2,4-dinitrobromobenzene
2,4-dinitrobromobenzene is a highly useful organic intermediate. The ortho and para nitro groups rel ... |
12-1-2014 at 23:22
by: UnintentionalChaos |
Little things that surprised you in chemistry
How bloody dense mercury is...and bromine for that matter.
Also I recently made a tiny bit of din ... |
12-1-2014 at 21:03
by: UnintentionalChaos |
New possible efficient and clean electrolytic hydrogenation/reduction of aromatic compounds
What the fuck are you talking about. I feel like I'm reading some sort of drivel posted by Anders Ho ... |
11-1-2014 at 13:46
by: UnintentionalChaos |
How do I make Phenol from dichlorobenzene
[rquote=314787&tid=28433&author=Jmap science]I was thinking they did would forum 1,4 phenol. ... |
9-1-2014 at 17:54
by: UnintentionalChaos |
Carbene mechanism with malononitrile
There is no carbene there. That is a carbanion. A carbene is a charge-neutral carbon species with tw ... |
9-1-2014 at 09:50
by: UnintentionalChaos |
Grignard SS compatibility?
The original question was posed in October of last year and was only replied to today. I suspect the ... |
9-1-2014 at 09:45
by: UnintentionalChaos |
Help synthesizing icilin
I have read considerably into this as the compound interests me (along with capsaicin...).
1) Nit ... |
9-1-2014 at 02:58
by: UnintentionalChaos |
stretch translucent sticky adhesive? used in packaging
Apparently this type of glue is referred to as "fugitive glue," a name I found by google searching f ... |
5-1-2014 at 21:10
by: UnintentionalChaos |
Benzoin condensation with thiamine
Yes. It's a well known procedure used for teaching purposes in undergrad organic labs. You could hav ... |
4-1-2014 at 17:30
by: UnintentionalChaos |
Ethyl Isopropyl Ether
Aluminum is an inappropriate metal choice here. It's oxide is amphoteric and it's halides are powerf ... |
4-1-2014 at 16:43
by: UnintentionalChaos |
Pretty Pictures (2)
[img]http://i.imgur.com/WlEuNxK.jpg[/img]
My brother is into photography and recently built a dif ... |
31-12-2013 at 13:03
by: UnintentionalChaos |
reduction of nitrobenzene -> p-aminophenol
[rquote=313183&tid=27849&author=Nickdul]
I'd have to find my notes, but the hydrolysis was ... |
29-12-2013 at 08:54
by: UnintentionalChaos |
reduction of nitrobenzene -> p-aminophenol
I am aware that I am somewhat off-topic here, but is acetaminophen not commonly available where you ... |
29-12-2013 at 08:30
by: UnintentionalChaos |
Pretty Pictures (2)
[rquote=312590&tid=26378&author=elementcollector1]
I thought this produced sodium hypopho ... |
26-12-2013 at 11:21
by: UnintentionalChaos |
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