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Crystals from vapor?
Almost all my salt solutions evaporated in repurposed glass jars does this, even more than shown her ...
21-4-2017 at 14:26
by: Σldritch
How to separate a bismuth - tin alloy?
Would not sodium hydroxide be the easiest and possibly cheapest way to dissolve the tin as sodium st ...
21-4-2017 at 14:11
by: Σldritch
Cheap nitrates to potassium nitrate
Coincidentally i made calcium nitrate from ammonium calcium nitrate today by dissolving it in tap wa ...
21-4-2017 at 14:07
by: Σldritch
Interesting benzyl chloride synth I discovered
TCCA should inhibit Friedel-Crafts chlorination by complexing to Ferric chloride. NaDCC complexes wi ...
5-4-2017 at 01:30
by: Σldritch
Oxidation of iron by ferric nitrate and oxygen
Im doing homework and i need to know the reaction in the title. I think it would go something like t ...
29-3-2017 at 11:51
by: Σldritch
Bad days in the lab or with glassware?
While on my accident streak I had an accidental detonation. I was trying to make nitrite by the redu ...
23-3-2017 at 13:26
by: Σldritch
Copper Peroxide
I was trying to make copper peroxide too until i ran out of ammonia but i tried
reacting copper h ...
10-3-2017 at 00:42
by: Σldritch
Dithonite and copper sulfate
Tried this and got a brown precipitate and horrable smell.

DO THIS OUTSIDE!!!

Still filtering, ...
6-3-2017 at 11:21
by: Σldritch
Ammonium Acetate
No Ammonia is a much weaker base than Sodium Hydroxide so the reverse reaction is favored. Also Ammo ...
8-2-2017 at 01:21
by: Σldritch
Best and worst smelling chemicals?
I was trying to make isopropyl benzoate by fischer esterification recently and it did not work very ...
3-2-2017 at 13:04
by: Σldritch
Unsure how to effectively filter nickle sludge and clean remaining residue from glasswear
Acidic iron (III) chloride might work but if piranha solution does not do it i doubt ferric chloride ...
3-2-2017 at 08:56
by: Σldritch
Fluorides from PTFE
Thanks, i used plenty of ventilation so i think i will be fine, still aproacing the 8 hour mark thou ...
31-1-2017 at 12:08
by: Σldritch
Fluorides from PTFE
Today I tried to make sodium fluoride from PTFE by fusing it with sodium hydroxide.

Guessing the ...
31-1-2017 at 10:14
by: Σldritch
Parafin wax at 70:1 potassium nitrate?
From my experience of potassium nitrate you want fuels that are not very volatile such as sugar or c ...
11-1-2017 at 11:51
by: Σldritch
Imidazole Synthesis Route
Thanks for all the replies, i think Cryolite is right about the hydantoin reduction too since one of ...
14-12-2016 at 10:25
by: Σldritch
Imidazole Synthesis Route
Potassium cyanate seems easy enough but glycine seems harder. I can not find any place that sells it ...
13-12-2016 at 12:27
by: Σldritch
Imidazole Synthesis Route
Im trying to make Imidazole and i have come up with a synthetic route which i would like the forums ...
13-12-2016 at 10:33
by: Σldritch
Preparation of ionic nitrites
[rquote=461279&tid=52&author=Melgar]
Blue Fe(II)SO4 mixed with yellow sulfur would give a g ...
17-9-2016 at 13:13
by: Σldritch
Preparation of ionic nitrites
Im trying too make nitrite by reduction with sulfur (2 NaNO3 + S + NaX --> 2 NaNO2 + NaSO4 + X2) ...
16-9-2016 at 06:02
by: Σldritch
Most overrated and underrated hazardous chemicals?
[rquote=459589&tid=68548&author=metalresearcher]What about ClF3 ?
I think that is the nasti ...
1-9-2016 at 07:46
by: Σldritch
Exotic Primaries - Complex Salts
[rquote=456425&tid=1778&author=PHILOU Zrealone]
The water content is also to blame...it wil ...
30-7-2016 at 11:50
by: Σldritch
Iron (III) Acetate Oxide Persulfate Trihydrate (?)
I tried to prepare the compound in the title and i think i have suceeded.
The name is kind of crazy ...
30-7-2016 at 10:14
by: Σldritch
Alkyl nitrites reduction
[rquote=448621&tid=65691&author=CuReUS][rquote=448083&tid=65691&author=Σldritch]
Y ...
11-5-2016 at 21:53
by: Σldritch
Alkyl nitrites reduction
I tought it was easy based on videos like this but maybe im wrong, atleast it would be easier for me ...
11-5-2016 at 08:13
by: Σldritch
Alkyl nitrites reduction
https://www.erowid.org/archive/rhodium/chemistry/nitrite2nitro.html

You might be able to make the ...
6-5-2016 at 12:09
by: Σldritch
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