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Trouble with synthesizing HClO4
Some of my prior research results on preparing perchlorate:

Per the supplied paper by Icelake, "P ...
22-3-2020 at 11:08
by: AJKOER
The simplest preparation of sulfuric acid?!
[rquote=631462&tid=79548&author=AJKOER]
....
Second, an interesting nonredox reaction equi ...
2-3-2020 at 19:21
by: AJKOER
Aerial oxidation of ferrous ions
From Chemosphere, 2007 Aug;68(11):2080-4. Epub 2007 Mar 21.

"The effect of pH on the kinetics of ...
28-2-2020 at 19:00
by: AJKOER
Ceric ammonium nitrate- uses and synthesis
Some interesting comments at this ScienceDirect source (see https://www.sciencedirect.com/topics/ch ...
27-2-2020 at 06:43
by: AJKOER
Marsh test : classical test for arsenic detection
As to mechanics, in an old text, it has been noted that nascent hydrogen generated in situ by an aci ...
26-2-2020 at 18:42
by: AJKOER
Why is sodium carbonate not used as starting point for hypochlorite/chlorate production?
Per a source (see https://books.google.com/books?id=dXn3aB1DKk4C&pg=PA454&lpg=PA454&dq=n ...
24-2-2020 at 13:57
by: AJKOER
Ammonium Nitrate in Canada
Find stump remover (containing near pure KNO3) and CuSO4. Mix in proper proportions and freeze out t ...
23-2-2020 at 10:31
by: AJKOER
The simplest preparation of sulfuric acid?!
Two comments:

First, on the alcohol/bisulfate mix, H2SO4/KHSO4 may be a case of a so-called acid ...
22-2-2020 at 18:27
by: AJKOER
is there any way to make antimony trioxide from antimony solutions
From atomistry.com (http://antimony.atomistry.com/antimony_trioxide.html), which sources its materia ...
21-2-2020 at 12:13
by: AJKOER
Advanced Re-Visit of Silver Cleaning
[rquote=631394&tid=154911&author=unionised][rquote=631388&tid=154911&author=AJKOER]
...
21-2-2020 at 10:35
by: AJKOER
Advanced Re-Visit of Silver Cleaning
I start with the usual simple depiction of the electrochemistry based removal of Ag2S from Sterling ...
21-2-2020 at 06:41
by: AJKOER
A true implosive
Suggested Safe Implosion Demo for a School Class

I once filled a plastic distilled water bottle ...
21-2-2020 at 04:11
by: AJKOER
Photochemical oxidation of oxalate
[rquote=630651&tid=150512&author=Bedlasky]Thank you very much Ajkoer for explanation. Would ...
7-2-2020 at 07:15
by: AJKOER
Photochemical oxidation of oxalate
[rquote=613726&tid=150512&author=Bedlasky]
......
Another good photoreaction is oxidation ...
6-2-2020 at 19:09
by: AJKOER
Attempts to make calcium iodide
Per below: a recipe for FeI2, which is the cited starting compound to make iodides, per prior discus ...
13-1-2020 at 10:36
by: AJKOER
anyway to make [Ag(NH3)2]Cl? (having trouble)
For the home chemist, one can prepare [Ag(NH3)2]Cl, by first dissolving Ag in a combination of vineg ...
13-1-2020 at 05:12
by: AJKOER
Attempts to make calcium iodide
[rquote=629369&tid=154697&author=unionised]Still waiting for anything to rule out the idea o ...
13-1-2020 at 04:34
by: AJKOER
Attempts to make calcium iodide
Thanks Unionised for your reveiw.

My further analysis, which is the heart of my atomic iodine pre ...
12-1-2020 at 08:01
by: AJKOER
Attempts to make calcium iodide
First, I cited an old prep for the salt in question, namely CaI2, not FeI2!

Next, I outlined the ...
11-1-2020 at 09:16
by: AJKOER
Attempts to make calcium iodide
Based on this source http://calcium.atomistry.com/calcium_iodide.html (extracted from old chemistry ...
10-1-2020 at 18:33
by: AJKOER
Autoignition temperature of mixed gases
My recollection is that it is red light from an LED that explodes a pure mixture of H2 and Cl2 with ...
13-12-2019 at 14:31
by: AJKOER
Yellowing of Sodium Methoxide
Actually, I would suspect it is the action of light, likely lab light rich in UV, as CH3OH is repute ...
13-12-2019 at 14:12
by: AJKOER
Best conditions for sulphur iodide
I would start by working with the 1940 process (I cited above) and potentially improve upon it by wo ...
12-12-2019 at 06:01
by: AJKOER
H2SO4 on an extreme budget?
From an old thread, which also provides this statement per a cited source:

"3 HOCl + Al --> Al ...
10-12-2019 at 14:03
by: AJKOER
H2SO4 on an extreme budget?
Just came across the following reported reaction at http://sulphur.atomistry.com/hydrogen_sulphide.h ...
10-12-2019 at 05:20
by: AJKOER
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