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Trouble with synthesizing HClO4
Some of my prior research results on preparing perchlorate:
Per the supplied paper by Icelake, "P ... |
22-3-2020 at 11:08
by: AJKOER |
The simplest preparation of sulfuric acid?!
[rquote=631462&tid=79548&author=AJKOER]
....
Second, an interesting nonredox reaction equi ... |
2-3-2020 at 19:21
by: AJKOER |
Aerial oxidation of ferrous ions
From Chemosphere, 2007 Aug;68(11):2080-4. Epub 2007 Mar 21.
"The effect of pH on the kinetics of ... |
28-2-2020 at 19:00
by: AJKOER |
Ceric ammonium nitrate- uses and synthesis
Some interesting comments at this ScienceDirect source (see https://www.sciencedirect.com/topics/ch ... |
27-2-2020 at 06:43
by: AJKOER |
Marsh test : classical test for arsenic detection
As to mechanics, in an old text, it has been noted that nascent hydrogen generated in situ by an aci ... |
26-2-2020 at 18:42
by: AJKOER |
Why is sodium carbonate not used as starting point for hypochlorite/chlorate production?
Per a source (see https://books.google.com/books?id=dXn3aB1DKk4C&pg=PA454&lpg=PA454&dq=n ... |
24-2-2020 at 13:57
by: AJKOER |
Ammonium Nitrate in Canada
Find stump remover (containing near pure KNO3) and CuSO4. Mix in proper proportions and freeze out t ... |
23-2-2020 at 10:31
by: AJKOER |
The simplest preparation of sulfuric acid?!
Two comments:
First, on the alcohol/bisulfate mix, H2SO4/KHSO4 may be a case of a so-called acid ... |
22-2-2020 at 18:27
by: AJKOER |
is there any way to make antimony trioxide from antimony solutions
From atomistry.com (http://antimony.atomistry.com/antimony_trioxide.html), which sources its materia ... |
21-2-2020 at 12:13
by: AJKOER |
Advanced Re-Visit of Silver Cleaning
[rquote=631394&tid=154911&author=unionised][rquote=631388&tid=154911&author=AJKOER]
... |
21-2-2020 at 10:35
by: AJKOER |
Advanced Re-Visit of Silver Cleaning
I start with the usual simple depiction of the electrochemistry based removal of Ag2S from Sterling ... |
21-2-2020 at 06:41
by: AJKOER |
A true implosive
Suggested Safe Implosion Demo for a School Class
I once filled a plastic distilled water bottle ... |
21-2-2020 at 04:11
by: AJKOER |
Photochemical oxidation of oxalate
[rquote=630651&tid=150512&author=Bedlasky]Thank you very much Ajkoer for explanation. Would ... |
7-2-2020 at 07:15
by: AJKOER |
Photochemical oxidation of oxalate
[rquote=613726&tid=150512&author=Bedlasky]
......
Another good photoreaction is oxidation ... |
6-2-2020 at 19:09
by: AJKOER |
Attempts to make calcium iodide
Per below: a recipe for FeI2, which is the cited starting compound to make iodides, per prior discus ... |
13-1-2020 at 10:36
by: AJKOER |
anyway to make [Ag(NH3)2]Cl? (having trouble)
For the home chemist, one can prepare [Ag(NH3)2]Cl, by first dissolving Ag in a combination of vineg ... |
13-1-2020 at 05:12
by: AJKOER |
Attempts to make calcium iodide
[rquote=629369&tid=154697&author=unionised]Still waiting for anything to rule out the idea o ... |
13-1-2020 at 04:34
by: AJKOER |
Attempts to make calcium iodide
Thanks Unionised for your reveiw.
My further analysis, which is the heart of my atomic iodine pre ... |
12-1-2020 at 08:01
by: AJKOER |
Attempts to make calcium iodide
First, I cited an old prep for the salt in question, namely CaI2, not FeI2!
Next, I outlined the ... |
11-1-2020 at 09:16
by: AJKOER |
Attempts to make calcium iodide
Based on this source http://calcium.atomistry.com/calcium_iodide.html (extracted from old chemistry ... |
10-1-2020 at 18:33
by: AJKOER |
Autoignition temperature of mixed gases
My recollection is that it is red light from an LED that explodes a pure mixture of H2 and Cl2 with ... |
13-12-2019 at 14:31
by: AJKOER |
Yellowing of Sodium Methoxide
Actually, I would suspect it is the action of light, likely lab light rich in UV, as CH3OH is repute ... |
13-12-2019 at 14:12
by: AJKOER |
Best conditions for sulphur iodide
I would start by working with the 1940 process (I cited above) and potentially improve upon it by wo ... |
12-12-2019 at 06:01
by: AJKOER |
H2SO4 on an extreme budget?
From an old thread, which also provides this statement per a cited source:
"3 HOCl + Al --> Al ... |
10-12-2019 at 14:03
by: AJKOER |
H2SO4 on an extreme budget?
Just came across the following reported reaction at http://sulphur.atomistry.com/hydrogen_sulphide.h ... |
10-12-2019 at 05:20
by: AJKOER |
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