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Replacement for acetonitrile in oxone oxidation
Does anyone have any idea if this method would work on conjugate dienes like sorbic acid and piperin ...
22-1-2023 at 02:41
by: Boffis
Synthesis of malonic acid
Hi kmno4. I haven’t replied to this thread earlier as when at home over the Christmas period I was ...
19-1-2023 at 13:05
by: Boffis
Can DCM act as a Lewis Acid?
If you have washed the reaction mixture with water then the AlCl3 will have hydrolysed and perform n ...
20-12-2022 at 01:15
by: Boffis
DNP synthesis
Firstly EvlRenne; from where did this procedure come? Phenol nitrates easily to the mononitro compou ...
20-12-2022 at 01:08
by: Boffis
Nitroguanidine reduction product
Is the stuff floating in the red liquor actually red or just the solution? I checked out Richter vol ...
16-12-2022 at 09:53
by: Boffis
Nitroguanidine reduction product
Under rather specific conditions with conventional reducing agents it is possible to reduce some nit ...
16-12-2022 at 05:50
by: Boffis
Analogs of haloform reaction?
@Falvin, if you want to get useful responses to a post you need to put a bit more effort into your p ...
14-12-2022 at 05:11
by: Boffis
Caffeine: reducing the keto-groups to alkanes
If you check out libgen there are a series of books on heterocyclic compounds and there are at least ...
14-12-2022 at 00:30
by: Boffis
Preparation of chlorosulfonic acid derived protecting groups
I have a real hard-copy book on naphthalene chemistry. Throughout the book it describes the preparat ...
3-12-2022 at 13:45
by: Boffis
Hydrazine Hydrate turning yellow
You need to be more specific with you details! How does IPA (= isopropyl alcohol I presume) free bas ...
3-12-2022 at 04:03
by: Boffis
allyl alcohol
Has anyone thought about trying this reaction with higher poly-hydroxyalkanes and sugar alcohols suc ...
30-11-2022 at 03:32
by: Boffis
Bromination of 1,3 benzodioxole to 5-Bromo-1,3-benzodioxole?
Hi Pumikli, I think the difference in the numbering is due to the fact it is regarded as a benzo-het ...
29-11-2022 at 06:30
by: Boffis
haloform reaction - cinnamic acid from benzylideneacetone
Hi Fery et al. While I haven't tried this reaction on benzalacetone type substrates I have recently ...
27-11-2022 at 12:10
by: Boffis
1,2,3,4-tetrahydrocarbazole
[rquote=678466&tid=159074&author=Fery]Hi Boffis, the experiment was for the beauty of chemis ...
21-11-2022 at 11:57
by: Boffis
2,2'-Bipyridine synthesis
Hi Diachrymnic, nice write up once again and I like your make-shift retort from copper pipe and fitt ...
21-11-2022 at 11:48
by: Boffis
Pyrazine Synthesis?
Diachrynic; nice write-up; its a pity about the yield. I may have a go at this synthesis myself when ...
21-11-2022 at 11:02
by: Boffis
Formic Acid Dehydration
Hi Chemist1357; I had this problem once and did some research into upgrading my formic acid and I fo ...
21-11-2022 at 09:50
by: Boffis
Interesting route to 4-methoxyphenol
@ tyro; nice work and an excellent write-up. There are echoes of this method in benignium's write-up ...
13-11-2022 at 13:39
by: Boffis
1,2,3,4-tetrahydrocarbazole
@ Fery; nice write-up once again. Any particular reason why you chose tetrahydrocarbazole as your ta ...
13-11-2022 at 13:38
by: Boffis
Synthesis of malonic acid
I agree with you kmno4 about the mp of the diacetic acid and I find this route rather implausible to ...
12-11-2022 at 07:46
by: Boffis
Synthesis of malonic acid
Hi kmno4, thankyou for the paper, I haven't seen this one before but I have looked at, and indeed tr ...
11-11-2022 at 12:15
by: Boffis
Removing graphite from glass frit filter
Have you tried reversing the flow of water through the frit. If this and Piranha solution don't move ...
11-11-2022 at 09:36
by: Boffis
Synthesis of malonic acid
Well, carried out a Mp test on my white crystals and got a figure of 93-93.5 C; the compound melted ...
9-11-2022 at 11:18
by: Boffis
Phosphorus pentachloride from phosphides
Where can you get cyanuric chloride?
8-11-2022 at 14:58
by: Boffis
Synthesis of malonic acid
@ kmno4; Well I have something to report but I am not quite sure what!!

I ran a 20g batch of beta ...
8-11-2022 at 14:56
by: Boffis
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