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PET + ammonia. white powder
There's a whole thread on this somewhere on SM that followed from one members observasion that PET b ...
18-1-2021 at 05:59
by: Boffis
Preparation of Acetanilide
Very interesting Pumukli and another good write up.

Which reactions contained the "anhydride"? Is ...
18-1-2021 at 01:40
by: Boffis
furfural
I have now run two attempts at Fenton oxidation of xylitol (Fe2+ catalyzed H2O2 oxidation) and then ...
16-1-2021 at 13:02
by: Boffis
An attempt at making Phorone
I hate to say this but I think that chinese patent is garbage. Just look at how much energy is relea ...
16-1-2021 at 10:53
by: Boffis
Why are sulfuric acid ratios the same for nitrate salt and nitric acid?
They aren't and you can't generalize aout such things but you are probably looking at ill designed a ...
16-1-2021 at 06:37
by: Boffis
C.T.M.T.N.A (R-salt)
Regarding the stability of this compound, I have just come across the jar of recrystallised material ...
16-1-2021 at 04:14
by: Boffis
An attempt at making Phorone
Hi EverythingAl2O3, I've been following your experimental endeavors with interest as I have been con ...
15-1-2021 at 15:27
by: Boffis
mononitrotoluenes (nitration of toluene)
Ahh. That is interesting. I presume you recovered your toluene from some solvent type material. I wo ...
15-1-2021 at 12:13
by: Boffis
mononitrotoluenes (nitration of toluene)
Ahh. That is interesting. I presume you recovered your toluene from some solvent type material. I wo ...
15-1-2021 at 11:54
by: Boffis
mononitrotoluenes (nitration of toluene)
Hi Fery, another nice write up. I haven't tried this preparation for over 30 years but I don't remem ...
13-1-2021 at 13:59
by: Boffis
1,4-naphtoquinone by naphtalene oxidation with dichromate
Interesting work Fery, and a nice write-up even if not 100% successful! I had been thinking about tr ...
13-1-2021 at 10:39
by: Boffis
furfural
While emptying out the flask from one of the reaction I found these beautiful hopper salt crystals i ...
11-1-2021 at 15:11
by: Boffis
Mercury selenite
Well, this is what my samples look like: mercury selenite, tellurite and tellurate,

[file]85977[ ...
11-1-2021 at 13:16
by: Boffis
Fenton type oxidation
Tried this again with 25g of xylitol, 220ml of 3% H2O2 that's a higher ratio of H2O2 to xylitol than ...
11-1-2021 at 12:20
by: Boffis
Friedel-Crafts acylation of anilides
Thanks njl, that is interesting!
11-1-2021 at 12:15
by: Boffis
Friedel-Crafts acylation of anilides
That is interesting, if it works with p-chloroacetyl chloride I can see no reason why it should not ...
11-1-2021 at 07:55
by: Boffis
Mercury selenite
Hi Vano, Many years ago I acquired a collection of mercury compounds from a guy who had worked on th ...
11-1-2021 at 06:59
by: Boffis
Fenton type oxidation
Thanks for the information Sedit!!

I have tried Fenton's type oxidations before and had variable ...
10-1-2021 at 04:14
by: Boffis
Friedel-Crafts acylation of anilides
Tricky :D, As we say "the Devil is in the detail"

If you mix the acetanilide with the acetylation ...
9-1-2021 at 15:39
by: Boffis
Friedel-Crafts acylation of anilides
Hi Pumukli, take a look at these two papers:

Chattaway, Proc. Chem. Soc. 1902, p173 and 1903, p12 ...
9-1-2021 at 12:58
by: Boffis
Fenton type oxidation
Does anyone have any actual experience of the se of Fenton's reagent in oxidation in organic chemist ...
9-1-2021 at 02:18
by: Boffis
Successful Synthesis of 1-Amino-3-nitroguanidine Nitrate
Did you check out this thread?:

http://www.sciencemadness.org/talk/viewthread.php?tid=83736
8-1-2021 at 14:46
by: Boffis
Things to do with Ethyl Formate
[rquote=652755&tid=156492&author=Pumukli]Why not combine the two? Alkaline sulfide precipita ...
8-1-2021 at 09:04
by: Boffis
Things to do with Ethyl Formate
I have now isolated over 60g of copper triazole sulphate, its composition is as yet unknown but look ...
8-1-2021 at 03:35
by: Boffis
p-Nitroso-dimethylaniline
Hi Pumukli, I had a go at recrystallising some of my least pure p-nitrosodimethylaniline from pet et ...
7-1-2021 at 14:39
by: Boffis
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