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worst stench
I had the (dis)pleasure of being involved in the manufacture of a whole series of isonitriles, ethyl ...
3-2-2023 at 23:15
by: BromicAcid
Phosphoric Acid dry distillation
There's a thread kicking around somewhere on the forum on pyro/poly phosphoric acids. In another li ...
1-2-2023 at 15:22
by: BromicAcid
The oldershaw column she told you not to worry about
How many plates? 30-40?
27-1-2023 at 15:31
by: BromicAcid
Free Stuff! To Wisconsin member in good standing
Picked up! Thanks for the space!
24-1-2023 at 14:25
by: BromicAcid
Safely quenching sodium?
Took about a week of refluxing, when I was cleaning the flask I noticed that there was waviness in t ...
1-1-2023 at 20:11
by: BromicAcid
Safely quenching sodium?
I had a reaction once where I had to prepare sodium isopropoxide. I thought it would be a simple ma ...
1-1-2023 at 10:52
by: BromicAcid
Keep the temperature
Put some marks on it when you figure out boiling points. You'll get to know your dial with practice ...
21-12-2022 at 19:57
by: BromicAcid
Wharever happened to... all of the images!
Gosh, I remember when I first started I had to login to the FTP to upload my images. I'm assuming t ...
8-12-2022 at 16:14
by: BromicAcid
can hydrogen be stored under low pressure for hydrogenation reactions?
Yeah, be very careful putting hydrogen into units not intended for it, hydrogen embrittlement is a r ...
1-12-2022 at 14:13
by: BromicAcid
New powerful Energetics based on Boron - Nitrogen reaction
At one time I wanted to make trinitroborazine. There was literature precedent for making triazobora ...
22-11-2022 at 19:40
by: BromicAcid
Ferrates vs. perxenates
Simple but probably effective. This was the exact post I was talking about though:

http://www.sc ...
10-10-2022 at 04:02
by: BromicAcid
Ferrates vs. perxenates
One of the Inorganic Syn volumes basically had a hardware store list to make a fluorine generator. ...
9-10-2022 at 12:17
by: BromicAcid
On The Synthesis of Nicotine
Speaking of the price difference between natural and manufactured. We made a synthetic cholesterol ...
6-10-2022 at 17:09
by: BromicAcid
Does triiodoethanol exist?
Usually simpler compounds like that have all been synthesized centuries ago. It's easy to think tha ...
29-9-2022 at 14:58
by: BromicAcid
Does the island of stability really exist ?
Question is "Does the island of stability actually exist?"

Consensus from people much smarter tha ...
16-9-2022 at 13:32
by: BromicAcid
Does the island of stability really exist ?
metalresearcher, the whole point of the island of stability is that theoretical modeling does indica ...
15-9-2022 at 17:14
by: BromicAcid
Does the island of stability really exist ?
It's a lot different making useful quantities of an element with a half-life of fractions of a secon ...
14-9-2022 at 13:28
by: BromicAcid
Does the island of stability really exist ?
I think it's there and some interesting elements are going to come from it. Nuclear physicists have ...
14-9-2022 at 03:29
by: BromicAcid
Don't ballmill magnesium.
On the one hand, magnesium can form a nitride so finely divided magnesium could potentially still ha ...
6-9-2022 at 13:47
by: BromicAcid
What is my best bet at diggesting a mix of all elements that can form acetates at once, as I would do with nitric acid?
I used to mainline 120V AC through flatware from the dollar store spaced about 5 inches apart in con ...
5-9-2022 at 18:43
by: BromicAcid
Osmium chemistry
From my recollection the big issue is damage to the eye tissues due to exposure to the tetroxide. J ...
5-9-2022 at 11:44
by: BromicAcid
Distillation tails at lower temperature. (Damn. I thought I fully understood distillation.)
Of course 185°C is around the temperature where dicyclopentadiene starts to really crack giving cyc ...
4-9-2022 at 05:13
by: BromicAcid
Distillation tails at lower temperature. (Damn. I thought I fully understood distillation.)
My guess would be you finished distilling off the volatile components in that temperature range. Yo ...
3-9-2022 at 04:24
by: BromicAcid
Purifying NaOH from drain opener
Might be worth investigating but I remember the procedure for making sodium peroxide hydrate where t ...
28-8-2022 at 13:12
by: BromicAcid
Quick and Efficient PTFE Testing
I remember one arm of our company using hydrophilic PTFE tubing, it definitely had a different feel ...
27-8-2022 at 10:18
by: BromicAcid
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