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Do not buy from laboyglass.com
I have always ordered from Deschem and the quality seems great to be honest.
10-1-2021 at 07:03
by: ChemichaelRXN
Reductions of Nitro groups with Zn and acid
If the reaction works ok, you can extract it with chloroform 1.49g/ml instead of toluene 0.865g/ml, ...
3-1-2021 at 23:09
by: ChemichaelRXN
New organic chemistry youtube video: Making isobutyl bromide
No problem, I messaged you.

Also I tried the sulfurol and HBr reaction in the past, but what I go ...
25-12-2020 at 12:33
by: ChemichaelRXN
New organic chemistry youtube video: Making isobutyl bromide
Nice work! If you want some sulfurol for free to halogenate, let me know. You can convert it to “b ...
25-12-2020 at 05:49
by: ChemichaelRXN
Organometallic liquid gold luster
Different subject a bit, but have you ever melted copper and silver together and make a ring. I made ...
23-12-2020 at 15:46
by: ChemichaelRXN
Formaldehyde bisulfite adduct preparation
Yea maybe rotovap half of the solution not crystallizing or add NaCl to make a brine to reduce the s ...
20-12-2020 at 06:59
by: ChemichaelRXN
AlCl3 is an alternative to SOCl2
Thanks for talking about it for me to get one. Not too familiar with titanium hydride, maybe sodium ...
15-12-2020 at 15:49
by: ChemichaelRXN
AlCl3 is an alternative to SOCl2
Mine are 0.6Mpa or 87psi. I guess a hot water bath would be safe enough.

I just bought one too; H ...
14-12-2020 at 16:35
by: ChemichaelRXN
AlCl3 is an alternative to SOCl2
Here is some more info. on TCCA reactions; https://www.organic-chemistry.org/chemicals/oxidations/tr ...
14-12-2020 at 14:49
by: ChemichaelRXN
2,2,7,7-tetramethyloxepane
Yea, it might just work. I recall hearing anything less than the 1,4-dibromobutane would just break ...
13-12-2020 at 09:43
by: ChemichaelRXN
2,2,7,7-tetramethyloxepane
Hello,

Has anyone ever performed a Grignard reaction where you are reacting two halogen groups wi ...
13-12-2020 at 06:59
by: ChemichaelRXN
Benzoyl chloride from benzoic acid
Ok, great, thank you for the info., I appreciate it!
9-12-2020 at 13:04
by: ChemichaelRXN
I need help finding the very bane of roaches existence...
You will have to experiment. You’d probably need like ten of these around the house in cabinets an ...
9-12-2020 at 10:58
by: ChemichaelRXN
Benzoyl chloride from benzoic acid
Here is knitting for you. Those who dare to think outside of the box always seem to get ridiculed.
...
9-12-2020 at 09:21
by: ChemichaelRXN
Benzoyl chloride from benzoic acid
You can distill benzoyl chloride.

I was talking about SnO2. I must have been misinformed about th ...
9-12-2020 at 09:06
by: ChemichaelRXN
Benzoyl chloride from benzoic acid
I am a laid back person, so you can just see how you sound...

Germanium, tin and lead oxides
For ...
9-12-2020 at 08:03
by: ChemichaelRXN
Benzoyl chloride from benzoic acid
What is your experience on this reaction?

With good ventilation, I was wondering what would occur ...
8-12-2020 at 15:56
by: ChemichaelRXN
Preparation of dimethylamine
What if you use methyl iodide in the right amount to ammonia and keep the product under 7C to have i ...
30-10-2020 at 04:19
by: ChemichaelRXN
Real sassafras oil from roots!
Thanks, I appreciate it. I strive to do more, but I am usually in a state of feeling miserable from ...
29-10-2020 at 09:16
by: ChemichaelRXN
Real sassafras oil from roots!
I dont do anything with anything scheduled, but if you were to get every last drop, Id extract the s ...
28-10-2020 at 22:09
by: ChemichaelRXN
Preparation of Red Selenium Gone Wrong
Thanks for the info. I notice just a slight sublimated amount in the air makes me nauseous. I must h ...
22-10-2020 at 07:31
by: ChemichaelRXN
Preparation of Red Selenium Gone Wrong
A little off topic, but have you noticed that selenous acid in ppm in the air makes you nauseous? I ...
22-10-2020 at 00:55
by: ChemichaelRXN
Real sassafras oil from roots!
MDMA is great, but it isnt worth risking your life over. There are many other compounds out there. U ...
21-10-2020 at 08:12
by: ChemichaelRXN
Ferric chloride and HCl halogenation of hydroxyl groups
I’ll think about it and may try it out. I was thinking of gassing the sulfurol with HCl too, but t ...
20-10-2020 at 07:21
by: ChemichaelRXN
Ferric chloride and HCl halogenation of hydroxyl groups
How about using Conc. HCl with addition of H2SO4? Reminds me of a nitration, but may help with repla ...
19-10-2020 at 11:25
by: ChemichaelRXN
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