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Evaporating methanol vaccum
So I have some P2NP that is damp from recrystallisation from methanol. The product is kind of sensit ...
25-12-2022 at 04:08
by: DocX
Great success
Another fruitful exchange of needed and hard-to get chemicals from this excellent and trustworthy se ...
10-12-2022 at 14:33
by: DocX
Drying ammonium acetate?
[rquote=678819&tid=159101&author=Rainwater]the search button at the top works great if you s ...
30-11-2022 at 08:33
by: DocX
Drying ammonium acetate?
So I just bought a small amount of ammonium acetate and DAMN is it hygroscopic. Its almost a slurry ...
23-11-2022 at 07:51
by: DocX
Preparation of Thalidomide
No, I haven't gotten round to it yet. I'm waiting for lab grade reagents to try and exclude all the ...
18-11-2022 at 12:21
by: DocX
TheVespiary downed?
and back again.
Up and down like the Assyrian empire!

Which brings me to thinking I should down ...
9-11-2022 at 13:36
by: DocX
Magnetic stirrer/hot plate $30
What would the shipping be to Northern Europe I wonder? Also, what are the dimensions and wattage of ...
9-11-2022 at 06:36
by: DocX
Any reaction between AL and ETN?
[rquote=677950&tid=159025&author=BlackPowderBoy] To give context, I need to make a detonator ...
28-10-2022 at 07:25
by: DocX
TheVespiary downed?
Him?
26-10-2022 at 07:09
by: DocX
Pyridine goo, what to do
[rquote=677882&tid=159014&author=Loptr]What were you trying to make with the original mixtur ...
24-10-2022 at 21:50
by: DocX
Pyridine goo, what to do
I was evaporating water from a mixture of pyridine, glutamic acid, phtalic anhydride and some DMF, a ...
24-10-2022 at 10:37
by: DocX
A foray into phenethylamines of the Shulgin kind
This is extremely impressive. Following your progress, I would probably have given up at least four ...
24-10-2022 at 10:04
by: DocX
Fractional freezing to GAA
I actually left this project. Gave up and ordered some GAA from the ultraprofessional Chemship1978. ...
24-10-2022 at 10:02
by: DocX
Everyday Chemistry (provisional)
[rquote=677543&tid=84298&author=DraconicAcid]
You don't think pyridine is that bad? Really ...
24-10-2022 at 09:32
by: DocX
Preparation of Thalidomide
My take on the failure to produce a bioactive end product is that I'm actually looking at a crystal ...
24-10-2022 at 07:55
by: DocX
Vacuum filtration sucking fluid
Sorry, no picture, but the extra bit of tubing attached to the outlet of the Buchner did the trick. ...
23-10-2022 at 13:10
by: DocX
TheVespiary downed?
Immediately when I type in the adress in my browser I get
[b]"This account has been suspended. Con ...
23-10-2022 at 08:26
by: DocX
Preparation of Thalidomide
So finally I got around to do this.

I thought I'd combine the two methods in the write-ups above ...
22-10-2022 at 13:22
by: DocX
Vacuum filtration sucking fluid
[rquote=677690&tid=158993&author=Texium]Sounds like you’re using a lot more vacuum than yo ...
18-10-2022 at 20:18
by: DocX
Vacuum filtration sucking fluid
Well, SOMETHING makes fluid enter the vacuum hose. I'll try the extra tube thang (next time I'm doin ...
17-10-2022 at 07:26
by: DocX
Vacuum filtration sucking fluid
But maybe I could attach the hose to the exit tube from the Buchner funnel? And make it so the inflo ...
16-10-2022 at 21:14
by: DocX
Vacuum filtration sucking fluid
[rquote=677653&tid=158993&author=Tsjerk]Can you post a picture of your setup? This should be ...
16-10-2022 at 09:05
by: DocX
Vacuum filtration sucking fluid
So I'm using ny new vacuum pump to vacuum filter some newly synthesised lovely salts.
Problem is, ...
16-10-2022 at 04:22
by: DocX
OTC nitroethane source
[rquote=677300&tid=158925&author=SuperOxide][rquote=677295&tid=158925&author=DocX]I ...
4-10-2022 at 21:47
by: DocX
OTC nitroethane source
[rquote=677304&tid=158925&author=Organikum]I asked a little bit around and this in the pict ...
4-10-2022 at 02:08
by: DocX
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