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H2SO4 by the Lead Chamber Process - success

Yes, I just discover that SnCl4 needs to be in H2SO4 solution at 100*C in order to react ... and S ...
30-4-2014 at 04:17
by: DoctorZET
HCN by chloroform and ammonia in base
Agree, but only if you have access to a hexacyanoferrate salt (just like K3Fe(CN)6).
And, by the w ...
25-4-2014 at 07:21
by: DoctorZET
Small scale preparation of Stannic Chloride (SnCl4)
Yes, Blogfast25 is right :

Tin tetrachloride is almost a covalent compound, meanwhile the copper ...
25-4-2014 at 06:26
by: DoctorZET
HCN by chloroform and ammonia in base
Well ... it's very possible to get a "bang" if you mix in a baloon Cl2 and CH4 (remember that H2+Cl2 ...
23-4-2014 at 14:24
by: DoctorZET
Quick and easy source of H2O2?
I think that any mixture of H2O2 and water (up to 50% H2O2) can be distilled without problems, becau ...
23-4-2014 at 14:05
by: DoctorZET
Quick and easy source of H2O2?

[quote]
"In aqueous solutions
In aqueous solutions hydrogen peroxide differs from the pure mater ...
22-4-2014 at 12:47
by: DoctorZET
Quick and easy source of H2O2?
Arr ... at 120 *C, H2O2 has a half-life about 20-25 min ... and in a distillation tube, H2O2 and wat ...
22-4-2014 at 09:47
by: DoctorZET
Quick and easy source of H2O2?
I remember that if sodium oxide is heated up to 200-300*C in oxygen atmosphere, for 15-30 min ... wi ...
22-4-2014 at 08:32
by: DoctorZET
Small scale preparation of Stannic Chloride (SnCl4)
Well... I think about this reaction, because I know that when 2 salts are melted together, a reactio ...
22-4-2014 at 05:27
by: DoctorZET
HCN by chloroform and ammonia in base
You should not smell it too much... it's highly toxic , remember O_o ?

Now I think about next pro ...
18-4-2014 at 05:54
by: DoctorZET
Acetaldehyde synthesis
also you can try to make the silver mirror reaction using the glass wool in the solution of glucose/ ...
17-4-2014 at 13:46
by: DoctorZET
Acetaldehyde synthesis
And the Ag powder / Al2O3 powder can be easily spread in the glass wool:
Take a piece of glass wool ...
17-4-2014 at 13:40
by: DoctorZET
Acetaldehyde synthesis
And here is the another process:

17-4-2014 at 13:22
by: DoctorZET
Acetaldehyde synthesis
Here is a process of making acetaldehyde:
17-4-2014 at 09:55
by: DoctorZET
HCN by chloroform and ammonia in base
I think the best way to get HCN in a home-lab is the proces involving chloroform and ammonia... ;)
...
16-4-2014 at 14:49
by: DoctorZET
Small scale preparation of Stannic Chloride (SnCl4)
I think about a reaction:

SnCl4 (anhydrous, liquid)(excess) + 2CuSO4(anhydrous) --> Sn(SO4)2 ( ...
16-4-2014 at 14:10
by: DoctorZET
H2SO4 by the Lead Chamber Process - success
Remember the "Bordeaux mixture" ?
Everybody can go to a agricultural-shop (farm-shop) and buy some ...
16-4-2014 at 13:12
by: DoctorZET
Permanganates
Bubbling with CO2 a boiling solution of potassium manganate, should work :

3 K2MnO4 (aq) + 2 CO2 ...
16-4-2014 at 11:47
by: DoctorZET
Nitryl Chloride
the reaction between N2O4 and Cl2 should be catalised by a intense blue-UV light, because Cl ions ar ...
15-4-2014 at 04:51
by: DoctorZET
Nitric Acid and Silver Nitrate
Well, I'm sorry for the stains leaved on the wall of this forum ... but, over all, this is a place t ...
15-4-2014 at 04:19
by: DoctorZET
P2O5 and P4O10
I just tried first reaction and the P4 burns in N2O4 ... is like burning P4 in NO2 atmosphere ... no ...
15-4-2014 at 03:20
by: DoctorZET
P2O5 and P4O10
I think about next 2 reactions:

P4 (CCl4 solution ) + 5 N2O4 --(? ...heat/UV/pressure)--> 10 N ...
14-4-2014 at 11:51
by: DoctorZET
P2O5 and P4O10
well...there might be other ways to oxidate phosphorus...

here are 2 links for all who want to "c ...
14-4-2014 at 09:24
by: DoctorZET
Sulfuric Acid Production: Revisited
warning: in the first process water must not be present !
14-4-2014 at 02:34
by: DoctorZET
Sulfuric Acid Production: Revisited
I'm thinking about 2 methods:

first involves a tin process:

1)take some soldering alloy (Pb+S ...
14-4-2014 at 02:32
by: DoctorZET
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