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Sodium Nitroprusside Synthesis
I've got the dried crystals. The yield is approximately 30% which is a lot better than my first att ...
11-4-2019 at 10:24
by: Doped-Al2O3-fusion
Sodium Nitroprusside Synthesis
I performed two attempts at synthesizing sodium nitroprusside recently. My first attempt was mostly ...
11-4-2019 at 07:21
by: Doped-Al2O3-fusion
Amateur Chemistry now vs several decades ago
[rquote=602894&tid=95348&author=itsafineday][rquote=581916&tid=95348&author=Chemistr ...
5-3-2019 at 00:50
by: Doped-Al2O3-fusion
1-chloro-2-propanone (chloroacetone)
Sorry to resurrect an old thread, but I'm really glad I found it. I was trying to find out what sub ...
8-2-2019 at 15:16
by: Doped-Al2O3-fusion
Power Supply from Model Train Control
[rquote=582073&tid=128526&author=Abromination]I was planning on spending the day building a ...
23-1-2019 at 00:29
by: Doped-Al2O3-fusion
Hydrothermal Synthesis of Sulfides
Further experimental update.

This most recent experiment appears to be a failure in an attempt at ...
9-1-2019 at 10:06
by: Doped-Al2O3-fusion
Corundum From Thermite Slag
[rquote=571798&tid=118594&author=MineMan]Super interesting! Have you tried making diamonds ...
31-12-2018 at 15:21
by: Doped-Al2O3-fusion
Corundum From Thermite Slag
Here is a gallery I made a while back with some of my first experimental samples of flame fusion bas ...
27-12-2018 at 22:44
by: Doped-Al2O3-fusion
Corundum From Thermite Slag
These crystals should actually be present in normal thermite as well, but it really depends on the b ...
27-12-2018 at 22:31
by: Doped-Al2O3-fusion
Corundum From Thermite Slag
[rquote=570250&tid=118594&author=MrHomeScientist]Nice! What was the composition of your ther ...
27-12-2018 at 22:17
by: Doped-Al2O3-fusion
Corundum From Thermite Slag
Since I've not been able to complete my Verneuil furnace yet, I've been playing with thermite seeded ...
27-12-2018 at 08:48
by: Doped-Al2O3-fusion
In praise of Deschem
I've got most of my glassware from Deschem and I've got nothing but praise for them. I've had items ...
15-11-2018 at 09:09
by: Doped-Al2O3-fusion
Hydrothermal Synthesis of Sulfides
I've refined my Batch05 of FeS2 and found some very interesting and exciting results. I found actua ...
5-10-2018 at 08:42
by: Doped-Al2O3-fusion
Hydrothermal Synthesis of Sulfides
[rquote]Ah sorry I misread/misunderstood your sentence, my bad:P[/rquote]

No worries. I do that ...
2-10-2018 at 13:14
by: Doped-Al2O3-fusion
Hydrothermal Synthesis of Sulfides
[rquote=540025&tid=85360&author=fusso][rquote=540018&tid=85360&author=Doped-Al2O3-fu ...
2-10-2018 at 11:46
by: Doped-Al2O3-fusion
Hydrothermal Synthesis of Sulfides
Here are my batch #5 results. I'm debating uploading a video to my YouTube channel upon first inves ...
2-10-2018 at 10:23
by: Doped-Al2O3-fusion
Hydrothermal Synthesis of Sulfides
Here are some pictures from my last batch (batch #4). This is probably the reason you don't see oth ...
27-9-2018 at 14:20
by: Doped-Al2O3-fusion
Preparation of elemental phosphorus
[rquote=538862&tid=65&author=Herr Haber]Has anyone during these experiments gotten white P t ...
27-9-2018 at 11:25
by: Doped-Al2O3-fusion
Preparation of elemental phosphorus
[rquote=538765&tid=65&author=BromicAcid]In your previous post you mention an energetic react ...
27-9-2018 at 11:21
by: Doped-Al2O3-fusion
Preparation of elemental phosphorus
I've learned quite a bit more since my last post just a couple weeks ago on this thread. I've succe ...
26-9-2018 at 12:53
by: Doped-Al2O3-fusion
Preparation of elemental phosphorus
[rquote=493792&tid=65&author=Magpie]yes, I believe the intimate contact provided by molten a ...
13-9-2018 at 13:01
by: Doped-Al2O3-fusion
Sodium Thiosulfate Synthesis and Purification
...I may have some incorrect logic in my understanding of a reaction, so I'm glad others in the comm ...
12-9-2018 at 16:51
by: Doped-Al2O3-fusion
Sodium Thiosulfate Synthesis and Purification
[rquote=534111&tid=88178&author=S.C. Wack][rquote=534078&tid=88178&author=Doped-Al2O ...
12-9-2018 at 16:46
by: Doped-Al2O3-fusion
Hydrothermal Synthesis of Sulfides
Here's an update on the FeS2 synthesis. The picture of the two black piles is of the 1st and 2nd ba ...
10-9-2018 at 08:06
by: Doped-Al2O3-fusion
Hydrothermal Synthesis of Sulfides
I was going through my first batch of synthesized FeS2 which I hadn't found any indication of any vi ...
9-9-2018 at 10:33
by: Doped-Al2O3-fusion
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