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I have been thinking about a homebrew system for controlled potential/current electrochemical work. ...
21-7-2009 at 12:03
by: Dr.3vil
Induction heating
Fantastic Job, I was just about to link your story from hackaday too. Im really impressed and would ...
24-6-2009 at 18:26
by: Dr.3vil
From personal experience while trying to quit smoking, the patch gives you some really odd dreams. I ...
17-6-2009 at 14:49
by: Dr.3vil
Home Made TLC plates
I don't have any experience with spin coating but I accept your reasoning. Looking back DJF90 mentio ...
14-6-2009 at 16:10
by: Dr.3vil
Home Made TLC plates
I think Watson is right on with the physical properties of the suspension. the quality and consisten ...
14-6-2009 at 12:06
by: Dr.3vil
Home Made TLC plates
hmm, good point on the UV indicator. I have a set of lab quality silica plates with the florescent i ...
13-6-2009 at 07:31
by: Dr.3vil
Home Made TLC plates
TLC plates are expensive, so, make your own.
giving credit where credit is due, original project b ...
11-6-2009 at 08:10
by: Dr.3vil
Book Sanning Process a la Sauron
a non-destructive book scanner made from trash. ...
9-6-2009 at 14:26
by: Dr.3vil
Home chemist raided in MA, lab seized.
[quote][i]Originally posted by BromicAcid[/i]
Dr.3vil, 1500 is just a number and it tells us nothin ...
13-8-2008 at 19:34
by: Dr.3vil
Repairing Infrared Spectrophotometers
hmmm, I'm in the same boat. I have Spectronic 2000 UV/VIS that is no longer operational. Right now i ...
13-8-2008 at 19:14
by: Dr.3vil
clean up your mess
"Firefighters found more than 1,500 vials, jars, cans, bottles and boxes in the basement Tuesday aft ...
13-8-2008 at 18:43
by: Dr.3vil
electrochemical benzaldehyde
I mentioned this in a prior post (kolbe) but figured it needed to be here since the scope of the art ...
30-7-2008 at 14:31
by: Dr.3vil
benzoic acid
From "electrochemistry oforganic compounds"
walther Lob

Benzoic Acid.—Benzoic acid and i ...
30-7-2008 at 08:41
by: Dr.3vil
Success with jade
I treated a jade plant with 500+PPM (i dont recall the exact concentration however it was only treat ...
30-6-2008 at 06:02
by: Dr.3vil
Cu/SiO2 a cheap versatil hydrogenation catalyst?
Nice work! I am looking forward to seeing the writeup for the reduction of the catalyst by H2. So fa ...
22-6-2008 at 13:35
by: Dr.3vil
silicon oil/distilling
so basically the idea here is to add a higher boiling point liquid in order to force out the product ...
29-4-2007 at 13:27
by: Dr.3vil
ozone generator for ozonolysis
would something like the device linked below be suitable for the production of ozone used in ozonoly ...
18-4-2007 at 15:29
by: Dr.3vil
Anodizing Aluminum

this guy sells anodizing kits for home use but hi ...
13-4-2007 at 15:28
by: Dr.3vil
KMnO4 + EtOH + NaOH ---> Sodium acetate --> Acetic acid
I need some help with the oxidation of ethanol in the presence of KMnO4 and NaOH to yield sodium ace ...
10-4-2007 at 18:09
by: Dr.3vil
how about Cl2 bubbled through NaOH and acetone?

"Yeah, I read about that on that Rhodium site bu ...
2-4-2007 at 05:25
by: Dr.3vil
ugh....we have degraded to a point of living in fear. (that means they won) i suggest the following ...
1-4-2007 at 08:06
by: Dr.3vil
Oxidation of ethanol
most electrochemical oxidations of EtOH involve Pt/Ru/C catalysts and belong to direct methanol fuel ...
29-3-2007 at 06:29
by: Dr.3vil
Paranoia while buying reagents?
[quote][i]Originally posted by evil_lurker[/i]
I've pretty much given up on OTC stuff... way to pla ...
23-3-2007 at 12:09
by: Dr.3vil
Paranoia while buying reagents?
eh, it sucks that meth has ruined such a nice hobby. I guess it all depends on where you live. If lo ...
23-3-2007 at 10:01
by: Dr.3vil
reaction conditions - chloroform from Cl2
rather then start a new thread....


C3H6O + Cl2 in base => chloroform + carboxcyli ...
16-3-2007 at 15:31
by: Dr.3vil
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