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Make Potassium (from versuchschemie.de)
I think it's a fairly simple slow distillation from acidified auto anitfreeze....only troublesome bi ...
1-5-2011 at 11:16
by: Eclectic
Make Potassium (from versuchschemie.de)
It should be easy enough to distill dioxane from Glycol antifreeze with a little sulfuric acid added ...
1-5-2011 at 09:42
by: Eclectic
Large scale vacuum distillation
Try dipropylene glycol as your heating bath fluid and a capillary tube or stainless steel bubbling s ...
1-5-2011 at 03:48
by: Eclectic
Synthesis of longer chain tertiary alcohols

Same here. Now I'm REALLY determined to make terpin hydrate.
I'll tap a pine tree and use nitric ...
19-4-2011 at 03:05
by: Eclectic
Has anyone made sodamide?
If you have good ventilation, delivering liquid anhydrous ammonia from tank bottom directly into a ...
16-4-2011 at 03:25
by: Eclectic
monopropellant project
Have you looked at N20 injected into cast solid fuel combustion chamber?
You wanted throttleable, y ...
14-4-2011 at 04:31
by: Eclectic
Synthesis of longer chain tertiary alcohols
Well, hell, Blogfast, if all you want is to buy it, I don't even want to know you :-D (reference to ...
11-4-2011 at 14:32
by: Eclectic
Synthesis of longer chain tertiary alcohols
You may be able to make it from hexachloroethane by refluxing with 25% H2SO4, and maybe some iron.
...
11-4-2011 at 06:59
by: Eclectic
Synthesis of longer chain tertiary alcohols
Careful with the Trichloroacetic...it causes liver tumors. But I'm tempted by that route also. It' ...
10-4-2011 at 13:23
by: Eclectic
Decontaminating HDPE
Try kerosene?
8-4-2011 at 08:51
by: Eclectic
Synthesis of longer chain tertiary alcohols
http://www.sciencemadness.org/talk/viewthread.php?tid=15455&goto=search&pid=206237

Terpin ...
8-4-2011 at 07:05
by: Eclectic
oxidizing limonene to carvone/carveol
http://pubs.acs.org/doi/abs/10.1021/ed057p741

Actual PDF would be appreciated.
7-4-2011 at 08:27
by: Eclectic
zinc-iron double oxide catalyst
I made some by coprecipitating from solution of the sulfate salts and calcining the washed precipita ...
7-4-2011 at 04:58
by: Eclectic
Synthesis of longer chain tertiary alcohols
I've found many references that indicate that both limonene and pinene will add water to form terpin ...
3-4-2011 at 07:57
by: Eclectic
Synthesis of Oleic Acid from Olive Oil
You might get good results with the fractionation if a little transesterification catalyst is added, ...
1-4-2011 at 07:21
by: Eclectic
Synthesis of longer chain tertiary alcohols
"Citrusy" sounds like you are making limonene. Terpineol should smell like lilac or hyacynth. I'm ...
1-4-2011 at 07:18
by: Eclectic
Hydrazine
Has anyone tried this with ice cold NaOH saturated solution and TCCA? Or making a concentrated NaOC ...
14-3-2011 at 07:21
by: Eclectic
Storage of pressurized liquid SO2 in plastic containers
I found a old patent or reference in Muspratt or the like from late 1800's where they used pumice st ...
14-3-2011 at 07:12
by: Eclectic
ClO2 from HCl + NaClO2 ... for medical purposes
A safer method might be to react NaClO3 with oxalic acid and make a saturated solution of ClO2 in wa ...
8-3-2011 at 09:01
by: Eclectic
Dystopian, Kafkaesque Nightmare???
Try Google Mail?
5-3-2011 at 09:47
by: Eclectic
triacetin synthesis
It boggles the mind how many times Wikipedia has had this phrase blindly copied:
Triacetin is also ...
5-3-2011 at 05:01
by: Eclectic
Synthesis of longer chain tertiary alcohols
That's from pinene though, with a strained ring. In
USA, pine turpentine is very cheap, and might ...
4-3-2011 at 10:01
by: Eclectic
Synthesis of longer chain tertiary alcohols
Could someone with a reflux/distillation setup try refluxing equal parts turpentine and glacial acet ...
3-3-2011 at 07:51
by: Eclectic
concentration Hydrogen fluoride gas
Seems like it would be simpler making your HF and then dealing with mixing to a known low concentrat ...
2-3-2011 at 05:04
by: Eclectic
Storage of pressurized liquid SO2 in plastic containers
GC, have you tried to find any catalysts for the H2SO4 + S8 reaction? Copper, iron, vanadium? We h ...
1-3-2011 at 02:07
by: Eclectic
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