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NaBH4 now on DEA Special Surveillance List
[rquote=688451&tid=159954&author=Texium]Most of “the chemistry world” doesn’t buy sodi ...
9-11-2023 at 09:28
by: German
NaBH4 now on DEA Special Surveillance List
https://www.dea.gov/stories/2023/2023-10/2023-10-30/dea-adds-precursor-chemicals-used-make-illicit-f ...
8-11-2023 at 19:20
by: German
Do I retain stereochemistry, alcohol>tosylate>halide?
I know I retain stereo-chemistry going from alcohol to tosylate. And I know I retain stereo-chemistr ...
4-8-2023 at 21:39
by: German
Got a weird result treating an alkyl azido with stannous chloride
So I treated an alkyl azido group with stannous chloride expecting to get the amine. But based on th ...
6-4-2023 at 15:00
by: German
TheVespiary downed?
Vesp (Cameron) seems to have been uninterested in the forum for the last couple years. There have b ...
29-10-2022 at 15:39
by: German
MW difference between hydrazine and hydrazone???
So I have a hydrazine group on my molecule and I wanted to turn it into a hydrazone so I boiled in s ...
9-6-2022 at 16:22
by: German
Hydrazine to Hydrazone question... please and thank you
[rquote=672946&tid=158549&author=njl]Do you mean oxidizing your existing alkyl hydrazine int ...
20-4-2022 at 09:20
by: German
Hydrazine to Hydrazone question... please and thank you
Could someone help me clear up my confusion? I have a hydrazine group on a molecule and I thought I ...
19-4-2022 at 16:26
by: German
HELP! Tiny differences in MW??? 253.33 vs 253.44
^^^^ Well that answers that. Thank you.
9-2-2022 at 21:15
by: German
HELP! Tiny differences in MW??? 253.33 vs 253.44
I was with you until I thought about it.

The cleaner procedure that gives me the slightly off and ...
9-2-2022 at 19:47
by: German
HELP! Tiny differences in MW??? 253.33 vs 253.44
So I am doing two different procedures to get to target compound 253.33. The first procedure uses a ...
9-2-2022 at 18:19
by: German
How sensitive is an imine to hydrolysis to an amine?
^^^^ Hey thanks. That paper gave me my answer. They actually converted back to the amine during work ...
1-6-2021 at 20:20
by: German
How sensitive is an imine to hydrolysis to an amine?
I have a molecule with a primary amine and a secondary amine. I want to turn the primary into an ami ...
1-6-2021 at 00:14
by: German
What acid is this?
Thank you very much
31-5-2021 at 23:55
by: German
What acid is this?
Sorry for the stupid question.
31-5-2021 at 23:32
by: German
Tosylate to Alkyl Azide reference please
^^^ Thank you very much.
13-4-2021 at 10:30
by: German
Tosylate to Alkyl Azide reference please
Yeah I saw that. There was only one for tosylates to alkl azide and it required a microwave. I've ne ...
12-4-2021 at 17:02
by: German
Tosylate to Alkyl Azide reference please
I planned on performing the fairly common substitution of tosylate to alkyl azide with sodium azide, ...
12-4-2021 at 12:07
by: German
Simplest "power solvent" synthesis?
[rquote=637851&tid=155543&author=Texium (zts16)]I second the suggestion of finding DCM. If y ...
10-6-2020 at 18:47
by: German
Sodium cyanide dissolved in water... anyone with experience??
I actually have tried for the last 2 months to avoid having to use cyanogen bromide. I have been try ...
10-6-2020 at 18:15
by: German
Sodium cyanide dissolved in water... anyone with experience??
[rquote=638073&tid=155560&author=Methyl.Magic]You are making cyanogen bromide and are afrain ...
10-6-2020 at 18:00
by: German
Sodium cyanide dissolved in water... anyone with experience??
This site actually has nice pictures to go with the standard synthesis listed above:

hXXps://thos ...
10-6-2020 at 17:47
by: German
Sodium cyanide dissolved in water... anyone with experience??
[rquote=638068&tid=155560&author=Methyl.Magic]

Why do you need water for BrCN ? BEcause i ...
10-6-2020 at 17:44
by: German
Sodium cyanide dissolved in water... anyone with experience??
I need to prepare some cyanogen bromide and the preparation calls for dissolving sodium cyanide in a ...
10-6-2020 at 17:15
by: German
Need help with a workup after a cleavage
EDIT: nevermind

[Edited on 7-4-2020 by German]
6-4-2020 at 15:46
by: German
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