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Whats the best way to obtain Sodium Bisulfite NaHSO3?
NaHSO3 can be prepared by burning sulphur in a can, sucking the SO2 into Na2CO3 solution in a wash b ...
2-6-2019 at 13:31
by: Jimmymajesty
Catalytic Converter PGM Recovery
I have <0.3wt% H2PdCl6 in AlCl3/Hcl pH~0.1 solution. I wanted to recover the Pd from a catalytic ...
2-6-2019 at 13:20
by: Jimmymajesty
The Short Questions Thread (4)
I did not add one thing to the story which is important to me, but for you it might be just a subjec ...
27-4-2017 at 13:45
by: Jimmymajesty
The Short Questions Thread (4)
Hi folks! I bought a memory foam mattress but after a week I had to get rid of it, I could not bear ...
26-4-2017 at 13:55
by: Jimmymajesty
Nitromethane, nitroethane, nitropropane synthesis via industrial route
Hey, thanks. I like the difficult ones because they send you on a learning trajectory, honestly I am ...
3-4-2016 at 03:48
by: Jimmymajesty
Nitromethane, nitroethane, nitropropane synthesis via industrial route
Hi, I made ~1ml nitroparaffins today.

I used ~80% white fuming NA. Set the temp just below its bo ...
28-3-2016 at 11:36
by: Jimmymajesty
toluene --> benzaldehyde
I have other ideas that I want to try out like, oxidizing the toluene with NO2 I just have to take a ...
21-3-2016 at 13:53
by: Jimmymajesty
toluene --> benzaldehyde
So... I also tried out copper plated kanthal wire and manganin as the heating element. Chunks of die ...
13-3-2016 at 16:50
by: Jimmymajesty
toluene --> benzaldehyde
Hi,

I gave it a decent try today. The toluene vapors went through a column which provided some de ...
12-3-2016 at 10:23
by: Jimmymajesty
toluene --> benzaldehyde
After the run, I let everyting cool, then take out 5ml yellow toluene, shook with 25ml water, then I ...
31-1-2016 at 13:42
by: Jimmymajesty
toluene --> benzaldehyde
blogfast you are right, the O2 concentration in the reactor is very low. 10ml of air to 3-5 drop of ...
30-1-2016 at 11:13
by: Jimmymajesty
toluene --> benzaldehyde
So... Toluene boils and it goes up in 1m long glass tube, at half way up is a thermometer to monitor ...
30-1-2016 at 07:51
by: Jimmymajesty
toluene --> benzaldehyde
Hi there,

So my horizontal oxidation reactor seems to be complete.

Features:
Wattage controll ...
29-1-2016 at 14:08
by: Jimmymajesty
Nitromethane, nitroethane, nitropropane synthesis via industrial route
I do not have ethane at hand, ofc the reaction products with ethane are simpler. My motive was the p ...
22-11-2015 at 02:46
by: Jimmymajesty
Nitromethane, nitroethane, nitropropane synthesis via industrial route
I totally redesigned the reactor today.

Upon disassembling after the test run the first wash flas ...
18-11-2015 at 14:48
by: Jimmymajesty
Nitromethane, nitroethane, nitropropane synthesis via industrial route
I did a testrun today with cc HNO3.

I flushed the setup with gas.
Heated up the reactor to 320 ...
15-11-2015 at 14:33
by: Jimmymajesty
Nitromethane, nitroethane, nitropropane synthesis via industrial route
I cut my hand pretty badly, now that the stitches are removed I gained back enough dexterity to make ...
8-11-2015 at 14:04
by: Jimmymajesty
Nitromethane, nitroethane, nitropropane synthesis via industrial route
Hi there

I finally scavenged all the parts to my new gas phase reactor, which happens to be good ...
23-10-2015 at 06:50
by: Jimmymajesty
Acetic Acid Distillation with an Entrainer
Ethyl acetate can be used but it is really difficult to remove all the water with it from a 20% hous ...
17-5-2015 at 12:25
by: Jimmymajesty
Oxidation of Isopropanol
byko3y I thought you were after an efficient catalyst, if your goal is to get 10+ liters of acetone ...
24-4-2015 at 00:47
by: Jimmymajesty
Bad Habits In The Lab
I just find it odd or rather a paradox when I see a smoking chemist. All chemists especially we hobb ...
23-4-2015 at 05:07
by: Jimmymajesty
Bad Habits In The Lab
I always wondered why smoking chemists (hobbyist or professional) need protective equipments like fu ...
22-4-2015 at 04:46
by: Jimmymajesty
Oxidation of Isopropanol
I did a run today.

-the IPA was brought to boil, then the wattage on the kanthal wire was set so ...
19-4-2015 at 11:03
by: Jimmymajesty
Making an Ozone Generator
For those who want to build an ozone generator with flyback, the oldest the tv is the better, in the ...
19-4-2015 at 07:25
by: Jimmymajesty
Silent discharge in preparative chemistry?
violet sin, thanks for the papers.

I tried out couple of things in the last days mainly with ace ...
19-4-2015 at 06:58
by: Jimmymajesty
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