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Synthesis of Chloroacetic acid
i tried it because i saw a comment suggesting using iodine as the catalyst and acetic anhydride to r ...
30-1-2024 at 15:29
by: Kloberth
Synthesis of Chloroacetic acid
and also the sodium acetate is useless in my opinion just a hassle trying to destill everything out ...
30-1-2024 at 08:08
by: Kloberth
Synthesis of Chloroacetic acid
well iodine doesnt work you just get finest tar in the end. i have tried in the past sulfur and it w ...
30-1-2024 at 08:07
by: Kloberth
Synthesis of Chloroacetic acid
My plan would be to use AcOH as solvent for Sodium acetate and a bit of Iodine as catalyst when bubb ...
30-1-2024 at 00:40
by: Kloberth
Praparation of Nitromethane
Ill try the reaction when I have time to synthesize more Chloroacetic acid and i also have to measur ...
27-1-2024 at 00:45
by: Kloberth
Praparation of Nitromethane
like this: https://youtu.be/8LSCJnqRjes?si=Eop8AqXyojwVk70g
26-1-2024 at 07:57
by: Kloberth
Praparation of Nitromethane
When preparing sodium nitrite from Nitrate via reduction you get a product contaminated heavily with ...
25-1-2024 at 11:58
by: Kloberth
High Boiling Solvents for HCl Synthesis to Prevent Flask Cracking
You do not need to worry about salt axpansion in that case. Only if you melt some salt then let it s ...
12-1-2024 at 01:12
by: Kloberth
Sm wiki looking weird
thank you!!
10-12-2023 at 08:51
by: Kloberth
Sm wiki looking weird
Recently my sm wiki looks like a unfinished html
Didnt change anything on my end.
Does anyone have ...
10-12-2023 at 07:01
by: Kloberth
Synthesis of disperse red 9
I would go with the 1-nitroanthraquinone to 1- aminoanthraquinone to the DR9.
The nitration of the ...
15-10-2023 at 13:25
by: Kloberth
Do i have Potassium Chromate?
watch explosions and fires video on this topic! he used calcium hypochlorite as the oxidiser.

htt ...
30-9-2023 at 08:20
by: Kloberth
NaClO from TCCA
i could but dont have it on hand

just wanted to know if there is a easy way to make it from stuff ...
14-9-2023 at 13:55
by: Kloberth
NaClO from TCCA
I did not find any other thread talking about this, but is it possible to prepare concentrated bleac ...
14-9-2023 at 08:22
by: Kloberth
Preparation of ionic nitrites
[rquote=686668&tid=52&author=Alkoholvergiftung]I ve never tried this way but i think its for ...
21-8-2023 at 04:11
by: Kloberth
Synthesis of Propylene Oxide (2-methyloxirane, 2-epoxypropane, etc.) via Chlorohydrin Intermediate
I have also looked into a possible rout to ethylene oxide in the past. From what I can piece togethe ...
4-8-2023 at 07:40
by: Kloberth
Synthesis of CAS 3179-63-3 or 3-Dimethylaminopropan-1-ol
Omg I completely forgot that wikipedia lists the sources below.
30-7-2023 at 22:12
by: Kloberth
Synthesis of CAS 3179-63-3 or 3-Dimethylaminopropan-1-ol
I am trying to synthesise an ester with this alcohol.

Finally at least some information on the s ...
29-7-2023 at 21:51
by: Kloberth
Synthesis of CAS 3179-63-3 or 3-Dimethylaminopropan-1-ol
I am trying to make this compound for a bigger synthesis I plan to do but I just cannot find any inf ...
29-7-2023 at 12:06
by: Kloberth
The First Room-Temperature Ambient-Pressure Superconductor
[rquote=686094&tid=159753&author=Rainwater]
But the 0.00001 torr. Thats not easy.
Have to ...
28-7-2023 at 21:39
by: Kloberth
Planned Polyethylene Glutamate Synthesis
How would you quaternize the amino group. (After a quick gpt explanation I am now wondering how this ...
22-6-2023 at 01:51
by: Kloberth

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