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Help with synthesis of substituted pyridine: 5-Bromo-6-Methyl-Nicotinic Acid.
2-Picoline -> sulfonic acid -> nitrile -> bromonitrile (questionable) -> the desired com ... |
27-4-2025 at 16:13
by: MaeBorowski |
Phenyl isonitrile: the worst stench ever.
For me, the smell of phenyl isocyanide resembles one of wet concrete but is emetic and scary. I was ... |
28-2-2024 at 19:07
by: MaeBorowski |
95% Ethanol from E85 Fuel
Fractional distillation, counterflow extraction with some water, fractional distillation again? |
27-2-2023 at 12:36
by: MaeBorowski |
Confusion on SO3 Synthesis
HCl is stronger than H2SO4 but here we are. Disulfuric acid isn't stable at elevated temperature and ... |
24-12-2022 at 13:21
by: MaeBorowski |
Cleaning glassware and other equipment
I found that boiling sulfuric acid destroys any crap including elemental carbon, sulfur, barium sulf ... |
20-1-2022 at 16:06
by: MaeBorowski |
Handling of Aniline
I worked twice with a significant amount of pure aniline (about 60 g). I think several drops on your ... |
20-1-2022 at 15:11
by: MaeBorowski |
Solvents ?
Ether looks like a bad solvent for Friedel-Crafts because of the nucleophilic oxygen. Hexane, as wel ... |
20-1-2022 at 14:54
by: MaeBorowski |
Successful distillation of antifreeze
This saturday I did the distillation of used antifreeze obtained from my father.
It is green liqui ... |
17-1-2022 at 18:15
by: MaeBorowski |
Oxalyl Chloride Challenge
And how will this help in the synthesis of oxalyl chloride? |
5-8-2021 at 14:40
by: MaeBorowski |
Oxalyl Chloride Challenge
[rquote=657229&tid=82462&author=mr_bovinejony]Bromine is much easier to handle than chlorine ... |
2-4-2021 at 17:53
by: MaeBorowski |
Oxalyl Chloride Challenge
[rquote=657181&tid=82462&author=clearly_not_atara]This is a pretty stark example of textbook ... |
29-3-2021 at 07:32
by: MaeBorowski |
Oxalyl Chloride Challenge
[rquote=656986&tid=82462&author=Triflic Acid]And, how are you going to deal with that nice c ... |
27-3-2021 at 18:09
by: MaeBorowski |
Oxalyl Chloride Challenge
everyone is lazy
IMHO, the most appropriate way is the decomposition of chlorination products of ... |
13-3-2021 at 16:55
by: MaeBorowski |
