| Search |
| [Next Page] |
Preparation of chlorosulfonic acid derived protecting groups
Hi All, I'm currently trying to make some sulfonic acid protecting groups for some upcoming project ... |
1-12-2022 at 11:05
by: Monoamine |
Hydrolysis of alkyl halides
Would NaBH[sub]4[/sub] or LiAlH[sub]4[/sub] reduce aliphatic halogens to H?
For instance would
... |
1-12-2022 at 04:48
by: Monoamine |
Question about amine protection for Grignard reaction
All nice tip! Than you folks. I'll give it a try.  |
4-4-2022 at 08:18
by: Monoamine |
Propionyl chloride with cyanuric chloride and anger
So what's the source of the chlorides? Neither the cyanuric acid, the water, or the propionic acid h ... |
2-4-2022 at 06:42
by: Monoamine |
Stoichiometry for Al(Ga) amalgam reduction of nitroalkane
So I've never done a reduction with an amalgam yet because mercury salts scare the bedoodles out of ... |
1-4-2022 at 20:57
by: Monoamine |
Preparation of Diethyl Sulfate
Impressive work! Thank you for sharing this detailed procedure.
I have a few questions if you do ... |
26-3-2022 at 15:17
by: Monoamine |
Can I open lithium thionyl chloride batteries?
But, yes. Do be careful not to short the battery. You definitely don't want to get splashed with thi ... |
26-3-2022 at 13:54
by: Monoamine |
Can I open lithium thionyl chloride batteries?
It's certainly doable. I did it before and had no issues.
You can read my notes on how to do it h ... |
26-3-2022 at 08:42
by: Monoamine |
Question about Zinc Mercury amalgam safety for Clemmensen reduction
I was wondering if anybody knows how to safely handle and work with Zn(Hg) zinc mercury amalgam for ... |
26-3-2022 at 00:55
by: Monoamine |
Question about amine protection for Grignard reaction
Imagine you need to form a Grignard reagent from a molecule containing both a halogen (from which we ... |
26-3-2022 at 00:27
by: Monoamine |
Question: Storing chlorine in solution
Thank you for all the advice! I also read that sulfuryl chloride can be used as a source of Cl-, as ... |
13-3-2022 at 18:26
by: Monoamine |
Question about SO2 generation
I'm currently trying to make some sulfuryl chloride (SO[sub]2[/sub]Cl[sub]2[/sub]), which can be mad ... |
12-3-2022 at 13:12
by: Monoamine |
Question about Friedel Crafts acylation and acid chlorides
Aaaand... were back.
Ok I did TLC with pure naphthalene and with pure nitrobenzene to see if they ... |
5-3-2022 at 22:47
by: Monoamine |
Question about Friedel Crafts acylation and acid chlorides
Actually, looking at these again I'm noticing that the brightest (orange) spot is actually still at ... |
5-3-2022 at 17:24
by: Monoamine |
Question about Friedel Crafts acylation and acid chlorides
I used nitrobenzene as the solvent, since it is polar enough to dissolve the AlCl3 complex so the re ... |
5-3-2022 at 17:02
by: Monoamine |
Analysis
So I finally tried this experiment and got a decent looking brown oil that had a smell of orange pee ... |
5-3-2022 at 00:47
by: Monoamine |
Triethylsilane
Actually, the method from this paper is for trypropylsilane, but this should be readily adaptable to ... |
1-3-2022 at 21:16
by: Monoamine |
Yes!
I'm actually super interested in this topic!! I just ordered all the raw materials I need to synthes ... |
1-3-2022 at 21:01
by: Monoamine |
a novel phenylmorpholine synthesis aka preludin
If preludin is what you want as the end-product, then you may just want to look into obtaining a chl ... |
1-3-2022 at 20:49
by: Monoamine |
Question: Storing chlorine in solution
I'm wondering if there is a way to make a stable solution of chlorine.
For instance would chlori ... |
19-2-2022 at 09:08
by: Monoamine |
Question about Friedel Crafts acylation and acid chlorides
Hi Fery, thank you for the link for the reagent supplier! My mouth is watering seeing all the wonder ... |
3-2-2022 at 21:42
by: Monoamine |
Question about Friedel Crafts acylation and acid chlorides
Thank you for the tips!
I'm planning to use anhydrous AlCl3 as the catalyst. From what I read, th ... |
2-2-2022 at 23:05
by: Monoamine |
Question about Friedel Crafts acylation and acid chlorides
I'm planning to do my first acylation experiment soon, but I've never done this reaction, so I'm a b ... |
2-2-2022 at 05:35
by: Monoamine |
Leonid Learner's Book
Hi Basement,
Props for mentioning Leonid Lerners book: "Small scale synthesis of laboratory reag ... |
29-1-2022 at 14:01
by: Monoamine |
Solvents ?
I really don't understand why people seem to use chlorinated solvents for performing AlCl[sub]3[/sub ... |
19-1-2022 at 11:32
by: Monoamine |
| [Next Page] |
