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IKA thermocouples for sale
Greetings,
I would have three IKA thermocouples available I don’t need anymore, two ETS-D5 and o ... |
19-7-2025 at 04:46
by: Niklas |
11 cm glass flange
Ended up getting things made by my university glassblower, he was so kind to do it for free 
[ ... |
8-7-2025 at 07:40
by: Niklas |
Energetic salts of cubane
That’s quite a neat idea, I was gonna order some aminoguanidine from Laboratoriumdiscounter soon a ... |
27-6-2025 at 22:22
by: Niklas |
Energetic salts of cubane
Greetings,
As you may know I‘m currently doing quite a bit of work on cubanes, documented on thi ... |
23-6-2025 at 12:46
by: Niklas |
Improved synthesis of endo-2,4-Dibromodicyclopentadiene-1,8-dione (“Bisketone“)
A 500 ml round bottom flask, equipped with an egg-shaped stirbar, was charged with 205 ml of concent ... |
21-6-2025 at 12:54
by: Niklas |
Improved one-pot synthesis of endo-2,4-Dibromodicyclopentadiene-1,8-dione diethylene ketal (“Bisketal“)
So I‘ve decided that I would stick to the one-pot procedure I described before (with the modificat ... |
19-6-2025 at 02:33
by: Niklas |
Synthesis of Polyethylene cubane-1,4-dicarboxylate (“Cubane-PET“)
Hello again,
I did a lot of testing regarding the purification of the diester lately, and I will s ... |
14-6-2025 at 02:46
by: Niklas |
Decarboxylation of Phenylalanine to Phenylethylamine with Acetophenone
Triturating with some acetone should get rid of most the remaining colored impurities I would guess. |
5-6-2025 at 12:28
by: Niklas |
Synthesis of cubane and cubane related compounds / derivatives
I did a first attempt of the cubane-1,4-diamine synthesis I proposed above, and while it unfortunate ... |
3-6-2025 at 12:55
by: Niklas |
Hexaphenyl benzene synthesis
On a different note, this made me remember this thing I was thinking about a long time ago, nanograp ... |
2-6-2025 at 23:12
by: Niklas |
Hexaphenyl benzene synthesis
Nice synthesis!
Using benzophenone as a solvent, never seen that before, great to see the yields be ... |
2-6-2025 at 22:30
by: Niklas |
Some considerations on the synthesis of the cubylethylamine-unit
On the topic of the planned cubane psychedelics, there is one aspect that seems really simple on fir ... |
2-6-2025 at 02:35
by: Niklas |
Synthesis of cubane and cubane related compounds / derivatives
That is actually on by bucket list of cubane substances to make, considering my early research was i ... |
28-5-2025 at 11:22
by: Niklas |
Some analysis of the dimethylesters
Finally got around to doing some analysis of the final products, and things appear to have indeed be ... |
28-5-2025 at 07:28
by: Niklas |
11 cm glass flange
Hm yeah, I guess I‘ll go ask my university glassblower.. Didn’t think of the option of a PTFE-li ... |
27-5-2025 at 23:16
by: Niklas |
11 cm glass flange
So, on Sunday I got a 10 l round bottom flask of Kleinanzeigen for 50€ (just couldn’t say no to ... |
27-5-2025 at 00:47
by: Niklas |
(Improved) small scale synthesis of dimethyl cubane-1,4-decarboxylate from the bisketone
So I redid the whole synthesis starting from my bisketone at the same scale (4,4 mmol), and even tho ... |
26-5-2025 at 10:37
by: Niklas |
Synthesis of cubane and cubane related compounds / derivatives
[rquote=700854&tid=161053&author=Niklas]So, first of all, by concentrating the mother liquor ... |
24-5-2025 at 02:35
by: Niklas |
Synthesis of cubane and cubane related compounds / derivatives
Had some thought on hypercubane as well lately, didn’t get anywhere with the idea I once mentioned ... |
23-5-2025 at 13:28
by: Niklas |
Synthesis of cubane and cubane related compounds / derivatives
So, first of all, by concentrating the mother liquors of the diacid to a volume of 10 ml, filtering ... |
21-5-2025 at 11:34
by: Niklas |
Synthesis of cubane and cubane related compounds / derivatives
The total yield of that small scale run would be a kinda disappointing 8,9% (80%, 47%, 71,8%, 35,8%, ... |
20-5-2025 at 09:28
by: Niklas |
Small scale synthesis of Dimethyl cubane-1,4-dicarboxylate
The most typical catalyst used for this esterification by far is hydrochloric acid, as has been desc ... |
20-5-2025 at 09:13
by: Niklas |
tramadol => faxeladol
Birch conditions are able to “hydrogenate“ alkenes to the trans products.
Also been thinking wh ... |
19-5-2025 at 07:46
by: Niklas |
Synthesis of cubane and cubane related compounds / derivatives
@wildfyr The conversion of the UV cyclisation itself should be basically quantitative, as the lamp i ... |
19-5-2025 at 07:32
by: Niklas |
Synthesis of cubane and cubane related compounds / derivatives
Having a type of immersion well reactor is by far the most efficient way to perform the UV step yeah ... |
19-5-2025 at 02:01
by: Niklas |
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